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11.
Microfabricated preconcentrator-focuser for a microscale gas chromatograph   总被引:1,自引:0,他引:1  
The design, fabrication, and testing of a preconcentrator-focuser (PCF), consisting of a thick micromachined Si heater packed with a small quantity of a granular adsorbent material are described. The PCF is developed to capture and concentrate vapors for subsequent focused thermal desorption and analysis in a micro gas chromatograph. The microheater contains an array of high-aspect-ratio, etched-Si heating elements, 520 /spl mu/m (h)/spl times/50 /spl mu/m (w)/spl times/3000 /spl mu/m (l), bounded by an annulus of Si and thermally isolated from the remaining substrate by an air gap. This structure is sandwiched between Pyrex glass plates with inlet/outlet ports that accept capillary tubes for sample flow and is sealed by anodic bonding (bottom) and rapidly annealed glass/metal/Si solder bonding (top). The large microheater surface area allows for high adsorption capacity and efficient, uniform thermal desorption of vapors captured on the adsorbent within the structure. The adsorbent consists of roughly spherical granules, /spl sim/200 /spl mu/m in diameter, of a high-surface-area, graphitized carbon. Key design considerations, fabrication technologies, and results of performance tests are presented with an emphasis on the thermal desorption characteristics of several representative volatile organic compounds as a function of volumetric flow rates and heating rates. Preconcentration factors as high as 5600 and desorbed peak widths as narrow as 0.8 s are achieved from 0.25-L samples of benzene at modest heating rates. The effects of operating variables on sensitivity, chromatographic resolution, and detection limits are assessed. Testing of this PCF with a micromachined separation column and integrated sensor array is discussed briefly.  相似文献   
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本文介绍了一个基于微机的X射线分析自动测量系统。该系统有三个基本功能:自动获取数据、自动换样和处理谱数据。  相似文献   
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本文介绍了模糊技术的发展和现状,以及在相关领域中的应用情况,并且讨论了模糊技术在我国的产业化方向等问题。  相似文献   
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Identifying the key factors of the disaster-related information propagation process can provide decision support for disaster management. This study characterizes the effects of content types, location, and social capital of social media users on the virality of disaster-related information. We found through the Weibo dataset of the Yiliang earthquake that the virality of different types of information can vary on the basis of the social capital of users who post the information. This study fills the current research gaps by examining the individual and joint effects of the content and creator characteristics on the virality of disaster-related information.  相似文献   
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Li  Hongjian  Wei  Yaojun  Xiong  Yu  Ma  Enjie  Tian  Wenhong 《The Journal of supercomputing》2021,77(10):11575-11596
The Journal of Supercomputing - With the fast growth of big data applications, it has brought about a huge increase in the energy consumption for big data processing in Cloud data centers. In this...  相似文献   
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The magnesium (Mg) alloy low-pressure expendable pattern casting (EPC) process is a newly developed casting technique combining the advantages of both EPC and low-pressure casting. In this article, metal filling and the effect of the flow quantity of inert gas on the filling rate in the low-pressure EPC process are investigated. The results showed that the molten Mg alloy filled the mold cavity with a convex front laminar flow and the metal-filling rate increased significantly with increasing flow quantity when flow quantity was below a critical value. However, once the flow quantity exceeded a critical value, the filling rate increased slightly. The influence of the flow quantity of inert gas on melt-filling rate reveals that the mold fill is controlled by flow quantity for a lower filling rate, and, subsequently, controlled by the evaporation of polystyrene and the evaporation products for higher metal velocity. Meanwhile, the experimental results showed that the melt-filling rate significantly affected the flow profile, and the filling procedure for the Mg alloy in the low-pressure EPC process. A slower melt-filling rate could lead to misrun defects, whereas a higher filling rate results in folds, blisters, and porosity. The optimized filling rate with Mg alloy casting is 140 to 170 mm/s in low-pressure EPC.  相似文献   
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金怡果  田艳丽 《机床与液压》2002,(3):131-132,31
本文介绍利用Visual Basic工具开发金属切削机床主传动非常规变速系统的设计总体结构,功能和方法,以重复转速的传动系统为例,重点介绍转速图的拟定过程,本系统具有界面美观,操作方便,易于理解的特点。  相似文献   
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