强化两相混合的超临界技术制备聚乳酸微粒

针对商品化聚乳酸微球粒径分布较宽难于适用气溶胶给药要求的不足,采用水力空化混合强化超临界流体辅助雾化技术(SAA-HCM)制备聚乳酸(PLA)超细微粒.该技术主要特点是通过在超临界流体和液相进料处引入水力空化混合器,强化两相间的混合.考察SAA-HCM过程混合器压力、温度、沉淀器温度、进料中CO2与液体溶液质量流量比和溶液质量浓度等操作参数对微粒形态和粒径分布的影响,成功制备出球形度较好,粒径分布较窄(1～3μm)的PLA微球.经X射线衍射(XRD)分析和差示扫描量热(DSC)分析显示,与原料PLA相比,微球晶型及热曲线变化不大,但结晶度下降.同时把操作参数与相行为进行关联,探讨了影响颗粒形貌的机理.对比超临界流体辅助雾化法(SAA)的实验结果表明:水力空化的引入能有效强化混合器内的两相传质,混合更好,能制备出适用于气溶胶给药要求的超细微粒.     

Investigation on film cooling characteristics from a row of converging slot-holes on flat plate

Experimental and numerical researches were conducted to investigate the cooling performance of a single row of consoles (converging slot-hole) on a large-scale flat-plate model. The results show that the coolant flow from a row of consoles shows good lateral uniformity of adiabatic effectiveness, with regions of slightly enhanced cooling occurring between the consoles. For the console cooling geometry, the interaction between coolant jet from inclined console and the mainstream flow results in reasonable vo...     

导电涂料的研制

为了获得性能优良的导电涂料 ,采用对比试验和正交试验的方法对导电涂料进行了研究 ,分别对导电涂料的电阻、硬度、耐冲击强度、柔韧性等性能进行了测试 ,经过试验 ,确定了无机导电涂料的最佳配方为 :石墨 10 0g ,铅酸钡 10g ,三氧化二锑 5g ,二氧化钛 35g ,碳化硅 10g ,硅酸盐溶胶 170g。以此配方研制出了一种成本较低、生产工艺简单、具有良好的导电、导热性能的无机导电涂料。     

高职学生学习主动性意识的缺失与重塑

分析高职学生的特点和学习主动性意识缺失的症状,从学生的学习自觉自信、教师的课堂教学反思、学校的学生评价机制等方面,对高职学生学习主动性意识的重塑策略进行探讨,并提出相应的对策。     

我国宏观经济与证券市场关系的实证分析--基于名义 GDP 和上证指数发展速度的视角

宏观经济和证券市场的关系一直受到人们的关注,由于数据的选取和研究方法上的不同,导致宏观经济与证券市场的关系存在不同的结论或解释。从名义 GDP 和上证指数发展速度的视角,运用 HP 滤波以及 SVAR 等方法实证研究了宏观经济和证券市场的关系。研究发现：宏观经济和证券市场存在显著的因果关系;短期证券市场的波动是经济偶然性波动的预期,两者之间的滞后期效应与当期效应相互影响;方差分解表明宏观经济对于证券市场的长期贡献度很大。     

(Short communication) Degradation of corrosion resistance of Zircaloy-4 in LiOH aqueous solution

To investigate the degradation of corrosion resistance of Zircaloy-4 in LiOH aqueous solution, SIMS (secondary ion mass spectrometry) analysis was performed to examine the profiles of Li~ , K~ , and OH~- in oxide layers formed in the same concentration (0.1 mol/L) LiOH and KOH solutions. Even though the oxide layers have an equal thickness, the penetration depth of K~ is shallower than that of Li~ , and the penetration depth of OH~- corroded in KOH solution is also shallower than that corroded in LiOH solution. It shows that the diffusion of OH~- into oxide layer is accompanied by the corresponding cation. The difference of degradation effect of LiOH and KOH solutions on the corrosion resistance of Zircaloy-4 was discussed.     

Experimental Study of Microstructure Evolution during Tempering of Quenched Steel and Its Application

LARGE-SIZED FORGINGS are usually intensivelyquenched to obtain the desired microstructuredistribution,high strength and hardness.Becauseresidual stresses are high in quenched large-sizedforgings,tempering processes follow quenchingprocesses to reduce the residual stress and obtain goodmechanical properties.Several differentmicrostructures are generated in quenched steelforgings,such as martensite,bainite and retainedaustenite.Modeling of microstructure evolution inquenched steel during …     

AVS-M帧间预测模式快速选择算法的研究

AVS-M是我国拥有自主知识产权的数字音视频编码系列标准的移动视频标准.AVS-M采用率失真优化(RDO)技术进行帧间模式的选择,增加编码过程中宏块进行模式选择的计算复杂度.本文提出一种快速的帧间模式选择算法.该算法首先对SKIP模式提前判决,再采用二分搜索法对帧间模式的选择,对于宏块层的模式划分采用MAD(平均绝对差...     

网络教学心得

该文主要讲了网络教学中必须掌握的知识要点。     

AD7794在高精度低功耗测量装置中的应用

采用AD7794,一种典型的仪用ADC,与超低功耗混合信号处理器MSP430F1611,构成了一个测量计量电路.实际使用表明,该电路具有低功耗、高精度和长期稳定性的特点;实测非线性度不大于10-3量级,能满足大多教工业测量计量的要求.