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71.
Jun Rong Li Jun Wang Jia Rui Xu Ming Qiu Zhang Min Zhi Rong Qiang Zheng 《Composites Science and Technology》2006,66(16):3126-3131
The authors of this paper synthesized a series of amphiphilic triblock copolymers of polystyrene-b-poly(ethylene glycol)-b-polystyrene (PS-PEG-PS) having different PEG/PS ratios with nearly identical molecular weights of the entire copolymers. The interfacial interactions in the composites consisting of carbon black and the copolymers can thus be tailored. When these conducting composites are exposed to certain solvent vapors, their electrical resistances greatly increase, showing the gas sensitivity. The present work indicated that this switching behavior is controlled by the structural relaxation of the composites because matrix swelling acts as the main mechanism. The response time has been correlated with absolute temperature by Arrhenius equation, and the estimated activation energy reflects mobility of the fillers involved in the solvent induced expansion of the surrounding polymer. Therefore, by using the gas sensibility of the conductive composites, the structure evolution of the composite materials in solid state and the effect of filler/matrix interfacial interaction on the relaxation property of the matrix polymer has been inspected. It was found that lower activation energy represents stronger interfacial interaction in case good solvent of the matrix was used for the test. 相似文献
72.
Biomimetic synthesis of spherical nano-hydroxyapatite in the presence of polyethylene glycol 总被引:1,自引:0,他引:1
Spherical nano-hydroxyapatite (nano-HA) was synthesized successfully by a biomimetic method using Ca(NO3)2·4H2O and (NH4)3PO4·3H2O as reagents in the presence of polyethylene glycol (PEG). The crystalline phase, microstructure, chemical composition, and morphology of the obtained samples were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM). The results show that spherical nano-HA with diameter of 30–50 nm can be synthesized in the presence of a certain concentration (2–6%) of PEG. The crystallinity of HA powder synthesized in the presence of PEG was higher than that synthesized in the absence of PEG, but the crystallinity of HA reduced with increasing the concentration of PEG. The electrical conductivity (EC) of the solution revealed that PEG reduced the transfer rate of Ca2+ in the process of HA crystallization, indicating the interaction between PEG and HA. The possible mechanism of formation spherical nano-HA was discussed. 相似文献
73.
A new efficient numerical method and the dynamic analysis of composite laminates with piezoelectric layers 总被引:1,自引:0,他引:1
Firstly, a numerical method for the inversion of Laplace transform is developed and its accuracy is shown through examples. Then, a state-vector equation for the dynamic problems of piezoelectric plates is deduced directly from a modified mixed variational principle for piezoelectric bodies and its exact solution for the dynamic problems of simply supported rectangle piezoelectric plate is simply given. For multilayered hybrid plates, we derive the solution in terms of the propagator matrices. The techniques accounts for the compatibility of generalized displacements and generalized stresses on the interface both the elastic layers and piezoelectric layers, and the transverse shear deformation and the rotary inertia of laminate are also considered in the global algebraic equation of structure. Meanwhile, there is no restriction on the thickness and the number of layers. As an application of the numerical inversion of Laplace transform presented in this paper, typical numerical examples of the harmonic vibration and transient response are proposed and discussed. Since the highly accurate numerical results, they can serve as benchmarks to test various thick plate theories and various numerical methods, such as the finite and boundary element methods for transient response problems. 相似文献
74.
In this research, Ni/SiO2 catalyst was modified with different amount of Gd2O3 and characterized with temperature-programmed desorption of CO2 (CO2-TPD) and NH3 (NH3-TPD), temperature-programmed reduction with H2 (H2-TPR) and X-ray diffraction (XRD). It was found that Gd2O3-modified Ni/SiO2 catalysts possessed higher CO2 adsorption and activation ability due to the formation of surface carbonate species. H2-TPR and XRD characterizations found that the strong interaction among nickel, Gd2O3 and SiO2 took place, which improved the dispersion of Ni. Gd2O3-modified Ni/SiO2 catalysts exhibited higher activity and stability for the combined oxy-CO2 reforming of methane in fluidized-bed reactor. The H2/CO ratio in produced syngas could be controlled via controlling reaction temperature and CO2/O2 ratio in feed. 相似文献
75.
��չ����Ȼ��Ϊԭ�ϵ�ȼ�ϵ������ 总被引:6,自引:0,他引:6
研究燃料汽车及其氢源系统是当今国内外能源工业与汽车工业的共同课题,而优选制氢能源则是这一课题的关键。章介绍了利用能源、经济、环境(EEE)——生命周期评估(LCA)这一综合评估方法,针对以天然气、煤或石油作为制氢能源的多种燃料电池氢源供应方式以及配套的燃料电池汽车系统,从经济性、能源利用效率和环境影响三个方面进行了生命周期清单分析和EEE综合评价。结果显示:天然气作为发展燃料电池汽车氢源的一次能源,具有氢制取技术路线多样化、经济上竞争力强、能源利用效率高和环境效益好等诸多优势,应为燃料电池汽车的首选制氢能源。对这一评估模型的敏感性分析显示,即使在天然气价格波动较大时,天然气制甲醇--甲醇车载重整车和天然气制氢--纯氢车这两个方案仍然最具优势。 相似文献
76.
77.
提高实现的并行性和实时性是目前FFT(快速傅里叶变换)研究的一个重点。介绍了在CPLD(复杂可编程逻辑器件)中实现高基数FFT的一种方法。以较低基数的FFT搭建高基数的FFT,大大提高了变换的速度。文中以基16 FFT的实现为例,介绍了以基2实现基16运算的过程,着重描述了运算核的设计以及数据的存储和调用。 相似文献
78.
79.
本研究在简介国际上先进的变参设计几种方法及优点后,叙述了一个国家863/CIMS项目:CAD/CAPP/NCP集成系统中二维尺寸驱动的变参设计子系统的构成与功能;然后着重阐述了本系统采用的尺寸驱动的变参设计思想和几何约束建立的原则,并提供了系统数据结构,最后以几个实例证明了此方法的正确性与工程实用性。 相似文献
80.
随着电力和电子技术的飞速发展,相应的元器件向高频化,小型化,高效率和节能的方向发展,从而对元器件用材料也提出了更高要求。为此,本文概述了冶金部钢铁研究总院近年来所研究的用于开关电源,脉冲变压器,传感器,电流互感器和电感器等方面的非晶软磁合金的性能及其应用概况。 相似文献