注射成型模具排气槽的设计

塑料注射成型模具的排气方式和排气槽结构直接影响塑料制品质量。介绍了塑料注射成型模具的排气方式、排气槽设计经验以及切实可行的排气方案和排气槽结构。     

高岭土尾砂综合利用工艺研究

高岭土是制瓷工业的主要原料，在开采用加工过程中生产大量尾砂，污染环境且导致资源浪费，通过本试验研究，从尾砂中分选出工业上可综合利用的长石，云母等系列产品，并实现了无尾矿选矿新工艺。     

LDE融合光谱回归分类的光照变化人脸识别

针对光照变化人脸识别问题中传统的光谱回归算法不能很好地进行特征提取而严重影响识别性能的问题,提出了局部判别嵌入优化光谱回归分类的人脸识别算法。计算出训练样本的特征向量;借助于数据的近邻和分类关系,利用局部判别嵌入算法构建分类问题所需的嵌入,同时学习每种分类的子流形所需的嵌入;利用光谱回归分类算法计算投影矩阵,并利用最近邻分类器完成人脸的识别。在两大人脸数据库扩展YaleB及CMU PIE上的实验验证了该算法的有效性,实验结果表明,相比其他光谱回归算法,该算法取得了更高的识别率、更好的工作特性,并且降低了计算复杂度。     

气烧明焰辊道窑烧嘴的三维数值模拟

采用FLUENT软件对气烧明焰辊道窑烧嘴进行三维数值模拟,模拟了其在辊道窑烧成带内的燃烧工况,研究了烧成带内烟气不同流速对窑内温度与烧嘴燃烧速度的影响,为辊道窑的运行提供了有益的参考。     

C2S转晶反应定量调控

综合报道了Ｃ２Ｓ转晶反应定量调控的研究结果。宏观工艺研究表明：γ－Ｃ２Ｓ适宜烧成温度为１２５０－１５００℃，冷却方式与速率对转晶反应影响不显著；微观研究表明：调节β－Ｃ２Ｓ稳定剂浓度可定量调控Ｃ２Ｓ转晶反应，稳定剂稳定效果与烧成温度有关，且受其它杂质离子干扰，Ａｌ２Ｏ３，Ｆｅ２Ｏ３组晶反应有双向调控效应。     

Integrated UV-based photo microreactor-distillation technology toward process intensification of continuous ultra-high-purity electronic-grade silicon tetrachloride manufacture

Ultra-high-purity silicon tetrachloride (SiCl₄) is demanded as an electronic-grade chemical to meet the stringent requirements of the rapidly developing semiconductor industry. The high requirement for ultra-high-purity SiCl₄ has created the need for a high-efficient process for reducing energy consumption as well as satisfying product quality. In this paper, a mass of production technology of ultra-high-purity SiCl₄ was successfully developed through chlorination reaction in the ultraviolet (UV)-based photo microreactor coupled with the distillation process. The influences of key operational parameters, including temperature, pressure, UV wavelength and light intensity on the product quality, especially for hydrogen-containing impurities, were quantified by the infrared transmittance of Fourier transform infrared spectroscopy (FT-IR) at 2185 cm^-1 and 2160 cm^-1 indicating that characteristic vibrational modes of Si—H bonds, as well as the operating conditions of distillation were also investigated as key factors for metal impurities removing. The advanced intensification of SiCl₄ manufactured by the integration of photo microreactor and distillation achieves the products with superior specifications higher than the standard commercial products.     

如何建立石化企业信息数据库--中石化股份有限公司巴陵分公司价格信息系统分析

针对中石化巴陵分公司价格信息系统实施案例进行分析，从用户需求、系统目标、系统体系结构、操作界面和系统特点等方面进行剖析，说明了从Internet这个庞大的信息库中迅速、准确地提取资料，并建立信息数据库的方法和重要性。     

Effect of Cr3C2 on Valence-Electron Structure and Plasticity of Rim Phase in Ti(C,N)-Based Cermets

Based on the empirical electron theory of solids and molecules, the valence-electron structure (VES) of the rim phase in Ti(C,N)-based cermets was calculated, and the relationship between the VES and plasticity was determined. The results indicated that the plasticity of the rim phase in a Ti(C,N)-based cermet could be defined using the sum of the n _a values for the covalent bonds, and that chromium dissolution in the rim phase improved the plasticity of the rim phase. Moreover, a series of experiments showed that adding Cr₂C₃ to a typical Ti(C,N)-based cermet strengthened the interface. Based on those results, a Ti(C,N)-based cermet with added Cr₃C₂ was manufactured; the new cermet had more than twice the transverse rupture strength of a typical cermet.     

Integrated UV-based photo microreactor-distillation technology toward process intensification of continuous ultra-high-purity electronic-grade silicon tetrachloride manufacture

Ultra-high-purity silicon tetrachloride (SiCl₄) is demanded as an electronic-grade chemical to meet the stringent requirements of the rapidly developing semiconductor industry. The high requirement for ultra-high-purity SiCl₄ has created the need for a high-efficient process for reducing energy consumption as well as satisfying product quality. In this paper, a mass of production technology of ultra-high-purity SiCl₄ was successfully developed through chlorination reaction in the ultraviolet (UV)-based photo microreactor coupled with the distillation process. The influences of key operational parameters, including temperature, pressure, UV wavelength and light intensity on the product quality, especially for hydrogen-containing impurities, were quantified by the infrared transmittance of Fourier transform infrared spectroscopy (FT-IR) at 2185 cm⁻¹ and 2160 cm⁻¹ indicating that characteristic vibrational modes of SiH bonds, as well as the operating conditions of distillation were also investigated as key factors for metal impurities removing. The advanced intensification of SiCl₄ manufactured by the integration of photo microreactor and distillation achieves the products with superior specifications higher than the standard commercial products.     

Glass‐transition temperature in the curing process of bismaleimide modified with diallylbisphenol A

The T_g‐conversion relationship, during the thermal curing of different stoichiometric formulations of 1,1′‐(methylene‐di‐4,1‐phenylene) bismaleimide (BMI), modified with o,o′‐diallyl bisphenol A (DABA), was investigated. The DiBenedetto equation was used to model this relationship for the formulation of DABA‐1 (BMI : DABA, 1 : 1). Based on this model, the T_g‐conversion relationship of formulation DABA‐0.5 (BMI : DABA, 1 : 0.5) was modeled. The high consistency between the model curve and experimental data showed that the change of T_g, attributed to copolymerization between BMI and DABA in DABA‐0.5, in the low‐conversion regime, was the same as that in DABA‐1. This also verifies that, for the formulation DABA‐0.5, copolymerization and homopolymerization do not overlap with each other. The reactions progressed sequentially and homopolymerization occurred after completion of copolymerization. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 91: 3244–3247, 2004