电镀废水中微量铜的快速测定

利用铜腙光度测定电镀废水中的微量铜，优选出最佳测量波长，研究了酸度，柠檬酸浓度，显色剂浓度，温度及干扰元素对测量的影响，铜含量在0-25μg/25mL范围内遵守比尔定律，该方法简便，快捷，具有良好的选择性。     

Preparation and characterization of a series of polyamides with long alkylene segments: Nylons 12 20, 10 20,s 20,6 20, 4 20 and 2 20

Summary A series of nylons with long alkylene segments between amide groups were newly prepared by step-heating melt-polycondensation of 1,lS-octadecanedicarboxylic acid with various diamines. The prepared polyamides were characterized carefully. The results show that many properties of the prepared nylons change regularly with the length of methylene segments in diamines. In addition, nylon 2 20 has a relatively low molecular weight and much different melting and thermal decomposition behaviors in comparison with other nylons. Received: 21 June 2OO2/Revised version: 18 September 2002/ Accepted: 18 September 2002 Correspondence to Deyue Yan E-mail: dyyan@mail.sjtu.edu.cn Tel: 0086-21-54742863 Fax: 0086-21-54741297     

基于MatLab的线性代数教学应用

文章针对学生学习线性代数困难原因的分析,说明在线性代数中引入Matlab进行教学改革创新的必要性。通过Matlab程序在初等矩阵教学中演示和练习,使学生能够直观形象地理解和掌握线性代数知识,为后续线性代数的学习打下牢固的基础。     

ZnHZSM-5催化丙烷芳构化的失活动力学研究

在等温积分反应器中实验研究了由丙烷制取轻质芳烃BTX（苯、甲苯及二甲苯）的芳构化过程中，锌改性的HZSM－5催化剂的积炭失活对反应过程的影响，通过对常压、不同反应温度下的实验数据所进行的动力学分析，建立起了失活动力学模型，并通过拟合实验数据对模型做了筛选，最终确定了基于Langumir-Hinshelwood模型的反应速率方程和由独立失活机理推出的2级独立失活速率方程，该模型对深入了解轻烃芳构化反应及指导反应器设计均具有重要的意义。     

环己烷在Au-Co/SBA-15上选择性氧化的研究

以沉积-沉淀法制备了Au-Co/SBA-15催化剂,在没有任何有机溶剂或助剂的条件下,研究了以空气为氧化剂的环己烷选择性氧化。当Au-Co/SBA-15催化剂中金的质量百分含量为1.0%,催化反应在423 K 3.0 MPa下进行120 m in时,催化效果最好,此时环己烷的转化率为22.7%,环己酮和环己醇的总选择性为95.2%,酮醇比为2.9,且催化剂重复使用五次后活性基本不变。     

PP/弹性体/无机纳米粒子复合材料的研究进展

概述了目前PP 弹性体 无机纳米粒子三元复合体系的研究进展情况,包括:基体树脂的选择与改性、弹性体尤其是新型聚烯烃弹性体(POE)的应用、无机纳米粒子对复合体系的影响、增韧增强机理的研究等。     

Charge/discharge characteristics of sulfur composite cathode materials in rechargeable lithium batteries

The charge and discharge characteristics of lithium batteries with sulfur composite cathodes have been investigated. The sulfur composites showed novel electrochemical characteristics. The analysis of the differential capacity indicated that the discharge process showed two voltage plateaus of 2.10 V and 1.88 V, and the charge process also presented two voltage plateaus of 2.22 V and 2.36 V. The overcharge test showed that the composite cannot be charged over 4.0 V, the voltage always stopped at about 3.9 V during charging, indicating that the composite presented the intrinsic safety for the overcharge of lithium batteries. The overcharge can cause serious safety problem for the conventional Li-ion batteries. The overcharge test also showed that the batteries with sulfur composite were destroyed when the upper cut-off voltage was over 3.6 V. However, the composite presented good reversible capacity after it was deep discharged even to 0 V. It showed stable cycleability and high cycling capacity of 1000 mAh g⁻¹ when cycling between 0.1 V and 3.0 V, indicative of the different characteristic from the conventional oxide cathode materials. The prototype polymer battery with the composite cathode material presented the energy density of 246 Wh kg⁻¹ and 401 Wh L⁻¹.     

An XML-based approach to represent generic bill of materials

To solve the difficulty in describing the generic bill of material (GBOM) with the conventional tabular structure in a relational database system,a novel XML-based approach is presented to represent GBOM. It can represent and maintain one generic structure that encompasses all variants of a product. With the combination of product-oriented notation,this approach further gives a high degree of flexibility to support the user in the product variant specification task. The generic BOM system is then introduced for the particular product variant,and a prototype system has been developed. It is indicated that the presented approach is feasible.     

自源无线温度检测技术的研究与应用

基于温差模块、DS18B20和红外技术的自源无线温度检测技术,利用故障发热部位与环境的温度差发电自给,解决高压现场内难以获得低压电源的问题;利用红外线传输信号,避免在高压变电站中布线和信号受高压现场的强电磁干扰.实验结果表明,半导体温差模块输出电压与温差在一定范围内呈线性关系,温差越大,输出电压越大.采用带有超低压启动器的DC/DC电压提升电路进行电压提升,解决实际应用中由于温差过小而导致的半导体温差模块输出电压过低,不足以提供所需的电压问题.     

浅析数据仓库中的元数据管理技术

数据仓库是数据库的发展方向之一,对企业管理和决策支持起着重要的辅助作用.简要介绍了数据仓库和元数据的基本概念,重点阐述了元数据的功能、管理、CWM标准、来源,并就元数据具体应用进行了初步的研究和探讨.