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991.
D. Galvan V. Ocelík Y. Pei B. J. Kooi Jeff Th. M. De Hosson E. Ramous 《Journal of Materials Engineering and Performance》2004,13(4):406-412
TiB/Ti-6Al-4V metal-matrix composite (MMC) layers were produced on Ti-6Al-4V substrates by laser cladding. A TiB2/Ti powder mixture was used as a precursor to obtain a dispersion of TiB needles in the Ti alloy matrix, with the aid of an
exothermic reaction between TiB2 and Ti. A eutectic microstructure was obtained that consisted of an extremely homogeneous dispersion of TiB eutectic needles
in the Ti alloy matrix, having a volume fraction as high as 0.33. Also, an equilibrium-like microstructure was found, consisting
of a dispersion of both primary and eutectic TiB needles inside the Ti alloy matrix. An analysis of the geometry of the layers
was performed and proved successful in determining the percentage of B. Further, it correctly predicted the variation of atomic
B content as a function of laser power. The relative wear resistance coefficient, defined as the wear coefficient of the uncoated
matrix divided by that of coating, shows an improvement by a factor as high as 1500 for the eutectic microstructure.
This paper was presented at the 2nd International Surface Engineering Congress sponsored by ASM International, on September
15–17, 2003, in Indianapolis, Indiana, and appeared on pp. 411–18 of the Proceedings. 相似文献
992.
研究了用溶胶.凝胶法制备ZAO薄膜的工艺、掺杂及其显微结构。用六水合氯化铝在溶胶中引入Al2O3。掺杂Al的含量为1%,3%,6%和9%。用浸涂法在石英玻璃基片上浸涂ZnAO薄膜,研究了热处理、掺杂对ZAO薄膜相组成和显微结构的影响。X射线衍射结果表明,衍射图谱中无Al2O3的衍射峰。随着掺杂量的变化,ZnO主要衍射峰的位置、晶面间距均发生了有规律的变化,说明Al掺杂进了ZnO晶格中。研究结果表明,溶胶浓度、Al掺杂量、热处理温度都影响薄膜的显微结构。当薄膜厚度较大时,热处理过程中ZnO晶粒呈现明显的择优生长现象。 相似文献
993.
Lars Arnberg Ragnvald H. Mathiesen 《JOM Journal of the Minerals, Metals and Materials Society》2007,59(8):20-26
The directional solidification of thin alloy sheets in a Bridgman furnace has been studied by x-radiography using high-brilliance
synchrotron x-radiation in combination with a low-noise, fast-readout camera. Spatial resolutions down to 1.5 μm and a temporal
resolution of about 0.15 s have permitted real-time video microscopy of microstructural evolution during columnar and equiaxed
dendrite growth and eutectic and monotectic growth. The technique has also allowed for direct observations of important solidification
phenomena such as dendrite fragmentation and porosity formation, primarily in aluminium alloys. As a result, insights have
been gained into mechanisms of dendrite fragmentation, criteria for dendrite tip kinetics and interface stability during transient
growth, and microstructure formation mechanisms during monotectic solidification. The results are expected to be important
for validation of dendrite growth models. This paper presents a review of the technique as well as examples of images obtained
during solidification of aluminum alloys. 相似文献
994.
用离子束增强沉积方法制备了SiN薄膜,其中Si由一束Ar离子从Si靶上溅射下来,在溅射沉积的同时,以一束N离子轰击正在沉积的膜层,于是获得了SiN膜。采用卢瑟福背散射、红外光谱和透射电镜对膜层的成分和结构进行了分析,结果表明:膜面平整,膜层为非晶或微晶结构,由Si和βSi3N4组成 相似文献
995.
The effects of joint design on the mechanical properties of AL7075-T6 aluminum sheet were studied on the latest automated
gas-tungsten arc-welding system. Using ER5356 filler metal, full-penetration welds were made on workpieces with various included
joint angles. Testing of the mechanical properties of the joints was done in the as-welded, naturally aged, and postweld heat-treated
conditions. The results show that by using crack-resistant filler, and by selecting the proper joint design and postweld heat
treatment, strong, dependable welds can be produced on thin AL7075 sheet material. An elasticity model of the weld joint was
established to help understand the mechanical behavior of the joints. An undermatched joint design is shown to be capable
of achieving a joint strength that matches the strength of the base alloy. 相似文献
996.
Kyung-Man Moon Hwang-Rae Cho Myung-Hoon Lee Sung-Kyu Shin Sung-Cheol Koh 《Metals and Materials International》2007,13(3):211-216
The differences between the general corrosion and microbiologically influenced corrosion (MIC) of steels were investigated
in terms of its electrochemical behavior and surface phenomena. The corrosion potential of steels in the absence of SRB (sulfate-reducing
bacteria) shifted to a negative value with the immersion time. However, the potential of the presence of SRB shifted to a
positive value after 30 days' incubation, indicating the growth of SRB biofilms on the test metal specimens and the formation
of corrosion products. In addition, the color of a medium inoculated with SRB changed from gray to black. The change in color
appeared to be caused by the formation of pyrites (FeS) as a corrosion product, while no significant change in color was observed
in a medium without SRB inoculation. Moreover, corrosion rates of various steels tested for MIC were higher compared to those
of steels in the absence of SRB. In particular, the corrosion current density of TMCP steels in the presence of SRB was larger
than that of other steels. Pitting corrosion was also observed at the surface of all steels in the SRB-inoculated medium.
The pitting corrosion likely occurred due to SRB that was associated with the increasing corrosion rates through increasing
cathodic reactions, which caused a reduction of sulfate to sulfide as well as the formation of an oxygen concentration cell. 相似文献
997.
Joon-Ho Shin Jong-Hwa Kim Ki-Won Kim Hyo-Jun Ahn 《Metals and Materials International》2002,8(4):417-422
Lead acid batteries have had restricted applications because of relatively low energy density below 50Wh/kg. Many efforts have achieved lighter battery components such as separators, connections and containers etc. Thus, the most important problem of the lead acid battery is to improve the low capacity of the active material in the positive electrode. The purpose of this study is to improve the utilization of the active material in the lead dioxide electrode for the lead acid battery through the production of lead oxide with better physicochemical characteristics through cementation. A cementation reaction was performed in 1.0wt.%HCl solution using pure magnesium plate as the reductant. We investigated the utilization of the active material and discharge characteristics of the positive electrode with a current density ranging from 3.4 to 108.8mAcm−2. As a result, the active material utilization was about 72% at 3.48 mAcm−2 and increased with decreasing current density. The discharge characteristics according to current density are especially very good at high current density 相似文献
998.
999.
Youtao Xie Xuebin Zheng Xuanyong Liu Chuanxian Ding 《Journal of Thermal Spray Technology》2007,16(4):588-592
Titanium/dicalcium silicate composite coatings with different ratios (weight ratios as Ca2SiO4: Ti = 3:7, 5:5, 7:3) were prepared by plasma spraying. Effects of titanium addition on coating properties, such as bonding
strength, flexural modulus, and dissolution in simulated physiological environment, were studied. Results showed that the
bonding strength between coating and Ti-6Al-4V substrate increased with increase of titanium content in the composite coatings.
It was explained by the narrowed dissimilarity of thermal expansion coefficients between the coatings and substrates. Degradation
of mechanical properties after immersion in simulated body fluid was also studied. The dissolution of dicalcium silicate in
the composite coatings resulted in the decrease of flexural strength and flexural modulus of the coatings in the simulated
physiological environment. The higher titanium content in the composite coatings, the stabler are the composite coatings in
the physiological environment. 相似文献
1000.
用循环伏安法、恒电位电解断电后的电极电位-时间曲线、电位阶跃法和X射线衍射法研究了Cu电极在NaCl-KCl-DyCl3熔体中的电化学行为,获知Dy在Cu电极上的还原过程是首先生成Dy-Cu合金,然后才析出纯金属Dy.测得Dy-Cu合金在1073K的标准生成自由能;在1023-1143K范围内,Dy原子在Dy-Cu合金相中的扩散系数与温度的关系式为lnD=-67.1×103/RT-15.8,其扩散活化能为67.1kJ·mol-1.用自耗阴极法制取了Dy-Cu中间合金并对其工艺条件进行了探讨。电解制取了含Dy高达92%(质量分数)的Dy-Cu中间合金,其组成为DyCu和Dy,电流效率可达80%. 相似文献