Analysis of vitamin formulations by electrokinetic chromatography utilizing tetradecylammonium ions as the pseudostationary phase

A recently proposed method for the separation of fat-soluble vitamins by electrokinetic chromatography was further developed and investigated in the present study. The separation medium consisted of acetonitrile-water (80:20 v/v) and contained 80 mM tetradecylammonium bromide (TDA+); the content of acetonitrile served to maintain the hydrophobic vitamins dissolved during electrophoresis, while the TDA+ ions served as the pseudostationary phase. With the cathode placed at the outlet of the capillary, the fat-soluble vitamins were separated based on different hydrophobic interactions to the TDA+ ions and migrated in order of decreasing hydrophobicity prior to the electroosmotic flow. Migration time stability was significantly enhanced by the addition of 4 mM borate to the separation medium. The separation system was validated for the determination of vitamin E acetate in commercial tablets; quantitative results deviated by less than 3.5% from specified values, varying by less than 2.5% relative standard deviation (RSD) for within-day experiments, and by less than 6.5% RSD during between-day experiments. The separation system was compatible with injection solvents ranging in polarity from water to tetrahydrofuran, and was even capable of separating the water-soluble vitamins B1, B2, B12, and nicotinamide.     

10MeV中子引起的~（238）U，~（209）Bi，Fe和~9Be的次级中子

１０ＭｅＶ中子引起的￣（２３８）Ｕ，￣（２０９）Ｂｉ，Ｆｅ和￣９Ｂｅ的次级中子双微分截面测量祁步嘉，唐洪庆，周祖英，周陈维，沈冠仁，柯尊建，孙振强，夏海鸿（中国原子能科学研究院核物理所，北京２７５－４６信箱，１０２４１３）次级中子双微分截面是核工程设...     

温度,压力对漂移室气体增益的影响

研究了温度及气体压力对漂移室（工作于正比区）气体放大倍数的影响，温度和气体压力的变化范围分别是５￣４０℃及９０￣１０５ｋＰａ。用实验数据拟合得到了函数关系并测量了几种饱和度下函数中的参数值。     

Expression of beta 2-integrins and L-selectin on polymorphonuclear leukocytes in septic patients

Adhesion molecules on polymorphonuclear leukocytes (PMNL) play an important role in nonspecific defense mechanisms directed at invading microorganisms. When local infection, however, cannot be controlled, a systemic inflammatory response syndrome (SIRS) ensues which may progress to septic shock and multiple organ failure, these being major determinants of the patient's outcome. In the present study, the expression of beta 2-integrins and L-selectin on blood PMNL was measured on subsequent days in patients with sepsis (n = 17) and in healthy volunteers (n = 15). beta 2-Integrins and L-selectin molecules were detected by flow cytometry, using the monoclonal antibodies IB4 (anti-CD18) and Dreg200 (anti-CD62L), respectively. Adhesion molecules were determined at baseline immediately after blood collection and also 45 min after incubation of cells in vitro at body temperature to allow for spontaneous regulation. In addition, PMNL were activated by receptor-dependent and receptor-independent stimuli to characterize stimulus-specific adhesion molecule expression. In parallel with the measurement of adhesion molecules, severity of sepsis was assessed by the Elebute score. The results demonstrate significant differences in the basal, spontaneous and stimulus-induced expression of adhesion molecules between healthy volunteers, survivors (n = 11) and nonsurvivors (n = 6). Moreover, when survivors and nonsurvivors with severe sepsis (Elebute score > 12) were compared, basal expressions of both beta 2-integrins and L-selectin were significantly lower in patients who did not survive. Thus, measurement of adhesion molecules on circulating PMNL may be useful to identify septic patients at high risk for lethal outcome.     

地方时与区时在电离层研究中的差异

本文指出混淆地时与区时两个时间概念在电离层研究中带来的差异的严重性，建议使用地方与区时这两个名词，而抛弃“本地时”和“当地时”等容易引起混淆的名词。     

设计沟通中的噪音——从传播学角度看设计沟通中的困难

文章从传播学的角度探讨设计沟通过程中的困难。设计沟通是贯穿于整个设计管理活动的重要环节,是传达信息的主要途径,但在实践过程中却经常遇到困难,导致设计活动无法顺利进行。文章通过引入噪音的概念,分析设计沟通的困难产生的原因,并利用传播学的理论提出通过冗余调节噪音的想法,以解决设计沟通中的问题。     

Intranet搜索引擎设计与实现

随着企业内部网络应用的深入,Intranet内部的信息资源越来越庞大,怎样为这些数据信息构建索引是我们面If缶的主要任务,而全文检索的产生解决了这一问题。目前越来越多的中小企业采用Linux系统作为Web平台,并且利用检索系统来管理内部繁多的文本和HTML文件。文章对www搜索引擎的全文检索及其相关技术进行了分析和讨论,实现了一个基于Linux环境的Intranet搜索引擎LISE（Linux Intranet Search Engine）。LISE利用了基于词表的索引方法,为用户提供了更加准确的信息,能满足多种中小企业用户的需求。     

无线传感器网络（WSN）在花卉大棚环境监测中的应用研究

针对传统花卉大棚环境参数监测系统的某些缺点,本文对基于Zigbee技术的无线传感器网络在花卉大棚中的应用可行性进行分析和研究,并建立了花卉大棚无线环境监测系统,使得该监测系统的各节点位置、监测范围、节点扩展性、节点间距离都得以改善和提高。     

串联谐振耐压试验仪的设计与仿真

针对XLPE电力电缆耐压测试成本高、操作复杂等问题,本文中设计了一种变频串联谐振耐压试验装置。利用串联谐振电路的升压原理,构建了硬件电路,通过仿真对选择谐振点等问题进行了探讨。为了改进普通串联谐振耐压测试装置寻找谐振点慢、精度低的缺点,提出了一种解决方案。仿真结果表明,该方法能精确地确定谐振点。装置输出波形可靠性好,谐波分量少,具有良好的性能。