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31.
Thi Thi Nge Makiko Yamaguchi Naruhito Hori Akio Takemura Hirokuni Ono 《应用聚合物科学杂志》2002,83(5):1025-1035
Polyelectrolyte complex based on chitosan and acrylic acid monomer by photoinitiated free‐radical polymerization in the absence of crosslinker showed a large transition in swelling in response to changes in pH of surrounding medium. Their ability to swell arises from polyelectrolyte interactions and molecular structure of the complex. The main properties of interest that related to the molecular structure, swelling volumes, glass transition temperature, and elastic modulus of the complex were investigated. The effect of water content, the only variable in the sample component, played an important role in molecular structure of the complex and as a consequence, the extent of intermolecular linkage, especially amide bonds which in turn governed the degree of swelling of the polyelectrolyte complex in this study. The decreased degree of swelling and higher temperature shift of glass transition temperature was found with increased water content, whereas increased modulus of elasticity of dry complex was found in lower water content of synthesis component. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 1025–1035, 2002 相似文献
32.
Rong-Jun Xie Mamoru Mitomo Kyota Uheda Fang-Fang Xu Yoshio Akimune 《Journal of the American Ceramic Society》2002,85(5):1229-1234
Rare-earth-doped oxynitride or nitride compounds have been reported to be luminescent and may then serve as new phosphors with good thermal and chemical stabilities. In this work, we report the photoluminescence (PL) spectra of europium-, terbium-, and praseodymium-doped Ca-α-SiAlON ceramics. The highly dense ceramics were prepared by hot pressing at 1750°C for 1 h under 20 MPa in a nitrogen atmosphere. Europium-doped Ca-α-SiAlON displayed a single broad emission band peaking at λ= 550–590 nm depending on the europium concentration. The emission bands in the spectra of europium-doped Ca-α-SiAlONs were assigned to the allowed transition of Eu2+ from the lowest crystal field component of 4 f 6 5 d to 8 S7/2 (4 f 7 ) ground-state level. The emission spectra of terbium- and praseodymium-doped Ca-α-SiAlON ceramics both consisted of several sharp lines, which were attributed to the 5 D4 →7 F j ( j = 3, 4, 5, 6) transitions of Tb3+ and 3 P0 →3 H j ( j = 3, 4, 5) transitions of Pr3+ , respectively. In particular, the terbium-doped α-SiAlON ceramics showed a strong green emission among these phosphors. 相似文献
33.
Yutaka Asako Hisayoshi KamikogaHisashi Nishimura Yoshiyuki Yamaguchi 《International Journal of Heat and Mass Transfer》2002,45(11):2243-2253
Compression is one solution to improve the strength of softwoods. The effective thermal conductivities of compressed Japanese cedars (cryptomeria japonica), which were compressed in the radial direction of the wood, were measured. Both the effective thermal conductivities in the tangential and fiber directions increase proportionally to the density increment due to the compression. However, the thermal conductivity in the radial direction (compression direction) increases slightly with the density increment. Numerical computations were conducted to explain the characteristics of thermal conductivity in the radial direction by using a microscopic heat conduction model for the compressed wood. The numerical results were compared with the measured values. And the physical mechanism of the heat conduction in the compressed woods is discussed. 相似文献
34.
35.
Yamaguchi Y. Mitsumoto M. Sengoku M. Abe T. 《Geoscience and Remote Sensing, IEEE Transactions on》1992,30(1):186-189
An FM-CW radar system was applied to detect a human body buried in a very wet snowpack. This radar uses the L -band microwave frequency with a maximum output power of 100 mW, and utilizes digital signal processing techniques. Field experiments were carried out to detect and map a human body embedded at a depth of 125 cm in a natural snowpack. The radar is shown to have a potential ability to detect avalanche victims, indicating that it may become a tool for snow rescuer operations 相似文献
36.
The conventional loading criterion in the theory of plasticity becomes ambiguous when it is applied to materials that exhibit straining softening. For instance, it can not differentiate the softening behavior from the unloading process. On the other hand, the loading criterion proposed recently by Qu and Yin is free from such problems, and is more suitable for a general elasto-plastic analysis by finite element method. In the first part of this paper the proposed loading criterion is first reviewed and discussed to highlight the difficulties associated with the inequality conditions used in the conventional as well as the proposed loading criteria. This paper then proceeds to discuss the proposed criterion and reveals its implications. Although the proposed inequality conditions are not generally known in the field, it is found that they are essential and significant in the theory of plasticity. 相似文献
37.
K-S. Park S-H. Park Y-K. Sun K-S. Nahm Y-S. Lee M. Yoshio 《Journal of Applied Electrochemistry》2002,32(11):1229-1233
The structural and electrochemical properties of LiNiO2 powders were investigated as a function of the oxygen flow rate employed in the preparation of lithium nickel oxide. It was found that oxygen played an important role in the synthesis of highly crystallized LiNiO2(R3¯m). In the crystallization process of LiNiO2, a deficiency of oxygen in the calcination reactor induced the formation of impurities and cubic rock-salt structure (Fm3m) in LiNiO2 powders. For LiNiO2 prepared at higher oxygen flow rates, the electrode delivered high discharge capacities with relatively good retention rates. But very low electrode capacity was obtained from LiNiO2 prepared at lower oxygen flow rates. 相似文献
38.
39.
Y Ota Y Nakano H Yamaguchi K Yoshida T Shirafuji A Adachi 《Canadian Metallurgical Quarterly》1993,20(8):1055-1057
In a 63-year-old male patient with gastric cancer having multiple liver metastases, the metastatic lesions responded well to postoperative staggered intraarterial infusion therapy with MTX and 5-FU. The intraarterial infusion therapy was administered once a week. A total of 5 courses of this therapy produced marked regression of liver metastases and remarkable necrosis. The effect was thus rated as PR. The patient is healthy and has been successfully rehabilitated. His dose is oral 5-FU (200 mg x 2). 相似文献
40.
H. Azuma A. Takeuchi T. Ito H. Fukushima T. Motohiro M. Yamaguchi 《Solar Energy Materials & Solar Cells》2002,74(1-4)
The pulsed KrF excimer laser annealing of silicon films for solar cell with EBEP-CVD and LP-CVD was studied theoretically and experimentally. Three-dimensional thermal diffusion equation for microcrystalline and amorphous silicon was solved by using the finite difference methods. The results of our heat-flow simulation of laser re-crystallization in a laser irradiation with 50 ns pulse duration almost agree with the experimental results in re-crystallization depth of 0.7 μm for microcrystalline silicon (EBEP-CVD) and 0.4 μm for amorphous silicon (LP-CVD) in a single pulse excimer laser annealing. 相似文献