UV法测定聚甲基丙烯酸酯纳米粒中胰岛素的包封率

建立一种简便易行的测定聚甲基丙烯酸酯胰岛素纳米粒中游离胰岛素含量方法.用Nanosep OD100C33超滤膜分离纳米粒和游离药物,在276 nm处测定药物的吸光度,建立胰岛素含量测定方法,并对线性、回收率、精密度等指标进行考察,最后测定各种胰岛素和载体比例混合的纳米粒的包封率.结果发现,该超滤膜能较好地分离纳米粒和游离的药物,在0.11～1.10 u/mL范围内,药物在276 nm的吸光度和浓度存在良好的线性关系(r=0.999 8),线性方程为A=0.868 8C-0.001 6,高、中、低3种浓度的回收率和精密度良好.该方法操作简单、结果可靠,可用于胰岛素纳米粒中药物包封率的测定.     

ZnSe棱镜折叠波导CO_2激光器的研究

研制了使用ZnSe棱镜折叠的波导CO_2激光器,提出一种CO_2激光—He-Ne激光调整光路的方法,并获得了该种折叠激光器的振荡。进一步的改进可以提高其输出功率而得到实用性的器件。     

Experimentally Verified Mn–Zn Ferrites' Intrinsic Complex Permittivity and Permeability Tracing Technique Using Two Ferrite Capacitors

After setting up a mathematical model for rectangular-shaped Mn-Zn ferrite capacitors, this paper investigates dimensional effects on the intrinsic complex permittivity and the measured apparent complex permittivity of Mn-Zn ferrite blocks. The simple block structure of the samples guarantees their easy and precise preparation. Above a few hundred kilohertz, dimensional effects make the measured apparent complex permittivity deviate from its intrinsic value. This paper uses a Newton-Raphson based method to trace the intrinsic complex permittivity and permeability from the measured impedances of two rectangular-shaped Mn-Zn ferrite capacitors in the frequency range from a few hundred kilohertz to 40 MHz. From the traced intrinsic complex permittivity and permeability, the apparent complex permittivity of a third sample with different dimensions is then calculated theoretically. The papers also presents results of experiments carried out to measure the apparent complex permittivity of the third sample; agreement between the measured and the calculated values is very good. This justifies the validity of the method presented in this paper, when used to determine the dimension-independent intrinsic complex permittivity and permeability of Mn-Zn ferrites     

浅谈做好螺丝湾水电站施工质量,工期,投资控制的几项措施

螺丝湾水电站作为云南省电力局（ 集团公司） 、迪庆州、省投资公司三方合资建设的电站，是迪庆藏族自治州自建国以来投资最大的一个建设项目，它的建成，开创了滇西北水电资源多方合资开发的先例，有其特殊的经济和政治意义。本文结合螺丝湾水电站建设的实际情况，论述了在市场经济条件下做好螺丝湾电站建设中“三控制”的几项措施     

利用5A284型铣齿机加工转盘螺旋锥齿轮探讨

利用引进设备5A284苏联铣齿机加工石油钻机转盘螺旋锥齿轮，建立计算程序并进行调整计算，详述了遇到的问题及解决方法，使所加工的锥齿轮质量良好。     

富氧氮氧化硅薄膜退火的研究

利用红外吸收(IR)谱和X射线光电子谱(XPS)对富氧氮氧化硅(oxygen-rich SiOxNy)及其在600、750和900℃下退火后样品的微结构进行了研究.实验中除观察到N、H的释放外,首次发现退火会导致SiOxNy中O的释放,同时还发现退火温度不同,H、O、N元素的释放量以及微结构的变化都不相同,根据这些现象,提出了5个化学反应过程并予以解释.     

钢铁表面黑色转化膜处理技术

黑色转化膜技术是目前较为先进的钢铁表面处理技术 ,本文试验研究了一种新工艺 ,提出了TB值的概念 ,通过控制TB值即可控制处理液的质量 ,获得性能优良的转化膜。此工艺性能可靠 ,可操作性强 ,并可应用于激光热处理前的预处理。     

脉冲功率器件直流和动态热特性探测

介绍了针对影响微波脉冲功率器件可靠性的热性能问题，应用红外热分析技术。对比探测微波脉冲功率器件在动态和直流状态下的温度分布，峰值结温，热阻及其变化规律。     

液氮温区同轴脉冲管制冷机的实验研究

脉冲管制冷机冷头朝上布置可以使制冷机与超导器件的耦合更方便 ,但对G -M型脉冲管制冷机 ,重力会对这种布置方式产生不利影响。对双向进气型脉冲管制冷机 ,直流和耦合传热会共同影响脉冲管制冷机的性能。介绍了液氮温区G -M型同轴脉冲管制冷机的实验结果 ,主要研究了蓄冷器温度分布和重力对脉冲管制冷机性能的影响     

Direct electroless Ni-P deposition on AM50 magnesium alloy from sulfate bath

A bright electroless Ni-P deposition on AM50 magnesium alloy in a sulfate plating bath was proposed by using direct plating process with non-chromate pretreatment. The electroless Ni-P plating on AM50 magnesium alloy has an admirable appearance and good adhesion. The results indicate that the electroless Ni-P deposition with non-chromate pretreatment has better adhesion than that of zinc immersion coating. Anodic polarization curves indicate that the electroless Ni-P deposition obtained from the sulfate bath has similar corrosion-resistance to that obtained from basic nickel carbonate bath. The deposition process generates less pollutant by a non-chromate plating bath and is suitable for the magnesium alloys manufacture because of its low cost. The hardness of the electroless Ni-P plated AM50 is about HV 720.6 and HV 969.7 after heat treatments at 180℃ for 2 h. The wear resistance of Ni-P plated magnesium alloy specimens is about 5 to 9 times as high as that of bare magnesium alloys.