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Gang Wang Wan Jiang Guangzhao Bai Libin Wu 《Journal of the American Ceramic Society》2003,86(4):731-34
A type of aluminosilicate that has a good wetting property for molybdenum disilicide (MoSi2 ) was added to a MoSi2 matrix to study the effects on the microstructure and low-temperature oxidation. It was found that the composites had not only good low-temperature oxidation resistance but also high thermal shock resistance when the added oxides formed a network microstructure in the matrix. There was no appreciable oxidation gain for MoSi2 /oxide composites with a network microstructure at 773 K for 2500 h. The results indicate that microstructure design is a simple and effective solution to preventing the low-temperature oxidation of MoSi2 . 相似文献
144.
The poly(styrene‐co‐octavinyl‐polyhedral oligomeric silsesquioxane) (PS–POSS) organic–inorganic hybrid nanocomposites containing various percent of POSS were prepared via one‐step free radical polymerization and characterized by FTIR, high‐resolution 1H NMR, 29Si NMR, GPC, DSC, and TGA technologies. The POSS contents in these nanocomposites were determined using FTIR calibration curve. The result shows that the POSS contents in nanocomposites can be tailored by varying the POSS feed ratios. On the basis of the POSS contents in the nanocomposites and the 1H NMR spectra, the number of reacted vinyl groups of each octavinyl‐POSS macromonomer were calculated to be 6–8. DSC and TGA measurements indicate that the incorporation of POSS into PS homopolymer can apparently improve the thermal properties of the polymeric materials. The dramatic Tg and Tdec increases are mainly due to the formation of star and low cross‐linking structure of the nanocomposites, where POSS cores behave as the joint points and hinder the motion and degradation of the polymeric chains. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007 相似文献
145.
研究了新型含镁络合物的结构、性质及其用于制备高效乙烯聚合催化剂的制备规律。结果表明:将镁、有机醇以及不与镁发生“格式反应”的卤代烷相互作用可迅速发生反应形成新型含镁络合物溶液。该络合物在溶液中可析出结晶。具有特定的化学结构.可以均匀承载于多孔硅胶的孔隙中,负载TiCl4后制备出形态良好的球形高效乙烯集合催化剂。 相似文献
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The diffusion coefficient of a dye in fibres is critical to understanding the dyeing process and coloration quality of products. In this paper, the diffusion kinetics of solvent dyes in the thermosol dyeing of polyester fibres was studied by measuring K / S of the dyed polyester fabrics based on the Kubelka–Munk equation. The diffusion coefficients of two model solvent dyes were estimated with Hill's equation using the experimentally measured K / S values and were found to be in good agreement with those calculated from the traditional extraction method. Such a measurement method was applied to several other solvent dyes and pigments that have different molecular sizes and a good correlation between the measured diffusion coefficients and sizes of these dyes and pigments was found. The results indicate that it is feasible to use K / S measurement of dyed fabrics and Hill's equation to evaluate the kinetics of the thermosol dyeing process under certain conditions. 相似文献
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A recently proposed pipelined multithreading (PMT) technique exhibits wide applicability in parallelizing general sequential programs on multi-core processors. However, significant inter-core communication overhead limits PMT performance and prevents its commercial utilization. A simple and effective clustered pipelined multithreading (CPMT) approach is presented to accelerate sequential programs on commodity multi-core processors. This CPMT technique adopts a clustered communication mechanism that can yield very low average communication overhead by eliminating false sharing as well as reducing communication operation and transit delays in the software-only approach. A single-producer/single-consumer concurrent lock-free clusteredQueue algorithm based on a two-level queue structure is also proposed. The accuracy of CPMT is theoretically demonstrated. The performances of the algorithm and CPMT are evaluated on a commodity AMD Phenom four-core processor. The number of enqueue and dequeue times of the algorithm are 20.8 and 23 cycles given an appropriate parameter, respectively. The speedup of CPMT ranges from 13.1% to 119.8% for typical loops extracted from the SPEC CPU 2000 benchmark suite. 相似文献
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BHT结晶采用乙醇作为溶剂。对不同浓度的乙醇,改变溶质与溶剂的物料配比,测定了BHT溶液的出晶点温度。结果表明:在乙醇浓度一定的条件下,出晶点温度随BHT与乙醇配比的增大而降低;而在相同物料配比的条件下,乙醇浓度越低,出晶点温度越高。 相似文献