甲基丙烯酸三氟乙酰氧乙酯的聚合

对甲基丙烯酸三氟乙酰氧乙酯(TFAOEMA)的阴离子聚合及原予转移自由基聚合进行了研究。常用的阴离于引发剂如丁基锂、1，1-二苯基已基锂等很难引发TFAOEMA的阴离子聚合，而碱性较弱的引发剂如三乙基铝却容易引发，且产率较高。以氯化亚铜、五甲基二乙基三胺、溴代丙酸乙酯为引发体系的TFAOEMA的本体原子转移自由基聚合符合活性聚合特征。但在四氢呋喃为溶剂的原子转移自由基聚合中却存在活性中心失活现象。以末端含卤素的聚甲基丙烯酸甲酯为大分子引发剂，引发TFAOEMA的原子转移自由基聚合，得到了含氟双嵌段聚合物。     

基于DSP+FPGA的扩频接收机快捕技术

提出一种在接收信号具有显著的多普勒频移的不确定性条件下,采用全数字的、适宜于扩频码和载波快速同步的新型扩频接收机结构。该接收机能在极短时间内建立快速同步,有效地实现实时突发通信。     

溅射靶材的应用及制备初探

随着电子及信息产业突飞猛进的发展，世界溅射靶材的需求越来越多，本文介绍了靶材的发展概况、分类和应用情况，以及靶材的特性要求．探讨Ni-Cr合金靶材的制备工艺，结果表明，产品能满足靶材特性要求。     

1400-1500 nm,Different Material-doped Raman Fiber Lasers Pumped by Nd∶YVO_4 Laser

Different material-doped Raman fiber lasers with very high efficiency operating in continuous-wave are presented.With 1 W Nd∶YVO 4 laser pumping at wavelength of 1 342 nm, single mode output power of above 500 mW (optical-to-optical conversion efficiency of 50%) is simulated in the range of 1 400-1 500 nm.Using high-germanium,high-phosphate and high-borate silicate fibers as the gain medium,laser output at wavelengths of 1 420,1 450,1 480 and 1 495 nm can be achieved with different geometries,which are just as pumping C-band and L-band distributed Raman fiber amplifiers.     

含氚废水水泥固化实验研究

研究用水泥固化处理氚废水,并选择了最佳配方:水与灰的重量比=0.45～0.5,水泥与石膏重量比=5∶1。用IAEA推荐的方法做浸出实验。为了减少水泥固化体中氚的浸出量,实验了几种涂层材料。沥青涂层可将固化体氚的浸出率降低1～2个量级。     

Preparation of nanosized titania powder via the controlled hydrolysis of titanium alkoxide

By controlling the hydrolysis of titanium butoxide, followed with or without an ethanol washing process, the preparation of nanoscale titania powder was studied in detail. The characteristics of different powders produced by the direct precipitation (without an ethanol wash) and ethanol wash processes were studied by X-ray diffraction, transmission electron microscopy, BET, thermogravimetry and differential thermal analysis techniques. By comparison, it was found that both the direct precipitation and ethanol wash methods can obtain slightly agglomerated nanoscale titania powders of less than 15 nm, but the ethanol wash can further reduce the agglomeration. The particle sizes of titania powders can be modified while still retaining the anatase structure.     

In-situ TEM Observation of Dislocation Emission, Multiplication and Motion Induced by Anodic Dissolution in Type 310 Stainless Steel

A special constant deflection device for TEM has been designed and then the dislocation configuration change ahead of a loaded crack tip after corrosion or anodic dissolution for some time but before the initiation of SCC can be observed in TEM. The results showed that anodic dissolution during SCC of a type 310 stainless steel in deionized water could promote dislocation emission,multiplication and motion before the initiation of SCC.     

被动锁模复合环形腔掺饵光纤激光器的自启动分析

本文对被动锁模复合环形腔掺饵光纤激光器的自启动工作特性进行了分析，指出谐振腔内残余反射面的存在是阻碍激光器实现自启动锁模的主要原因。利用半导体激光器有源区的折射率随注入电流的变化而改变的特性，在谐振腔中获得了一个可移动腔镜，克服了腔内残余反射面的影响，实现了锁模的自启动。     

颗粒状物料气力输送系统中输料管的连接方式

对颗粒状物料的气力输送 ,人们往往只重视所要采用的输送方式 ,而忽视了输料管连接方式的正确选择、施工与安装。输料管连接方式的正确与否 ,直接影响到输送量和物料的品质。详细介绍了常用的几种连接方式 ,分析了它们的优缺点 ,并提出了比较合理的连接方式     

中国爆破安全网

中国爆破安全网是由中国工程爆破协会主办的涉爆行业信息专业网 ,开通于 2 0 0 3年 4月。该网是民爆器材生产流通主管部门、使用部门和公安机关实施联网监控和规范化管理的有力工具 ,最主要的功能是为涉爆行业管理部门和从业单位提供一个功能完善的管理和办公平台。该网的开通 ,有利于民爆器材生产、销售、购买、使用流向监控制度的贯彻实行。文章介绍了网络的组成、建设原则 ,并给出了中国爆破安全网网络拓扑图