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991.
Chlorinated isotactic polypropylenes (CPP) having various chlorine contents were blended with poly(ethylene-co-vinyl acetate)s (EVA) having various vinyl acetate (VA) contents. The blends were made by casting films from dilute THF solutions and miscibility of the blends was identified by single glass transition temperature, which was confirmed by DSC and dynamic mechanical measurements. Based on the miscibility data from a large number of CPP/EVA combinations, a miscibility map was depicted where CO equivalent weight (CO-EQW) of EVA was plotted against chlorine equivalent weight (Cl-EQW) of CPP. Though an attractive interaction between CPP and EVA could be detected in all the miscible and immiscible blend pairs, miscibility of the CPP/EVA blends could solely be observed in a relatively narrow range of Cl-EQW ca. 65–100 and CO-EQW ca. 170–230. 相似文献
992.
Experimental investigations were performed to see how the die exit geometry and the extrusion velocity influence on extrudate
swell and melt fracture for several polymer melts [low-density polyethylene, styrene-butadiene rubber (SBR) and SBR/HAF (carbon
black) compound]. Four different types of die exit geometry were considered; 0° (symmetric. usual capillary die), and 30°,
45° and 60° (asymmetric dies) were chosen for the die exit angle. Extrudate diameters were measured without draw-down under
isothermal condition. Polymer melts were extruded into an oil that has the same density and temperature as those of the extrudate.
Extrudate swells from dies with different diameters were correlated with volumetric flow rates. It was observed that the extrudate
swell increases with increasing volumetric flow rate and exhibits through a minimum value at about 45° die exit angle. As
to the fracture phenomena, it was observed that the critical shear for the onset of melt fracture increases with the increasing
die exit angle up to 45°. However, for 60° die exit angle, the onset of melt fracture is again similar to that of 0° exit
angle. 相似文献
993.
This study was carried out to compare EPS (Extracellular Polymeric Substances) composition between conventional activated
sludge (AS) and activated sludge dosed with clinoptilolite (CAS). Additionally, those were compared with organic removal efficiency
in the effluent in conjunction with EPS concentrations. The experiments were conducted at SRT (Solids Retention Time) ranging
from 5 to 100 d. For the CAS, proteins were more readily observed for SRT 20 and 100 d compared to that of the AS. Polysaccharide
concentration in the sludge was greatly increased for the CAS, but it was significantly diminished when the SRT was extended.
The level of EPS concentration observed from the effluent had the same pattern of variation for the two different types of
systems. Regardless of type of reactor, the ratio of proteins for sludge versus effluent was independent of SRT, but the ratio
of polysaccharides diminished as SRT increased. In the long run, the degree of protein synthesis directly ascribed to concurrent
enhancement of SCOD removal efficiency was slightly more in the CAS. It was decided that clinoptilolite added system could
be more reliably retrofitted to a conventional activated sludge process. 相似文献
994.
Summary Anisotropic orientation of liquid crystalline epoxy(LCE) resin on carbon fiber(CF) surface was investigated and it was correlated
with curing behavior and thermomechanical properties of LCE. Anisotropic orientation of a LCE resin was spontaneously induced
on CF surface along a long molecular axis of CF during curing and the anisotropic orientation was maintained after curing.
Curing of LCE was accelerated by alignment of LCE on CF and anisotropic orientation of LCE enhanced dynamic modulus of CF
reinforced LCE composites. 相似文献
995.
Gel permeation chromatography and thin layer chromatography have been used respectively to separate and characterize the first seven members of an epoxy resin polymer homologous series on a preparative and analytical scale. The epoxy resin was formed by the reaction between Bisphenol-A and epichlorhydrin. NMR was used to identify the oligomers. The relationship between extinction coefficient and degree of polymerisation was also determined. 相似文献
996.
Bothexo- andendo-brevicomin reduced the response of flyingDendroctonus ponderosae (Coleoptera: Scolytidae) to an attractant composed oftrans-verbenol and terpenes or oftrans- andcis-verbenol and terpenes in a stand ofPinus contorta var.murrayana. These data suggest that racemicexo- andendo-brevicomin may interrupt aggregation in populations of mountain pine beetle colonizing lodgepole pine; functions of the natural chiral compounds are unknown.Research supported by NSF grants DEB 77-11367 and PCN 79-21708 and the O.S.U. School of Forestry. O.S.U. Agric. Exp. Sta. Tech. Paper No. 5713. 相似文献
997.
抗rHu-IFN-αMcAb亲和常数的测定 总被引:1,自引:0,他引:1
采用ELISA间接法检测抗原-抗体反应系统中游离抗体量的方法,对本实验室制备的5系抗rHu-IFN-αMcAb进行了亲和力测定,获得比较准确的McAb亲和常数。 相似文献
998.
We construct constitutive relations for friction stress, slide stress and collision stress of cohesionless granular flows. We propose that the friction stress and slide stress could be neglected when τc/τe < 0.02, where τc represents the interval time experienced by a given particle between two consecutive binary collisions and τe the particle relaxation time. We applied these constitutive relations to a simulation of solid-liquid flow in an inclined chute and found the simulation results agree with experimental data. 相似文献
999.
Kwang‐Pill Lee Anantha Iyengar Gopalan See‐Hee Lee Ali Md Showkat Young Chang Nho 《应用聚合物科学杂志》2006,102(4):3912-3918
Conducting polydiphenylamine was used to encapsulate silica nanoparticles through the oxidative polymerization of diphenylamine in the presence of ultrasonic irradiation. The polymerization was performed in the presence of sodium lauryl sulfate as a surfactant. Experiments performed in the absence of ultrasound clearly demonstrated that the application of ultrasonication played multiple roles in the preparation of a composite of polydiphenylamine with silica nanoparticles. Ultrasonication dispersed the silica nanoparticles, converted sodium lauryl sulfate to lauryl alcohol, and augmented the dispersion of the silica‐nanoparticle/polydiphenylamine composite in an organic medium. Silica‐nanoparticle/polydiphenylamine composites were also prepared in the absence of ultrasound and/or sodium lauryl sulfate. The silica‐nanoparticle/polydiphenylamine composites were characterized with Fourier trans form infrared spectroscopy, ultraviolet–visible/near‐infrared spectroscopy, and thermogravimetric analysis. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3912–3918, 2006 相似文献
1000.
A new graphical estimation technique is proposed for the determination of the kinetic parameters describing an autocatalytic reaction. A differential scanning calorimeter was used to monitor the reaction kinetics of an epoxy-based vinyl ester resin. The method utilizes information from a zero initial reaction rate, conversation at vitrification, the ratio of reaction rate constants under different isothermal conditions, and characteristics of the phenomenological kinetic model with assumptions being made about the overall reaction order. By fitting data to the integrated reaction rate equation with adjustments for the isothermal conditions, the kinetic parameters are estimated without using a linear or nonlinear regression method. Different kinetic parameters can be estimated from data before and after the gel point which was obtained from the relationship between the glass transition temperature and the degree of cure. 相似文献