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11.
Elif Kacar Ahmet Erdem Mesure Mutlu Sanli Asgar Kayan Levent Candan Ufuk Yildiz Arif Demir 《Journal of Inorganic and Organometallic Polymers and Materials》2016,26(4):895-906
It is important to give water-repellent and antibacterial properties to the acrylonitrile butadiene styrene (ABS) surfaces of the hearing aids. In this study, the sol–gel Si and sol–gel Ti solutions were prepared from the reactions of silicon ethoxide, titanium butoxide and methacrylic acid. The catalyst and Dynasylan F8815 were added to the sol–gel solutions to give hydrophobic properties onto the ABS surfaces. Additionally, silver nanoparticles were synthesized by nanosecond laser and added to the coating solutions to give extra antibacterial properties. The surfaces of the ABS targets were coated using the sol–gel dip coating and pulsed laser deposition techniques. The coatings with good adhesion between film and substrate and good water-repellent properties were achieved. The average contact angles for the coated ABS surfaces were measured in the range between 120 and 125 degrees. The obtained sol–gel materials and produced thin films onto the ABS surfaces were also analyzed in terms of the antibacterial properties. The highly antibacterial properties were observed in the sol–gel solutions and the thin films. 相似文献
12.
João Luiz Pozzobon Taiane Missau Carolina Ceolin Druck Mutlu Özcan 《Journal of Adhesion Science and Technology》2016,30(4):412-421
This study evaluated the effect of air-abrasion parameters such as particle size, distance, and time on adhesion of resin cement to zirconium dioxide (Y-TZP) and t→m phase transformation. Y-TZP blocks (N = 80) (In-Ceram YZ, Vita) (4 mm3?×?4 mm3?×?3 mm3) were assigned into eight groups (n = 10): air-abrasion with 30 μm (CoJet Sand, S30) and 110 μm (Rocatec-Plus, S110) silica-coated alumina particles, applied for either for 10–20 s (T = time), from a distance of 10–20 mm (D = distance), composing the following groups: S30T10D10, S30T10D20, S30T20D10, S30T20D20, S110T10D10, S110T10D20, S110T20D10, and S110T20D20. Resin composite (RelyX ARC) was bonded to Y-TZP blocks in polyethylene molds. The specimens were aged (10,000 thermal cycles and water storage for 90 days) prior to shear bond test. Failure types were analyzed under stereomicroscope and SEM, and phase transformation was calculated. Data (MPa) were analyzed using 3-way ANOVA and Tukey’s tests. Air-abrasion with 110 μm silica particles (10.96) presented significantly higher bond strength (p = 0.0149) compared to 30 μm (8.96). Time (p = 0.403) and distance (p = 0.179) parameters did not affect the results significantly. Air-abrasion with 110 μm particles (12.3) promoted higher bond strength than that of 30 μm (6.4) when applied for 10 s from a distance of 10 mm (Tukey’s). Failure types were predominantly adhesive. Phase transformation ranged between 30.3 and 35.9% for 30 μm particles and 23.8–43.7% for 110 μm particles. While the size of silica-coated alumina particles were more relevant parameter for resin cement adhesion to Y-TZP, time (up to 20 s) and distance (up to 20 mm) appear to be less pertinent. 相似文献
13.
Genoveva Buelna Mutlu Ulutagay-Kartin Tina M. Nenoff 《Chemical Engineering Communications》2006,193(5):606-619
Alkylation reactions of benzene with propylene using heterogeneous catalysts H+-β zeolite, MCM-22, and ZSM-5 were studied for their affinity for cumene production. This work focused on the gas-phase reaction using different crystalline catalysts at several temperatures and amounts of reactants using both batch and continuous fixed-bed reactors. The properties of baseline commercial H+-β catalysts versus versions modified with Ga, La, and Pt were studied. Quantitative analysis of product mixture was performed by gas chromatography. For the batch reactor, β-zeolite produced the highest cumene yield and selectivity of 72% and 92%, respectively, at 225°C. At this temperature, a benzene:propylene dilution of 7:1 molar ratio was the optimum. For the continuous system, cumene production is favored at lower space velocities, higher benzene-to-propylene ratio, and temperatures close to 225°C. Ga modification of the H+-β zeolite significantly enhanced cumene yield in the continuous fixed-bed reactor at 225°C, from 27% of the unmodified β-zeolite to 36% for the Ga-modified one. The life span of modified β-catalysts was studied in the fixed-bed reactor for the first eight hours of reaction. 相似文献
14.
Hynek Biederman Ismail H. Boyaci Petra Bilkova Danka Slavinska Selma Mutlu Josef Zemek Miroslava Trchova Josef Klimovic Mehmet Mutlu 《应用聚合物科学杂志》2001,81(6):1341-1352
Cellulose acetate membranes (CA) were modified by means of plasma polymerization of ethylene diamine (EDA) and n‐butylamine (n‐BA). The motivation for this work was the application of a modified membrane for the single‐layer enzyme electrode. A tubular reactor with the external radiofrequency (13.56 MHz) excitation was used. Surface modification was performed at 5, 10, and 15 W power (at 27 Pa working pressure) for 5, 10, 15 min. Modified surfaces were characterized in detail by FTIR–ATR, XPS (ESCA), contact angle, and enzyme immobilization activity. The best treatment results were obtained for EDA with 5 W and 30 min and 15 W and 10 min. These results are discussed using surface analysis data. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 81: 1341–1352, 2001 相似文献
15.
The aim of the present study was to formulate suspension type inhalation aerosols by various types of auxiliary materials, and to select the formulation with the highest proportion of the effective particle size. The examined suspension type aerosol contained sodium cromoglycate as an active compound. For the stabilization of the suspension, the applied surface active ingredients were oleic acid and oleyl oleate, and dimethyl siloxane polymer was selected as hydrophobizing agent. Factorial design was used for the optimization of the experimental results. On the basis of our results, the correct types and amounts of auxiliary materials can be selected to obtain the therapeutically effective formulation. 相似文献
16.
Smart structures and their applications on active vibration control: Studies in the Department of Aerospace Engineering, METU 总被引:1,自引:0,他引:1
Melin Sahin Fatih Mutlu Karadal Yavuz Yaman Omer Faruk Kircali Volkan Nalbantoglu Fatma Demet Ulker Tarkan Caliskan 《Journal of Electroceramics》2008,20(3-4):167-174
This work presents the theoretical and experimental studies conducted in Aerospace Engineering Department of Middle East Technical
University on smart structures with particular attention given to the structural modelling characteristics and active suppression
of in-vacuo vibrations. The smart structures considered in these analyses are finite and flat aluminium cantilever beam-like
(called as smart beam) and plate-like (called as smart fin) structures with surface bonded lead–zirconate–titanate patches.
Finite element models of smart beam and smart fin are obtained. Then the experimental studies regarding open loop behaviour
of the structures are performed by using strain gauges and laser displacement sensor to determine the system models. Further
studies are carried out to obtain H
∞ and μ-synthesis controllers which are intended to be used in the suppression of free and forced vibrations of the smart structures.
It is observed that satisfactory attenuation levels are achieved and robust performance of the systems in the presence of
uncertainties is ensured. In that respect a comparative study involving H
∞ and sliding mode controls is also conducted. Recently, the studies involving aerodynamic loading are also gathering pace. 相似文献
17.
Ilven Mutlu Sinasi Ekinci Enver Oktay 《Journal of Materials Engineering and Performance》2014,23(6):2083-2091
This study presents nondestructive characterization of microstructure and mechanical properties of heat treated Ti, Ti-Cu, and Ti-6Al-4V titanium-based alloys and 17-4 PH stainless steel alloy for biomedical implant applications. Ti, Ti-Cu, and 17-4 PH stainless steel based implants were produced by powder metallurgy. Ti-6Al-4V alloy was investigated as bulk wrought specimens. Effects of sintering temperature, aging, and grain size on mechanical properties were investigated by nondestructive and destructive tests comparatively. Ultrasonic velocity in specimens was measured by using pulse-echo and transmission methods. Electrical conductivity of specimens was determined by eddy current tests. Determination of Young’s modulus and strength is important in biomedical implants. Young’s modulus of specimens was calculated by using ultrasonic velocities. Calculated Young’s modulus values were compared and correlated with experimental values. 相似文献
18.
Critical assessment of extracellular polymeric substances extraction methods from mixed culture biomass 总被引:3,自引:0,他引:3
Extracellular polymeric substances (EPS) have a presumed determinant role in the structure, architecture, strength, filterability, and settling behaviour of microbial solids in biological wastewater treatment processes. Consequently, numerous EPS extraction protocols have recently been published that aim to optimize the trade off between high EPS recovery and low cell lysis. Despite extensive efforts, the obtained results are often contradictory, even when analysing similar biomass samples and using similar experimental conditions, which greatly complicates the selection of an extraction protocol. This study presents a rigorous and critical assessment of existing physical and chemical EPS extraction methods applied to mixed-culture biomass samples (nitrifying, nitritation-anammox, and activated sludge biomass). A novel fluorescence-based method was developed and calibrated to quantify the lysis potential of different EPS extraction protocols. We concluded that commonly used methods to assess cell lysis (DNA concentrations or G6PDH activities in EPS extracts) do not correlate with cell viability. Furthermore, we discovered that the presence of certain chemicals in EPS extracts results in severe underestimation of protein and carbohydrate concentrations by using standard analytical methods. Keeping both maximum EPS extraction yields and minimal biomass lysis as criteria, it was identified a sonication-based extraction method as the best to determine and compare tightly-bound EPS fractions in different biomass samples. Protein was consistently the main EPS component in all analysed samples. However, EPS from nitrifying enrichments was richer in DNA, the activated sludge EPS had a higher content in humic acids and carbohydrates, and the nitritation-anammox EPS, while similar in composition to the nitrifier EPS, had a lower fraction of hydrophobic biopolymers. In general, the easily-extractable EPS fraction was more abundant in carbohydrates and humic substances, while DNA could only be found in tightly bound EPS fractions. In conclusion, the methodology presented herein supports the rational selection of analytical tools and EPS extraction protocols in further EPS characterization studies. 相似文献
19.
Abdullah Goktas Ferhat Aslan ?brahim Halil Mutlu 《Journal of Materials Science: Materials in Electronics》2012,23(2):605-611
The effect of annealing temperature on selected characteristics of polycrystalline La0.67Sr0.33MnO3 films, which have been produced on quartz substrates, was investigated. X-Ray powder diffraction patterns showed that the
phase formation started at 873 K and all the films had perovskite structure. By increasing the annealing temperature, the
lattice parameters were decreased. Scanning electron microscope indicated that the film thicknesses were approximately 3 μm
and the average grain size of the samples varied between 30–100, 50–110, 70–120, and 100–150 nm for films annealed at 873,
973, 1,073, and 1,173 K, respectively. All the films showed a paramagnetic–ferromagnetic (TC) and metal–insulator (TIM) phase transition. The TC indicated a small variation [from 131 K (S4) to 124 K (S1)] as a function of annealing temperature, whereas the TIM went down from 212 K (S4) to 110 K (S1), a strong decrease of 102 K. A colossal magneto resistance with magneto resistance
ratios of 130, 139, 156, and 163% were observed near TC and at 6 T magnetic field. 相似文献
20.
Engin Baysoy Dursun Korel Yildirim Cagla Ozsoy Senol Mutlu Ozgur Kocaturk 《Magma (New York, N.Y.)》2017,30(1):93-101