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991.
992.
S. V. Prikhodko Y. Ma A. J. Ardell D. G. Isaak J. D. Carnes S. Moser 《Metallurgical and Materials Transactions A》2003,34(9):1863-1868
The adiabatic elastic stiffness constants C
ij of Ni-Si single-crystal solid-solution alloys of two slightly different compositions, 10.78 and 11.17 at. pct Si, were measured
over the temperature range from 20 °C to 900 °C using the rectangular parallelepiped resonance method. The isotropic elastic
constants of the polycrystalline ordered intermetallic compound Ni3Si containing 23 at. pct Si were also measured over this temperature range. Values of the C
ij for Ni3Si were estimated from the data on the polycrystalline alloy, as well as from published data in the literature on isomorphous
ternary ordered intermetallic compounds containing different amounts of Si. Using measured values and previously published
data, the stiffness constants of Ni3Ti were estimated; these are the only available data on this alloy. The estimated single-crystal elastic constants of Ni3Si, as well as the experimentally measured bulk modulus, are considerably smaller than published values calculated from first-principles
methods. The same is true for the C
ij of Ni3Ti, but the discrepancies are smaller. 相似文献
993.
Cold-rolling texture and partially recrystallized texture of polycrystalline 3 pct Si-Fe were investigated using high-resolution
electron backscattered diffraction (EBSD) method. From the measurement on a deformed grain with {211}〈011〉∼{111}〈011〉 orientations,
deformation bands with {12 4 1}〈014〉 orientation were found. It turned out that the orientation rotation relationship between
deformation bands and surrounding deformed grain can be explained by the activation of the slip system, which has a common
slip plane with an adjacent grain. Oriented nucleation of recrystallized grains with {12 4 1}〈014〉 orientation was observed
in a deformed grain with {211}〈011〉∼{111}〈011〉 orientation. Exactly the same orientation relationship that was observed between
deformed grain and the deformation bands was also observed between the deformed grain and the recrystallized grain. A hypothesis
that recrystallization nuclei are generated directly from the deformation bands formed by an activation of the slip system
that has a common slip plane of neighboring deformed grains was proposed from the present experimental results. 相似文献
994.
G. C. Coelho J. A. Golczewski H. F. Fischmeister 《Metallurgical and Materials Transactions A》2003,34(9):1749-1758
Thermodynamical equilibria have been calculated for a wide variety of high-speed steel compositions belonging to the multicomponent
system Fe-C-W-Mo-V-Cr-Nb as well as for two series of white-cast-iron alloys containing niobium. Some temperature-concentration
diagrams for both classes of alloys are presented and calculated quantities (melting and transformation temperatures, amounts
and compositions of phases) are compared with experimental data. Good agreement between calculated and experimental information
has been obtained, with the exception of the MC phase compositions and transformation temperatures for white-cast-iron alloys
with high carbon and chromium contents. These differences can, however, be satisfactorily explained by plausible kinetic effects. 相似文献
995.
Thin-film nickel coatings on fiber materials 总被引:1,自引:0,他引:1
L. M. Lyn’kov V. A. Bogush E. A. Senkovets S. M. Zavadskii 《Technical Physics Letters》2003,29(8):641-642
Vacuum deposition of thin films onto fiber materials is a promising method of obtaining electromagnetic screens. We have studied the structure and the electromagnetic properties of machine-knitted fabric coated with nickel by means of magnetron sputtering. When the fabric is irradiated from the metal-coated side, the reflection coefficient is higher by a factor of 1.4 as compared to the case when the same source of electromagnetic radiation is situated on the opposite side (facing the uncoated surface), while the absorption coefficient in both cases is the same. 相似文献
996.
997.
Titanium oxides were reduced to metallic titanium using the liquid calcium floating on the molten CaCl2. A part of Ca dissolved into CaCl2 and reacted with TiO2 settled below CaCl2. The by-product CaO also dissolved by about 20 mol pct into CaCl2, which was effective in reducing the oxygen concentration in the obtained Ti particles. The compositional region in the Ca-CaCl2-CaO system was examined for the less oxygen contamination in Ti and the better handling in leaching. A large amount of the
residual calcium oxidized the titanium powder in leaching. The metallic Ti powder less than 1000 mass ppm oxygen could be
obtained only for 3.6 ks using 5 to 7 mol pct Ca-CaCl2 at 1173 K. The powder was slightly sintered like sponge, and contained approximately 1500 ppm Ca. The anatase phae, the intermediate
product in the refining process of TiO2, could be also supplied as raw material as well as rutile. 相似文献
998.
The corrosion behaviour of nitrogen-containing austenitic stainless steel in methanol containing different concentrations
of H2SO4, HCl, LiCl and H2SO4 + HCl has been investigated using a potentiostatic polarization method. The cathodic reaction in the H2SO4, HCl and H2SO4 + HCl solutions was proton reduction whereas in the neutral LiCl solution, oxygen reduction was the predominant cathodic
reaction. Active, passive and transpassive behaviours were observed only for higher concentrations of H2SO4 (0.01–2.0 M) due to the inherent water content. A cathodic loop, characterized by measured negative current in the anodic
region, was also observed in solutions, in which the concentration of H2SO4 was 1.0 M or higher. The relative stability of the passive films decreased as the H2SO4 concentration increased, and thus the steel suffered from mild pitting corrosion. In the chloride environment, the rate of
corrosion increased as the Cl− ion concentration increased. The presence of acid along with Cl− ions enhanced corrosion, and the corrosion rate increased significantly. The steel suffered from mild intergranular corrosion
in acidic chloride solutions of methanol. In the H2SO4 + HCl solutions, passive films were only formed when the H2SO4 to HCl concentration ratio was greater than ∼10:1. 相似文献
999.
The effect of a gas dissolved in a liquid on the variation of the refractive index of the compressed mixture was studied.
The compression process was monitored with the aid of a holographic interferometer. The sensitivity of this method allows
the compressibility of water and the solubility of helium and nitrogen to be studied at pressures below 4 atm. A procedure
for obtaining qualitative and quantitative data on the solubility of gases in liquids is proposed. 相似文献
1000.
V. A. Kagadei E. V. Nefyodtsev D. I. Proskurovsky S. V. Romanenko 《Technical Physics Letters》2003,29(11):897-900
Using one-or two-layer films of transition metals, it is possible to determine the atomic hydrogen flux density under reduced
gas pressure conditions (10−1–10−3 Pa). The method consists in monitoring a change in the film resistance caused by selective dissolution of atomic hydrogen
in the metal during exposure of the film in a mixed atomic-molecular flow, followed by determining a characteristic time τ
required for the hydrogen concentration in the film to reach 63% of the maximum possible level. The hydrogen flux density
is then calculated within the framework of a simple mathematical model of the film saturation with hydrogen described by a
relaxation law. The proposed method is characterized by a high selective sensitivity to atomic hydrogen. The atomic hydrogen
flux density in a mixed atomic-molecular flow can be determined in a range from 5×1013 to 1016 cm−2 s−1. 相似文献