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301.
The microstructure and thermal behavior of the Sn-Zn-Ag solder were investigated for 8.73–9% Zn and 0–3.0% Ag. The scanning
electron microscopy (SEM) analysis shows the Ag-Zn compound when the solder contains 0.1% Ag. X-ray diffraction (XRD) analysis
results indicate that Ag5Zn8 and AgZn3 become prominent when the Ag content is 0.3% and above. Meanwhile, the Zn-rich phase is refined, and the Zn orientations
gradually diminish upon increase in Ag content. The morphology of the Ag-Zn compound varies from nodular to dendrite structure
when the Ag content increases. The growth of the Ag-Zn compounds is accompanied by the diminishing of the eutectic structure
of the Sn-9Zn solder. Differential scanning calorimetry (DSC) investigation reveals that the solidus temperature of these
solders exists at around 198°C. A single, sharp exothermic peak was found for the solders with Ag content less than 0.5%.
Liquidus temperatures were identified with the DSC analysis to vary from 206°C to 215°C when the Ag content ranges from 1.0%
to 3.0% 相似文献
302.
M. D. Joseph Sebastian B. Rudraswamy M. C. Radhakrishna Ramani 《Bulletin of Materials Science》2003,26(5):509-515
Cobalt ferrite (CoxFe3?xO4) is prepared in powder form by thermal decomposition of iron and cobalt salts and is analysed by X-ray diffraction and Mössbauer spectroscopic techniques. The variation of Mössbauer parameters, lattice parameters and crystallite size of the products formed with variation in the composition of Fe and Co ratios are studied. The studies confirm the formation of nano-size cobalt ferrite particles with defect structure and it is found to be maximum for the Fe : Co = 60 : 40 ratio of the initial precursor oxides. 相似文献
303.
Woo-Seok Cheong 《Journal of Electronic Materials》2003,32(4):249-253
For the lowest resistance, it is required to have the epitaxial silicon contact between the silicon plug and the substrate
and good step coverage at the high aspect-ratio contact holes, simultaneously. In this work, a double polysilicon (DPS) deposition
technique was proposed for the requirements. The first, thin silicon layer is deposited in a single-wafer process chamber
with an in-situ H2-RTP (rapid thermal process) treatment for the epitaxial contact, and the second silicon layer is formed in a batch-type furnace
for good step coverage. From chain resistance, Kelvin Rc, and current-voltage (I–V) measurement, the DPS process meets both low resistance and good uniformity, so that it suggests
a breakthrough in the small-sized, semiconductor device application. 相似文献
304.
305.
It is generally appreciated that the mechanical behavior of granular media depends fundamentally on the interaction of the
constituent particles, and that the validity of numerical models of granular media would be greatly improved with knowledge
of the grain-scale mechanics. However, most supporting experimental work has been conducted on highly idealized materials,
and a limited amount of information exists on grain-scale force–displacement relationships for naturally occurring materials.
To address this shortcoming, we are conducting a program that integrates laboratory experiments on grains of naturally occurring
aggregate with the discrete element modeling method, with the goal of relating the grain-scale physical and mechanical properties
of granular media to bulk behavior. The paper describes the equipment and methods that have been developed to conduct close-loop
controlled, grain-scale experiments under monotonic and cyclic loading conditions, and presents results from an initial set
of experiments on unbonded grains. The implications of the grain-scale results to the discrete element model are discussed.
Discussions center on the applicability of a physically based approach to the mechanics of granular media in general. In light
of future exploration missions and the resulting need to predict the mechanical properties of lunar and planetary regoliths,
the paper examines the potential usefulness of our physically based approach to the problem of predicting the behavior of
the types of materials found in those environments. 相似文献
306.
A series of polyesters was prepared to evaluate hydrolytic stability as a function of cyclohexyl dibasic acid content. The
three cyclohexyl dibasic acids: 1,2; 1,3; and 1,4 were formulated into polyesters with two glycols. The proportion of cis
and trans isomers was evaluated via 1H NMR. The hydrolytic stability of short chain polyesters was evaluated in an acetone/water mixture which solubilized the
polyesters to mimic oligoester behavior within a thermosetting polyester coating environment. The rate of hydrolysis was monitored
by acid titration and corroborated by GPC. Surprisingly, 1,2-cylohexyl diacid-based polyesters were robust, and 1,3-cyclohexyl
diacid-based polyesters were the most susceptible to hydrolysis. Evidently, a 1,2-anchimeric effect for cyclohexyl dibasic
acid polyesters was not an important consideration, while the 1,3-cyclohexyl ester interaction was. Consequently, an anomeric
effect was proposed.
Presented at the 81st Annual Meeting of the Federation of Societies for Coatings Technology, November 12–14, 2003, in Philadelphia,
PA. 相似文献
307.
Barbara K. Reck Robert B. Gordon 《JOM Journal of the Minerals, Metals and Materials Society》2008,60(7):55-59
Nickel and chromium are essential ingredients in alloys increasingly important for energy-efficient, environmentally friendly
modern technology. Quantitative assessment of the flows of these metals through the world economy from resource extraction
to final disposal informs resource policy, energy planning, environmental science, and waste management. This article summarizes
the worldwide technological cycles of nickel and chromium in 2000. Stainless steel is the major use of these metals, but they
serve numerous other special needs, as in superalloys for high-temperature service, as plating materials, and in coinage.
Because they are used primarily in alloys, novel recycling issues arise as their use becomes more widespread.
“... the great New York and St. Louis double track, nickel plated railroad...”
— Norwalk, Ohio, Chronicle 10 March 1881 announces arrival of surveyors for the future Nickel Plate Railway
“Later [1911] I formed an alloy of Iron and Chromium, which showed remarkable resistance to rust and tarnish ... [It was]
rediscovered by an Englishman named Brearley, in 1914.”
—Elwood Haynes to Stephen F. Roberts, 17 January 1925 相似文献
308.
Shafeeque G. Ansari Mushtaq Ahmad Dar Young-Soon Kim Hyung-Kee Seo Gil-Sung Kim Rizwan Wahab Zubaida A. Ansari Jae-Myung Seo Hyung-Shik Shin 《Korean Journal of Chemical Engineering》2008,25(3):593-598
A comparative study for the nucleation of diamond was carried out using surface treatment like (i) surface scratching with
1 μm diamond paste and (ii) surface etching using chlorine plasma at different RF powers (50, 100 and 150 W). Atomic force
microscopic study shows variation in roughness from 31 nm to 110 nm. Scratching results in random scratches, whereas plasma
etches a surface uniformly. Scanning electron microscopic observations show well faceted crystallites with a predominance
of angular shaped grains corresponding to 〈100〉 and 〈110〉 crystallite surfaces for the scratched as well as plasma etched
substrate. Surface etching at 150 W plasma power results in a better growth in comparison with 50 and 100 W plasma powers.
Chlorine-radical is found responsible for the changes in the growth morphology. Raman spectroscopy shows a sharp peak at 1,332
cm−1 and a peak at ∼1,580 cm−1 for both samples. 相似文献
309.
310.
Mold-slag friction and fracture may cause heat-transfer variations in continuous casting, which leads to steel shell temperature
and stress variations, resulting in surface cracks. Analytical transient models of liquid slag flow and solid slag stress
have been coupled with a finite-difference model of heat transfer in the mold, gap, and steel shell to predict transient shear
stress, friction, slip, and fracture of the slag layers. The models are validated by comparing with numerical models and plant
measurements of mold friction. Using reported slag-fracture strength and time-temperature-transformation (TTT) diagrams, the
models are applied to study the effect of casting speed and mold-powder viscosity properties on slag-layer behavior between
the oscillating mold wall and the solidifying steel shell. The study finds that liquid-slag lubrication would produce negligible
stresses. A lower mold-slag consumption rate leads to high solid friction and results in solid-slag-layer fracture and movement
below a critical value. Crystalline slag tends to fracture near the meniscus and glassy slag tends to fracture near the mold
exit. A medium casting speed may be the safest to avoid slag fracture, due to its having the lowest critical lubrication consumption
rate. The high measured friction force in operating casters could be due to three sources: an intermittent moving solid slag
layer, excessive mold taper, or mold misalignment.
Other symbols are defined in Table I 相似文献