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991.
探讨了液下气泡检漏法的基本原理、泄漏率计算方法以及检漏精度和分辨率。应用该方法对石棉橡胶垫片的泄漏率进行了测定 ,试验结果与采用集漏空腔增压法测得的泄漏率具有较好的可比性。分析了液下气泡法用于工程实际时应注意的问题。 相似文献
992.
双效变压精馏节能技术的应用 总被引:5,自引:0,他引:5
以新开发设计的C-1305塔和C-1303塔联塔取代耗能大户DA-303塔,使C-1305塔顶热物为的汽化潜热在C-1303塔的再沸器中得到二次利用,从而形成双效变压精馏节能系统达到节能增效的目的。 相似文献
993.
994.
995.
Polypropylene (PP) nanocomposites filled with the pristine multi‐wall carbon nanotubes (CNTs) and the purified CNTs were prepared by melt blending. The microstructure and linear viscoelastic properties wereinvestigated using rheological and morphological measurements. The results show that the purified CNTs disperse uniformly in the PP matrix. At low frequencies, frequency dependence of modulus weakens clearly with the addition of the CNTs, indicating that the long‐range motion of the polymer chains is restrained by the presence of the CNTs. Percolation networks form when the loading levels achieve up to 3 and 1.5 wt% for the composites with the pristine CNTs (PPCNTs) and the purified CNTs (PPcCNTs), respectively. The linear relaxation modulus increases with increasing loading level. And for composites with loading levels above percolation concentration, the modulus appears to reach a plateau at long time scales due to the formation of percolation network. Tensile strength and impact strength are simultaneously improved with the addition of the CNTs. The better the dispersion of the CNTs, the greater the improvement of the tensile strength and the impact strength. POLYM. ENG. SCI., 2012. © 2012 Society of Plastics Engineers 相似文献
996.
In this study, 2‐hydroxyethyl methacrylate and N‐isopropyl acrylamide was block grafted onto the polypropylene macroporous membrane surface by photo‐induced reversible addition‐fragmentation chain transfer (RAFT) radical polymerization with benzyl dithiobenzoate as the RAFT agent. The degree of grafting of poly(2‐hydroxyethyl methacrylate) on the membrane surface increased with UV irradiation time and decreased with the chain transfer agent concentration increasing. The poly(2‐hydroxyethyl methacrylate)‐ grafted membranes were used as macro chain transfer agent for the further block graft copolymerization of N‐isopropyl acrylamide in the presence of free radical initiator. The degree of grafting of poly(N‐isopropyl acrylamide) increased with reaction time. Furthermore, the poly(2‐hydroxyethyl methacrylate)‐ grafted membrane with a degree of grafting of 0.48% (wt) showed the highest relative pure water flux and the best antifouling characteristics of protein dispersion. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2012 相似文献
997.
Hongbo Gu Yudong Huang Xi Zhang Qiang Wang Jiahua Zhu Lu Shao Neel Haldolaarachchige David P. Young Suying Wei Zhanhu Guo 《Polymer》2012,53(3):801-809
Magnetic polyaniline (PANI) polymer nanocomposites (PNCs) reinforced with magnetite (Fe3O4) nanoparticles (NPs) have been successfully synthesized using a facile surface initiated polymerization (SIP) method. The chemical structures of the PANI/Fe3O4 PNCs are characterized by Fourier transform infrared (FT-IR) spectroscopy. The thermal stability of the PANI/Fe3O4 PNCs is performed by thermogravimetric analysis (TGA). Both transmission electron microscopy (TEM) and scanning electron microscopy (SEM) are used to characterize the morphologies of the PANI, Fe3O4 nanoparticles (NPs) and the PNCs. X-ray diffraction (XRD) shows a significant effect of the Fe3O4 NPs on the crystallization structure of the formed PANI. The dielectrical properties of these PNCs are strongly related to the Fe3O4 nanoparticle loadings and unique negative permittivity is observed in all the samples. Temperature dependent resistivity analysis from 50 to 290 K reveals a quasi 3-dimension variable range hopping (VRH) electron conduction mechanism for the nanocomposite samples. The PNCs do not show hysteresis loop with zero coercivity, indicating the superparamagnetic behavior at room temperature. The PNCs with 30 wt% Fe3O4 NP loading exhibit a larger positive magnetoresistance (MR = 95%) than 53% of the pure PANI. 相似文献
998.
In this paper, amphiphilic biodegradable methoxy-poly(ethylene glycol)-poly(l-histidine)-poly(l-lactide) (mPEG–PH–PLLA) triblock copolymers with pH sensitivity were synthesized. The properties of mPEG–PH–PLLA triblock copolymers were investigated by GPC, 1H NMR, DSC, TGA, XRD and polarized optical microscopy. The results showed that the thermal properties of the triblock copolymers varied with the chain length of PH blocks. The glass transition temperatures (Tg) of the triblock copolymers increased with increasing poly(l-histidine) chain length. The morphologies of PLLA crystals changed from spherulite to dendritic crystal. Moreover, the crystallization rate of triblock copolymers was faster than that of PLLA homopolymer. The pH sensitivity of the self-assembled mPEG–PH–PLLA nanoparticles was investigated. The mean diameter and morphology of the nanoparticles were characterized by DLS, AFM and TEM. The results showed that the mean diameter of mPEG45–PH30–PLLA82 nanoparticles in pH = 5.0 was smaller than that in pH = 7.4. 相似文献
999.
A new type of stretchable poly(caprolactone)/graphene oxide (PCL/GO) aerogel with fast chemo‐responsive shape memory effect is fabricated by one‐step method of a sol‐gel procedure. The PCL/GO aerogels show uniformly circular and interconnected pores formed by twisted PCL nanolayers. GO platelets improve the crystallinity of PCL and increase the fracture stress and strain by 150% and 300% respectively, although the GO loading is only 0.5%. The dramatic increment of break strain is attributed to the uniform and circular pores that can afford large deformation and the interaction of GO and PCL. The aerogels can be programmed by external stress at ambient temperature without heating and recover upon ethyl acetate (EA) in 1 s. The fast chemo‐responsive shape recovery is ascribed to the fast wrinkle of the PCL nanolayers that decrease the diffusion time greatly and the interconnected micrometer pores that are in favor of penetrating for EA molecules. 相似文献
1000.
AbstractThe impacts of using radio frequency (RF) energy to dry purple-fleshed potatoes were investigated and compared to infrared radiation (IR) and microwave (MW) drying techniques. The gelatinization rate, color, flavor, morphological, and structural characteristics, thermodynamic properties, as well as antioxidant capacity were examined. The results indicated that the drying time of RF (70?min) and MW (21?min) were shorter than IR (105?min). The gelatinization ratio of MW, RF, and IR were 94.4?±?2.0, 88.3?±?1.4, and 64.5?±?1.1%, respectively. The degree of crystallization of purple-fleshed potato powder decreased with all three drying methods. RF-dried potatoes were able to retain higher polyphenols (loss rate: 4.3%), total anthocyanin (3.7%), and total flavonoid content (35.1%), whereas IR showed the lowest retention. The content of polyphenols also decreased significantly. Furthermore, after RF heating, the scavenging of free radicals was higher compared to MW and IR. 相似文献