杂多酸(盐)催化新型香料草莓酯的合成

采用硅钨酸铝作催化剂 ,以乙酰乙酸乙酯和 1 ,2 丙二醇为原料合成草莓酯。优化的反应条件为 :0 2mol乙酰乙酸乙酯 ,0 2mol1 ,2 丙二醇 ,40ml环己烷 ,0 3 g硅钨酸铝 ,反应 3 5h ,草莓酯收率达 81 6%。产物经理化检验和红外光谱确证     

智能卡COS的快速烧写技术研究与实现

对智能卡COS现有USB、串口读写器的烧写技术进行了研究与分析,提出了一种以ARM处理器为母片硬件平台,通过智能卡接口对其他智能卡COS进行快速烧写的片拷贝方法。该方法具有硬件设计简单、烧写速度快,稳定性、安全性高等优点,且易于扩展为批量智能卡COS烧写器平台。目前该技术已在贴片智能卡生产厂商得以全面应用,大大提高了COS的烧写效率,具有较好的应用前景。     

Microstructure and mechanical properties of AZ31 alloy ingot fabricated by semi-continuous casting

The AZ31 alloy ingot with diameter of 110 mm and length of 3500 mm was fabricated successfully. The compositions and microstructure morphologies of the ingot at different locations were performed, which indicated that the chemical composition distributed homogeneously through the whole alloy ingot and the average grain size increased from the surface to the center. The results of the EDS and element face-scanning illustrated that the eutectic compounds mainly consisted of fl-Mg17Al12 and a small amount of fl-Mgl7（AlZn）12. Furthermore, slight improvements of the strength and ductility were observed from the center to the surface along the axial direction of the alloy ingot, while both the strength and elongation to failure of the samples along the radial direction are higher than that along the axial direction. The fine grain strengthening was the main contributors to the strength of the as-casted AZ31 alloy.     

现行热处理和相关的国家及行业标准

本文较全面地收集了现行的热处理和相关的国家及行业标准 ,将按 (一 )热处理技术条件和工艺、(二 )金相检验标准、(三 )性能测试和质量检验标准、(四 )材料标准、(五 )设备和工艺材料、(六 )环保和安全等几方面分期刊登     

Microstructure characterization of reinforcements in in-situ synthesized composites of Al-Zr-O system

A novel in-situ reaction system Al-Zr-O was developed. In-situ Al3Zr and Al2O3 particulates reinforced aluminum matrix composites were fabricated by the direct melt reaction technique in the Al-Zr-O system. Microstructures of the composites and crystal morphology of in-situ formed Al3Zr and Al2O3 particulates were analyzed by scanning electron microscope (SEM) and transmission electron microscope (TEM). Results indicate that in-situ formed Al3 Zr and Al2O3 particles are finer and well distributed in aluminum matrix. Al3Zr particulates with a tetragonal structure are mainly in the shape of polyhedron. A few of them are in the form of rectangle. The length/width ratio of the rectangular Al3Zr is less than 2.0 and the maximum size is 2μm. In addition, a certain number of Al2O3 submicro particles with a hexagonal structure are also generated in this system. Furthermore, it is found that Al3Zr crystal grows by the mechanism of twinning. The twin plane is (114). The twinning direction is [221]. The tensile tests show that the composites synthesized in the Al-Zr-O system exhibits high strength and ductility. There are a lot of ripples with fine particles on the fracture. The principal strengthening mechanisms for (Al3Zr Al2O3 )p/Al composites may include Orowan strengthening, grain-refining strengthening, solid-solution strengthening and dislocation strengthening.     

板料拉深成形过程中的变压边力技术

压边力是板料成形过程中的重要参数之一。在概述压边力在生产中的主要用途和意义的基础上，从压边力的加载模式、理论模型、实验研究变压边力技术与拉延筋、人工智能技术的交叉应用等方面，比较全面的综述了压边力技术的研究现状及存在问题，并探讨压边力技术的研究方向。     

限动芯棒连轧管机芯棒直径系列的设计方法

分析了通过调节辊缝获得期望的平均壁厚时钢管的横断面特性与辊缝调整量之间的关系，并由此推导出给定壁厚范围时满足某一附加公差率的芯棒直径计算公式。最后结合某西180mm连轧管机组提供的壁厚和芯棒直径系列，对芯棒直径系列的设计和选用方法进行了探讨。     

表面处理对球墨铸铁接触疲劳性能的影响

本文研究了激光微熔处理和高频感应加热淬火对球墨铸铁表面组织、接触疲劳强度和接触疲劳破坏过程的影响。结果表明,激光处理和高频淬火均可提高球铁的接触疲劳强度,但其接触疲劳破坏过程和形式却不同,前者是由于硬化层与基体间裂纹扩展造成大块深层剥落,后者则是表层裂纹在油楔作用下造成小块浅层脱落。     

板料多道次拉深成形规律和性能的研究

在物理模拟的基础上，研究了板料拉深成形过程中，材料的性能参数和工艺参数对板料成形性能的影响，着重分析了对多道次拉深成形的影响。结果表明，无论是材料性能参数还是材料的工艺参数都对再拉深的影响比对单道次拉深的影响林大得多，但两种参数对多道次拉深的影响过程前后是一致的。同时可以看出，多道次拉深之间是相互影响的，不能割裂开来考虑。     

提高机械专业学生应用计算机的能力

提高机械专业学生应用计算机的能力中南工业大学罗家美，王琴一、用系统的观点组织教学机械类专业计算机课程教学的目标是培养学生掌握最基本的科学计算能力、运用计算机技术进行机械辅助设计能力和进行科学管理的能力，在内容多、学时少的教学矛盾中，如何进行教学改革是...