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51.
A formation of poly(vinyl alcohol) (PVA)/alumina gel composite was investigated with a viewpoint of compatibility of the composite. An alumina sol was prepared from aluminium iso-propoxide (Al(iPro)3). The alkoxide was hydrolyzed and the resultant hydrate was peptized to a clear sol with acetic acid. The composite were transparent in whole content of alumina. The effects of dispersed alumina on the sorption of water and mechanical properties of composite were examined. The composites containing PVA 40–50% are flexible. They are folded in various forms and can be drawn five times the initial length in humid state. The residues obtained by calcination to remove PVA at 600°C keep its original form and transparency. 相似文献
52.
In order to obtain quantitative relationship between (0002) texture intensity and hot rolling conditions, conventional rolling experiments on AZ31 magnesium alloys were performed with 20%–40% reductions and temperatures within the range of 300–500 °C. Shear strain and equivalent strain distributions along the thickness of the rolled sheets were calculated experimentally using embedded pin in a rolling sheet. Rolling microstructures and textures in the sheet surface and center layers of the AZ31 alloys were measured by optical microscopy (OM), X-ray diffractometry (XRD) and electron back scatter diffraction (EBSD). Effects of the rolling strain, dynamic recrystallization (DRX) and twinning on the texture evolution of the AZ31 alloys were investigated quantitatively. It is found that the highest (0002) basal texture intensities are obtained at a starting rolling temperature of 400 °C under the same strain. Strain–temperature dependency of the (0002) texture intensity of the AZ31 alloy is derived. 相似文献
53.
The Akashi Kaikyo (Strait) Bridge, one of the major bridges of the Honshu-Shikoku bridge network connecting the main island and the Shikoku island, is the world's longest suspension bridge with a center span of about 2,000 m. The bridge was constructed over the Akashi Strait and opened to traffic in 1998 after a construction period of about 10 years. The granite stratum in the Akashi Strait was very deep, while the granite stratum provides the foundations for the other long span bridges which have been constructed in Japan. Three of the four foundations had to be constructed on either a weakly cemented gravelly soil deposit or a sedimentary soft rock layer. The geological structure was carefully investigated and the geotechnical properties, in particular the strength and deformation characteristics of these geomaterial types, were carefully evaluated. To this end, a comprehensive series of advanced triaxial compression (TC) tests were performed on rotary core tube samples of sedimentary soft rock after it was found that the due design was not possible based on unconfined compression tests. Both CD and CU TC tests and cyclic undrained triaxial tests were performed on rotary core tube samples (30 cm in dia.) of the gravelly soil. Based on the data, the long-term and seismic stabilities of the foundations were evaluated. The importance of strain- and pressure-dependent nonlinear stress-strain behaviour at small strains, as well as accurate strain measurements in the laboratory stress-strain tests, was confirmed by analyzing the full-scale behaviour of the foundation during and after construction and comparing the back-calculated stiffness values with those obtained from laboratory stress-strain tests, pressure-meter tests, plate loading tests and field shear wave velocity measurements. 相似文献
54.
The Sonogashira-Hagihara polymerization of 3′,5′-diiodo-N-α-tert-butoxycarbonyl-l-tyrosine methyl ester (1) and 3′,5′-diiodo-N-α-tert-butoxycarbonyl-O-methyl-l-tyrosine methyl ester (2) with para-diethynylbenzene (3) was carried out to obtain optically active poly(m-phenyleneethynylene-p-phenyleneethynylene)s [poly(1) and poly(2)] with Mn’s ranging from 9900 to 15,000 in 80-87% yields. Poly(1) exhibited intense CD signals in DMSO and THF, but did not in CH2Cl2, indicating that it took a predominantly one-handed helical conformation in the former two solvents. On the other hand, there was no evidence for poly(2) to take a helical structure in these solvents. Poly(1) turned the CD sign at 390 nm from plus to minus in DMSO/H2O = 9/1 (v/v) by the addition of NaOH. Alkaline hydrolysis of ester moieties of poly(1) and poly(2) gave the corresponding polymers having carboxy groups [poly(1a) and poly(2a)]. Poly(1a) and poly(2a) increased the CD intensity by the addition of NaOH. 相似文献
55.
56.
NAZAMID BIN SAARI SHUJI FUJITA RYUICHI MIYAZOE MASAHIKO OKUGAWA 《Journal of Food Biochemistry》1995,19(4):321-327
Activities and some other properties of ascorbate oxidases (AAO) from the fruits of family Cucurbitaceae were investigated. The peel and the flesh of seven varieties had activities ranging between 35–56500 units/mg protein and 14–1250 units/mg protein, respectively. AAO from different varieties had a similar pH optimum of around 6–6.5 and a broad pH stability ranging from pH 5 or 6 to pH 10 or 11. These properties appear to be conserved in the AAO's from the family of Cucurbitaceae. The AAO's of melon cv. andes, kinsho and papaya were more susceptible to heat denaturation than AAO from pumpkin. 相似文献
57.
Takuya Kitabatake Tetsuo Uchikoshi Fumio Munakata Yoshio Sakka Naoto Hirosaki 《Journal of the European Ceramic Society》2012,32(7):1365-1369
The compaction of a Eu-doped Ca-α-SiAlON phosphor powder was performed by electrophoretic deposition (EPD). The effect on the adhesion and optical properties of the silica precursor as both a binder of the powder and a filler of the air voids were evaluated. The adhesion of the silica impregnated composite film to the silica glass substrate was characterized by the tape test. The improvement of the external quantum efficiency was confirmed from the PL spectra measurement after the silica impregnation. The temperature dependence of the external quantum efficiency was also investigated in order to discuss the advantage of using the silica precursor as a binder for high-brightness LED applications. 相似文献
58.
Ronaldo Fumio Hashimoto Junior Barrera 《Journal of Mathematical Imaging and Vision》2001,15(3):197-216
W-operators are discrete set operators that are both translation invariant and locally defined within a finite window W. A particularly interesting property of W-operators is that they have a sup-decomposition in terms of a family sup-generating operators, that are parameterized by the operator basis. The sup-decomposition has a parallel structure that usually is not efficient for computation in conventional sequential machines. In this paper, we formalize the problem of transforming sup-decompositions into purely sequential decompositions (when they exist). The techniques were developed for general W-operators, specialized for increasing W-operators and applied on operators built by compositions of dilations and erosions. 相似文献
59.
60.
Yoshihisa Maruyama Fumio Yamazaki 《Journal of Wind Engineering & Industrial Aerodynamics》2006,94(4):191-205
In expanding expressway networks in Japan, various types of structures have been constructed, e.g., long span bridges and bridges with high piers. The expressway structures are well designed for the external dynamic forces, e.g., earthquakes and strong winds. However, for further safety promotion of the expressway networks, it is important to evaluate the drivers’ responses under strong dynamic disturbances. The present authors have investigated the moving stability of a vehicle under seismic motion based on both numerical simulation and virtual experiments using a driving simulator. Strong crosswind is considered as another factor that makes it difficult for drivers to control their vehicles. This study investigates the moving stability of a vehicle under strong crosswind based on numerical analyses and driving simulator experiments. To predict the future position of a moving vehicle including the reaction of a driver, the second-order predictable correction model is used in the numerical analyses. The results obtained from the numerical and experimental studies are compared and the validity of the driver model is discussed. It is expected that this research is helpful for the decision-making of expressway closure under strong wind and the design of wind barriers. 相似文献