Synthesis of multiwalled carbon nanotubes supported on M/MCM-41 (M = Ni,Co and Fe) mesoporous catalyst by chemical vapour deposition method

Aim of this research is to develop an effective way in producing multi-walled carbon nanotubes (MWNTs) via chemical vapour deposition method using acetylene as carbon source and synthesized mesoporous M/MCM-41 (M?=?Ni, Co and Fe) as catalyst. The mesoporous MCM41 is synthesized by using sodium metasilicate as silica source of frameworks and cetyltrimethylammonium bromide as template. The effect of temperatures and growth times are investigated to produce MWNTs with high yield and high quality. The low-angle X-ray diffraction (XRD), Fourier transform infrared spectroscopy and scanning electron microscopy results verified the formation of MCM41. Meanwhile, high-angle XRD, Raman spectra and transmission electron microscopy results confirmed the synthesized carbon nanotubes at 600?°C and growth time for 30 min are multi-walled. The yield obtained is 1353 mg in 30 min. It shows that the MCM-41 has a promising potential to produce MWNTs at low cost and shorter duration.     

Effect of multi-ions doping on the properties of carbonated hydroxyapatite bioceramic

The effect of multi-ions (Mg²⁺, SiO₄^4-, Zn²⁺, Cu²⁺) doping on the properties of carbonated hydroxyapatite (CHA) prepared by a wet chemical method has been investigated. Different combinations of ions were doped into the CHA and the as-synthesized compacts were sintered at 900?°C prior to body characterization. It was found that regardless of ions doping, the lattice structure of the CHA was not disrupted. In addition, secondary phases were not detected for all the multi-ions doped samples. The XRD and FTIR results further confirmed the presences of a B-Type CHA in the sintered samples. The XRD analysis revealed that the lattice parameters (c/a ratio) increased with dopant addition and resulted in a smaller crystallite size. The FESEM examination also showed the presences of smaller grain size for the multi-ions doped CHA samples thus indicating that the doping was beneficial in suppressing grain coarsening in carbonated hydroxyapatite.     

The design and development of suspended handles for reducing hand-arm vibration in petrol driven grass trimmer

The portable petrol driven grass trimmer is identified as a type of machine whose operator can be subjected to large magnitude of hand-arm vibration. These vibrations can cause complex vascular, neurological and musculoskeletal disorder, collectively named as hand-arm vibration syndrome. The vibration total level on the handle of grass trimmer of 11.30 m/s² was measured, and it has reached the exposure limit value of 5.0 m/s² for daily vibration exposure A(8). New suspended handles were designed to reduce the vibration level. Three different prototype handles with rubber mounts were designed. Handles were made of different materials, and the distance of rubber mounts were varied. From the study, it was observed that not all the handles with rubber mounts were effective in reducing hand-arm vibration. The reduction of vibration depended on the handle material and distance installed between rubber mount and vibration transmissibility of handle-isolation system. Subjective ratings of perception of vibration were measured, and the results indicated that operators were not fully aware of the level of vibration. A prototype handle that is made of heavier material results in the lowest hand-arm vibration of 2.69 m/s². The new handle has significantly reduced the vibration total value by 76% compare with the existing commercial handle.

Relevance to industry

Large numbers of workers are employed to perform grass trimming job in many developing countries. This paper presents the effect of handle types (commercial and prototype) on the commonly used grass trimmer.     

A new denoising method for removing salt & pepper noise from image

Multimedia Tools and Applications - Digital image has a significant importance in many fields in human life such as, in medicine, photography, biology, astronomy, industry and defense. Thus, it...     

Optimum mechanical behavior of calcium phosphate cement/hydroxyl group functionalized multi-walled carbon nanotubes/bovine serum albumin composite using metaheuristic algorithms

Injectable calcium phosphate cements have been introduced as adjuncts to internal fixation for treating selected fractures. These cements harden without producing much heat, develop compressive strength, and are remodeled slowly in vivo. The main purpose of the cement is to fill voids in metaphyseal bone, thereby reducing the need for bone graft. However, such cements may also improve the holding strength around metal devices in osteoporotic bone. This paper presents the optimum mechanical behavior of calcium phosphate cement/hydroxyl group functionalized multi-walled carbon nanotubes/bovine serum albumin (CPC/MWCNT-OH/BSA) composites in terms of compressive strength using well-known metaheuristic optimizers. The process parameters studied were wt% of MWCNT-OH (0.2–0.5 wt%) and wt% of BSA (5–15 wt%). The obtained results from metaheuristic algorithms were compared with the results from the response surface methodology (RSM) in the literature. The results obtained from metaheuristic algorithms outperformed the results given by the RSM in terms of less error percentage and high compressive strength.     

Enhanced backstepping sliding mode controller for motion tracking of a nonlinear 2-DOF piezo-actuated micromanipulation system

Microsystem Technologies - In this paper a robust backstepping sliding mode controller is developed for tracking control of 2-DOF piezo-actuated micromanipulation system. The control approach is...     

Single-Row Transformation of Complete Graphs

A complete graph is a fully-connected graph where every node is adjacent to all other nodes in the graph. Very often, many applications in science and engineering are reducible to this type of graph. Hence, a simplified form of a complete graph contributes in providing the solutions to these problems. In this paper, we present a technique for transforming a complete graph into a single-row routing problem. Single-row routing is a classical technique in the VLSI design that is known to be NP-complete. We solved this problem earlier using a method called ESSR, and, the same technique is applied to the present work to transform a complete graph into its single-row routing representation. A parallel computing model is proposed which contributes in making the problem modular and scalable. We also discuss the application of this work on the channel assignment problem in the wireless cellular telephone networks.     

Siamese convolutional neural network and fusion of the best overlapping blocks for kinship verification

Multimedia Tools and Applications - Analysis of facial images decoding familial features has been attracting the attention of researchers to develop a computerized system interested in determining...     

A Robust Peak-to-Average Power Ratio Reduction Scheme by Inserting Dummy Signals with Enhanced Partial Transmit Sequence in OFDM Systems

Peak-to-average power ratio (PAPR) is one of the main drawbacks in orthogonal frequency division multiplexing (OFDM) systems. High PAPR forces the power amplifier to back off in order to operate in its linear region, which degrades the power efficiency of the system. Several PAPR reduction techniques have been developed, but most of them have not considered both complexity and PAPR reduction. In this paper, a novel PAPR reduction scheme based on the insertion of dummy sequences to an enhanced partial transmit sequence is proposed. By applying this scheme the PAPR performance is enhanced compared to the conventional methods while the complexity is significantly reduced. Numerical analysis is carried out with OFDM signal and QPSK modulation.     

Tribological Properties of Electroless Nanocomposite Deposits with Influence of Aliquat 336 on 6061 Aluminium Alloy

The process of electroless nanocomposite deposit on 6061 aluminium alloy was significantly enhanced with influence of Aliquat 336. The present investigation dealt with the analysis for the influence of Aliquat 336 surfactant on tribological properties of ENi–P–ZnO nanocomposite deposit on 6061 aluminium alloy sample. Wear resistance was calculated by pin-on-disc tribometer wear testing machine for the coated substrate by varying the surfactant concentration. Addition of surfactant has shown significant enhancement in the wear resistance of the coated surface. Surfactant was distinctively added in the chemical bath which resulted in decline of the surface tension, helped to bind the particles of nickel to the bubbles of hydrogen gas produced throughout the process of deposition. However, the impact of surfactant reached to its maximum value (critical micelle concentration) and got stabilized. The surface morphology and phosphorus content were characterized by field emission of scanning electron microscopy and energy dispersive X-ray analysis respectively. The worn surface morphology also revealed the abrasive wear mechanism. The complete experimental details, results obtained and their analyses have been presented in this paper.