Structure study on the thermoelectric materials CexCo4Sb12 (x = 0.5, 1.0) by neutron diffraction

In order to understand the relationship between crystal structure and thermoelectric properties, the neutron diffraction patterns of the thermoelectric materials with the nominal composition Ce_xCo₄Sb₁₂ (x = 0.5, 1.0) were measured at room temperature, the data were fitted by the Rietveld profile refinement method using the Fullprof2k program. It is found that the sample Ce_0.5Co₄Sb₁₂ is composed of two phases, its major phase is CoSb₃ with skutterudite-structure and the Ce atom is not incorporated into the lattice, the impurity is monoclinic CoSb₂. In the case of Ce_1.0Co₄Sb₁₂, the major phase is filled skutterudite, about 10% of the 2a site is occupied by Ce atom, the second phase is monoclinic CoSb₂.     

用PowerBuilder实现标签页式应用程序界面

标签页式用户界面简洁、清晰，适用于从小型到大型的各类数据库应用程序。本介绍一种基于PowerBuilder和PFC的标签页式界面的实现方法。     

含3-三氟甲基的均三唑并[3,4-b]-1,3,4-噻二唑类化合物的合成

以 3-三氟甲基 - 4-氨基 - 5 -巯基 - 1 ,2 ,4-三唑为原料 ,分别与 2 - ,3- ,4-吡啶甲酸及α-萘乙酸在 POCl3催化下反应 ,制得 4种新的 3-三氟甲基 - 6-取代均三唑并 [3,4- b]- 1 ,3,4-噻二唑( 3a～ 3d) ,并利用 EA,IR,1H NMR等确定了其结构     

关于抽水蓄能电站水库优化调度的研究

针对某抽水蓄能电站水库运行的特点，在满足电力系统调度要求的前提下，以整个调度周期内总发电收益现值最大为目标建立了优化调度模型。通过径流描述以及应用动态规划法进行优化计算，求解抽水蓄能电站水库优化调度方案。在求解寻优的过程中，既兼顾了面临时段和余留时期的效益，又考虑上水库的天然来水和下水库的区间来水，通过分析表明，所提模型与计算方法是可行和实用的。     

滑步与再同步过程的微观结构分析

按照定常两机电力系统平衡点的属性，将其轨迹分类为稳定的结点、不稳定的结点、稳定的焦点、不稳定的焦点和鞍点这5种不同运动模式。利用互补群惯量中心(CCCOI)：R^n→R^2保稳映射将实际多机受扰轨迹映射为时变的两机等值轨迹，进而分析后者如何由对应于上述运动模式的多个轨迹段构成，并用符号序列反映其微观结构。以电力系统从一连串的滑步进入再同步为例，研完了多机电力系统的后期动态行为会随着参数的细微变化而显著改变的现象。如果一段具有鞍点特性的相轨迹的起始点从稳定流形的一侧变到另一侧，那么不论系统参数的变化多么细微，其后继轨迹将有完全不同的动态。     

一种基于显微多光谱宫颈细胞图像自动分割方法

介绍了一种基于多光谱宫颈显微图像自动分割方法。细胞涂片每一个局部区域经过显微镜放大后再通过电调谐光器件分别取出不同光谱波段的图像，经过CCD送入计算机后得到该视场分析所需的多光谱图像。从所获得的多光谱图像中选择一定的波段图像对数变换相除、多阈值分割和形态学操作，最后获得宫颈细胞的胞浆和胞核覆盖层。本文首次将多光谱分析应用到宫颈显微图像分割中，具有分割准确、分割速度快、能够去除胞浆重叠和受外界干扰少的特点。     

Providing adaptive QoS to layered video over wireless local area networks through real-time retry limit adaptation

Robust streaming of video over 802.11 wireless LANs (WLANs) poses many challenges, including coping with packets losses caused by network buffer overflow or link erasures. In this paper, we propose a novel error protection method that can provide adaptive quality-of-service (QoS) to layered coded video by utilizing priority queueing at the network layer and retry-limit adaptation at the link layer. The design of our method is motivated by the observation that the retry limit settings of the MAC layer can be optimized in such a way that the overall packet losses that are caused by either link erasure or buffer overflow are minimized. We developed a real-time retry limit adaptation algorithm to trace the optimal retry limit for both the single-queue (or single-layer) and multiqueue (or multilayer) cases. The video layers are unequally protected over the wireless link by the MAC with different retry limits. In our proposed transmission framework, these retry limits are dynamically adapted depending on the wireless channel conditions and traffic characteristics. Furthermore, the proposed priority queueing discipline is enhanced with packet filtering and purging functionalities that can significantly save bandwidth by discarding obsolete or un-decodable packets from the buffer. Simulations show that the proposed cross-layer protection mechanism can significantly improve the received video quality.     

燃油泵弹性薄元件断裂原因分析

从显微组织、断口形貌、原材料状态、加工工艺和装配等方面对燃油泵弹性薄元件在生产中常见的断裂原因进行了分析；并对其进行了工艺试验的对比分析。认为其失效模式主要与氢脆、回火脆及原材料组织状态有关。提出了预防措施。     

2,4,6-三氨基嘧啶在玻碳电极上的电化学行为

用线性扫描伏安法 (LSV)、循环伏安法 (CV)和微分脉冲伏安法 (DPV)等电化学手段研究了 2 ,4,6 三氨基嘧啶 (TAP)的电化学行为。结果表明 :该化合物在玻碳电极表面存在吸附特性 ,在 0 .1 0mol·L- 1 的 pH 5 .0Britton Robinson (B R)缓冲溶液中于1 .2 0V(vs.Ag/AgCl)处有一灵敏的氧化峰。在选定的最佳条件下 ,其浓度在 8.0× 1 0 - 6～ 3.2×1 0 - 4 mol·L- 1 范围内与氧化峰电流有良好的线性关系 ,检测限为 6.5× 1 0 - 6mol·L- 1 。