Ta-2．5W焊接工艺试验研究

通过对Ta-2.5W难熔重金属换热管的一系列焊接工艺试验研究,掌握了钽材的特殊焊接技术工艺和要求,满足了今后制造和修复苯胺装置中硫酸蒸发器管束的需要。     

La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectrics

La doping effects on intergrowth Bi₂WO₆–Bi₃TiNbO₉ ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La³⁺ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La³⁺ content, the site of dopant ion varies, the grain growth of Bi₅TiNbWO₁₅ is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process.     

氧化铝厂渣浆泵机械密封的失效形式及改进措施

本文介绍了渣浆泵机械密封的失效形式,并根据长期现场工作经验,分析了机械密封泄漏的主要原因,据此提出了改进措施,通过对动静环密封面倒角,改变密封面尺寸及载荷系数后有效地解决了由于径向跳动过大而引起的密封面刮碰擦裂的失效问题。     

借鉴英国经验完善中国土地产权流转

本文在简要介绍中、英两国土地产权制度和土地产权流转的基础上，分析了我国土地产权流转过程中出现的问题，如征地过程中的赔偿过低且不完善、国有土地拆迁补偿不公以及补偿的分配方式不公平等问题。由于英国在土地制度方面与中国的相似性，文章借鉴英国土地补偿中的补偿金与改善金相结合原则、土地使用权的租赁行为以及开发收益回馈社会的方法，为完善和健全我国的土地产权流转机制提出措施和建议。     

企业开展质量成本研究工作的思考

质量成本是指企业为保证产品质量而支出的一切费用，以及产品质量未达到规定的标准而造成的一切损失的总和。开展质量成本研究工作是企业深化质量管理和成本管理的一条有效途径。     

岩盐钻井水溶双井连通开采工艺的研究与推广

文章就全国井矿盐采区多年的开采工艺技术，进行了系统的研究与总结，并提出了岩盐钻井水溶开采双井连通的各种开采工艺及其关键技术，具有很强的适用性和推广价值。     

Formation of mushroom-like ZnO microcrystals through a solution calcination process

Mushroom-like ZnO microcrystals have been prepared via a solution calcination route, using Zn(NO₃)₂ as Zn source in the absence of any surfactants, templates or catalysts. This is the first example to prepare mushroom-like crystals as semiconductors, which are expected to show particular physical properties. The ZnO products were investigated by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy and photoluminescence (PL) spectrum measurements. A suitable concentration of Zn(NO₃)₂ solution was important for the growth of the mushroom-like products. The reported synthetic procedure is straightforward and inexpensive, and thus can be readily adopted to produce large quantities of mushroom-like ZnO microcrystals.     

Nanocrystalline Ni coatings strengthened with ultrafine particles

In this study, nanocrystalline Ni powders and thermally sprayed coatings, containing ultrafine AlN particles, were synthesized and characterized. The results indicated that the presence of AlN particles in the powders drastically decreased the dimension of agglomerates formed by cryomilling and increased the surface roughness of the agglomerates. The AlN phase was broken down into ultrafine particles of approximately 30 nm in size. These particles were dispersed in the Ni matrix and enhanced the development of a nanocrystalline structure in the Ni matrix during cryomilling. Selected-area diffraction patterns, obtained from transmission electron microscopy (TEM) and X-ray mapping with scanning electron microscopy (SEM), confirmed the presence of AlN particles in the coatings. The presence of AlN particles also led to an increase in the amount of NiO phase that was distributed in the coating, in the form of ultrafine, round particles. AlN particles increased the microhardness of the Ni coating by approximately 60 pct. Indentation-fracture results also indicated that the fine, dispersed AlN particles raised the apparent toughness of the Ni coating. The synthesized Ni coatings containing ultrafine AlN particles were characterized as equiaxed nanocrystalline grains with an average size of 24 nm, in which twins were observed. The increase in microhardness resulted from both grain refinement and the presence of ultrafine particles. The latter played the primary role in strengthening.     

会计信息失真原因及防范

虚假的会计信息,将严重扭曲股票的价值,扰乱资本市场秩序,侵害投资者的利益。笔者就会计信息失真的原因进行了分析,并就如何防范进行了探讨。