Effect of extrusion ratios on hardness,microstructure, and crystal texture anisotropy in pure niobium tubes subjected to hydrostatic extrusion

Nb tubes were fabricated through hydrostatic extrusion at extrusion ratios of 3.1 and 6.1 at ambient temperature, and then their microstructure, texture, and Vickers hardness were investigated based on electron back-scattered diffraction (EBSD) data. The fraction of low-angle boundaries (LABs) largely decreased with a sharp decrease in mean grain sizes after hydrostatic extrusion and was not proportional to extrusion ratios, assuming that mixed-asymmetrical junctions forming LABs dissociate at high extrusion ratios from the external stress (>981 MPa) with thermal activation by the generated heat. The correlation between grain size and Vickers hardness followed the Hall?Petch relationship despite the texture gradient of the 〈111〉 cyclic fiber textural microstructure at low extrusion ratios and the 〈100〉 true fiber textural microstructure at high extrusion ratios. The increase in hydrostatic pressure on the Nb tubes contributed to texture evolution in terms of extrusion ratios due to the difference between {110}〈111〉 and {112}〈111〉 components based on EBSD data.     

Syntheses and photovoltaic properties of polymeric sensitizers using thiophene-based copolymer derivatives for dye-sensitized solar cells

We synthesized the thiophene-based copolymers (P(3TAF-co-3TAa)-A-n and P(3TAF-co-3TAa)-B-n) using two different kinds of thiophene monomers, (N-(3-thienylmethylene)-2-aminofluorene and 3-thiophene acetic acid), as sensitizers on the DSSCs. P(3TAF-co-3TAa)-A-n (n=1, 2, 3) was synthesized with different molar ratios (3TAF:3TAa=1:5, 1:10, 1:20) of monomers at room temperature, respectively. Also, P(3TAF-co-3TAa)-B-n (n=1, 2, 3) was synthesized with above molar ratios of monomers at 0 °C, respectively. The DSSCs devices were fabricated using the thiophene-based copolymers as sensitizers and their photovoltaic performances were measured by using a solar simulator under AM 1.5. In the DSSCs devices using polymeric sensitizers, V_oc is 0.53-0.60 V, J_sc is 1.9-4.5 mA/cm², FF is 0.51-0.63 and the power conversion efficiency is 0.63-1.53%, respectively.     

EXTRACTION, FRACTIONATION AND ACTIVITY CHARACTERISTICS OF PROTEASES FROM SHRIMP PROCESSING DISCARDS

Proteases recovered from Northern pink shrimp (NPS) and Southern rough shrimp (SS) processing discards (heads, shells, tails) were characterized. Shrimp processing discards were extracted with water following homogenization and centrifugation in order to obtain the crude extract which was subsequently fractionated with solid ammonium sulfate. Two fractions sedimenting with 30–50% (designated as NPS‐I and SS‐I), and 50–70% (designated as NPS‐II and SS‐II) ammonium sulfate were collected following centrifugation, respectively. Endoprotease activity of the crude extract was 0.02 U/mg for hemoglobin (Hb, pH 3.0), 0.16 U/mg for azocasein (Ac, pH 6.0) and 0.12 U/mg for benzoyl‐Arg‐β‐naphthylamide (BANA, pH 7.0). The exoprotease activity was 0.11–0.17 U/mg for Arg‐β‐naphthylamide (ArgNA, pH 7.0), 0.06–0.11 U/mg for Lys‐β‐naphthylamide (LysNA, pH 7.0) and 0.08–0.09 U/mg for Leu‐β‐naphthylamide (LeuNA, pH 7.0). Endoprotease activity increased 5–7.4 fold for NPS‐I and SS‐I, and 1.9–2.7 fold for NPS‐II and SS‐II against crude extract. Meanwhile, exoprotease activity increased 3.6–4.8 fold for NPS‐I and SS‐I, and 5.6–7.2 fold for NPS‐II and SS‐II. Meat treated with NPS‐I and SS‐I was tenderized more extensively than that treated with NPS‐II and SS‐II. The results of this study suggest that proteases recovered from shrimp processing discards may potentially be used as processing aids in formulated foods.     

Heat transfer characteristics of nanofluid through circular tube

Nano fluid is considered to be a class of high efficient heat transfer fluid created by dispersing some special solid nanoparticles (normally less than 100 nm) in traditional heat transfer fluid. The present experiment was conducted aiming at investigating the forced heat transfer characteristics of aqueous copper (Cu) nanofluid at varying concentration of Cu nano-particles in different flow regimes (300相似文献   

Development of high-accuracy image centroiding algorithm for CMOS-based digital sun sensors

A digital sun sensor calculates the incident sunlight angle using the sunlight image registered on a Complimentary Metal Oxide Semiconductor (CMOS) image sensor. In order to accomplish this, an exact center of the sunlight image has to be determined. Therefore, an accurate estimate of the centroid is the most important factor in digital sun sensor development. The most general method for determining the centroid is the thresholding method, and this method is also the simplest and easy to implement. Another centering algorithm often used is the image filtering method that utilizes image processing. The sun sensor accuracy using these methods, however, is quite susceptible to noise in the detected sunlight intensity. This is especially true in the thresholding method where the accuracy changes according to the threshold level. In this paper, a template method that uses the sunlight image model to determine the centroid of the sunlight image is suggested, and the performance has been compared and analyzed. The template method suggested, unlike the thresholding and image filtering method, has comparatively higher accuracy. In addition, it has the advantage of having consistent level of accuracy regardless of the noise level, which results in a higher reliability.