The α- to β-Si3N4 transformation in the presence of liquid silicon

The compacts consisted of , -Si₃N₄ and free silicon are heat treated in the range 1650° C to 1750° C in an argon atmosphere in order to observe the following behaviours; the to phase transformation and variations of the microstructure during heat treatment in silicon nitride. For the microstructural observation of the heat treated specimens, the same grains in the polished surface were investigated before and after eliminating the retained silicon by etching. The to phase transformation, in this case, occurs via silicon melts irrespective of added -Si₃N₄. Both and phases are soluted and precipitated into molten silicon and their morphology are changed from an equiaxed shape to prismatic one. Although elongated grains are precipitated at low temperature or in the early stage of heat treatment, fine precipitated grains are mainly observed with increasing heat treating temperature.     

使用Dreamweaver结合ASP技术构建企业科技与节能管理系统

节能减排和科技创新是我国保持可持续发展的重要保障,国家高度重视这两项工作,十一五以来陆续出台了鼓励节能减排和科技创新的相关鼓励政策。节能与科技管理系统是企业展示自身节能减排和科技创新成果和经验的窗口,在节能减排和科技创新工作中发挥着重要作用。本文介绍了作者利用Dreamweaver和ASP技术构建企业节能与科技管理系统的一些认识和经验。     

基于JAVAEE的工作流引擎设计的探究

工作流系统作为办公自动化软件重要组成部分,其不仅能将企业相应数据有效的和网络连接起来,同时也能将之前单独的计算机个体组成一个有机的并能自动化运行的网络系统,以便为企业提供更多信息,为企业更好的服务。就目前来看,工作流系统不仅仅在办公自动化软件中应用,在其他生产销售领域也得到了广泛应用。但是这种工作流数据在一定程度上还处于运转过程中,而新的基于JAVAEE工作流引擎程序在目前不同企业使用中,其效果还是比较可观的。本文主要从工作流管理系统概念及构成、JAVAEE技术概况、基于JAVAEE工作流引擎的设计等方面,对基于JAVAEE的工作流引擎设计进行相应探讨。     

探索物联网人才培养模式

物联网在众多领域有着广泛的应用,产业空间巨大。物联网人才的培养变的尤为重要。根据国家和东莞经济结构的调整及发展战略,本着服务地方经济的理念,调整高等院校的专业方向和专业结构;根据社会经济的需要和安排,制订高等院校的专业人才培养方案和课程标准;根据地方经济环境,建设物联网专业,培养企业需求的人才。     

基于多波束合成孔径声呐的三维场景构建仿真研究

多波束合成孔径声呐(Multibeam Synthetic Aperture Sonar)是一种新型的图像声呐,具有独特的阵列结构,兼具合成孔径声呐与多波束测深声呐的优点。本文为了满足多波束合成孔径声呐仿真的需求,提出了一种基于延时表和阴影区的多波束合成孔径声呐的三维场景构建仿真模型。此仿真模型在点目标的基础上,根据延时表算法的基础上构建三维数据仿真模型,并通过阴影区算法模型添加不同波束照射下目标区域的阴影区域。点目标和体目标的仿真数据结构表明了此仿真模型的可行,可以为多波束都合成孔径声呐的信号处理、目标识别、测深成像绘图提供有力的支持。     

硝基联苯、氨基联苯及啶酰菌胺的高效液相色谱分析方法

建立了一种高效液相色谱定量方法,测定以4-氯-2'-硝基联苯制备4-氯-2'-氨基联苯合成啶酰菌胺路线各步反应中的有效成分含量.采用InertSustain ODS-C18不锈钢柱(250 mm×4.6 mm i.d.×5μm)和二极管阵列检测器,以乙腈和0.02％磷酸水为流动相,流速为1.0 mL/min,在220 nm波长下对中间体4-氯-2'-硝基联苯进行分离和定量分析;在254 nm波长下对中间体4-氯-2'-氨基联苯进行分离和定量分析;在254 nm波长下对啶酰菌胺进行分离和定量.分析结果表明,4-氯-2'-硝基联苯保留时间约24.3 min,线性相关系数为1.0000,标准偏差为0.04,变异系数为0.34％,平均回收率为100.04％;4-氯-2'-氨基联苯保留时间约18.0 min,线性相关系数为1.0000,标准偏差为0.05,变异系数为0.33％,平均回收率为99.94％;啶酰菌胺保留时间约11.9 min,线性相关系数为1.0000,标准偏差为0.21,变异系数为0.32％,平均回收率为100.09％.方法 操作简便,精密度与准确度较高,满足定量分析要求.     

预测帧编码中基于场景信息的宏块模式跳过算法*

在对场景信息进行分析的基础上,提出了H.264/AVC中预测帧的一种快速算法.对于未发生场景切换的预测帧,采用INTRA模式跳过算法(IMSA),跳过该帧中所有的INTRA模式的决策过程.对于发生场景切换的预测帧,跳过INTER模式的决策过程(PMSA).仿真结果显示,与采用完整的率失真优化(RDO)决策过程相比,未发生场景切换时,所提方法能减少30%～60%的编码时间;发生场景切换时,能减少60%～70%的编码时间,并且未导致明显的图像质量下降和码率的增加.     

Effect and Evolution of Oxide Film in the HDH-Ti Powder Surface on Densification Behavior During Sintering

Metallurgical and Materials Transactions A - In this work, we used hydride-dehydride Ti (HDH-Ti) powders (with the oxygen levels of 0.17 and 0.51 wt pct, respectively) combined with microstructural...     

Mold-filling characteristics of AZ91 magnesium alloy in the low-pressure expendable pattern casting process

The magnesium (Mg) alloy low-pressure expendable pattern casting (EPC) process is a newly developed casting technique combining the advantages of both EPC and low-pressure casting. In this article, metal filling and the effect of the flow quantity of inert gas on the filling rate in the low-pressure EPC process are investigated. The results showed that the molten Mg alloy filled the mold cavity with a convex front laminar flow and the metal-filling rate increased significantly with increasing flow quantity when flow quantity was below a critical value. However, once the flow quantity exceeded a critical value, the filling rate increased slightly. The influence of the flow quantity of inert gas on melt-filling rate reveals that the mold fill is controlled by flow quantity for a lower filling rate, and, subsequently, controlled by the evaporation of polystyrene and the evaporation products for higher metal velocity. Meanwhile, the experimental results showed that the melt-filling rate significantly affected the flow profile, and the filling procedure for the Mg alloy in the low-pressure EPC process. A slower melt-filling rate could lead to misrun defects, whereas a higher filling rate results in folds, blisters, and porosity. The optimized filling rate with Mg alloy casting is 140 to 170 mm/s in low-pressure EPC.     

鞍钢鲅鱼圈4038m3高炉高比例使用中块焦炭生产实践

针对鞍钢股份有限公司鲅鱼圈钢铁分公司4038 m3高炉高比例使用中块焦炭后出现的风量萎缩、顺行变差,尤其是高炉休送风恢复过程中炉缸活跃性差、煤气流中心通道打不开、频繁崩滑料现象,提出采取合理匹配上下部调剂、组织好炉前渣铁排放、小焦布料制度以及改善休风料结构等措施.实践后,高炉实现了中块焦比为90 kg/t情况下的长期稳定顺行,休送风恢复未出现超时现象,适应了高比例使用中块焦炭的生产.