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961.
Various nitroaromatics are successfully reduced to amines with 100% conversion and selectivity in methanol at low temperature (≈5 °C), by using versatile system of 5% Ni–SiO2 catalyst and NaBH4 and in situ generation of Ni boride. The catalytic efficiency of Ni loading (5%, 10% and 15%) with silica or titania as support materials is investigated for reduction of nitrobenzene. The Ni–titania/NaBH4 system recorded lower conversion and selectivity. The IR studies indicate that silica support does not have free –OH group on its surface. Thus the nickel boride is anchored to the silica to facilitate the catalytic process. 相似文献
962.
963.
P. M. Solozhenkin E. A. Deliyanni V. N. Bakoyannakis A. I. Zouboulis K. A. Matis 《Journal of Mining Science》2003,39(3):287-296
The original method is developed for producing the new inorganic sorption material of akaganeite bgr-FeO(OH). The material in question is characterized relative to arsenic contained in aqua. The possibility is established for removing arsenate ions from water by contemporary physicochemical methods. 相似文献
964.
The results of computer simulations demonstrate the possibility of light energy transmission through band gaps of a one-dimensional photonic crystal with fluctuating lengths of individual layers. In the case of weak (±5%) fluctuations, the light pulse energy partly penetrates in depth a photonic crystal. If fluctuations of the layer length are strong (±20%), the light pulse energy can be partly transmitted through the crystal. 相似文献
965.
966.
Matthias Zobel Joachim Denzler Benno Heigl Elmar Nöth Dietrich Paulus Jochen Schmidt Georg Stemmer 《Machine Vision and Applications》2003,14(1):26-34
Abstract. This contribution introduces MOBSY, a fully integrated, autonomous mobile service robot system. It acts as an automatic dialogue-based
receptionist for visitors to our institute. MOBSY incorporates many techniques from different research areas into one working
stand-alone system. The techniques involved range from computer vision over speech understanding to classical robotics.
Along with the two main aspects of vision and speech, we also focus on the integration aspect, both on the methodological
and on the technical level. We describe the task and the techniques involved. Finally, we discuss the experiences that we
gained with MOBSY during a live performance at our institute. 相似文献
967.
The discrimination problem for two normal populations with the same covariance matrix when additional information on the population is available is considered. A study of the robustness properties against training sample contamination of classification rules that incorporate this additional information is performed. These rules have received recently attention where their total misclassification probability (TMP) is proved to be lower than Fisher's linear discriminant rule. The results of a simulation study on the TMP which compares the behaviour of the new rules against Fisher's rule and some of its robustified versions under different types of contamination are presented. These results show that the rules that incorporate the additional information not only have lower TMP, but they also prevent against some types of contamination. In order to achieve prevention from all types of contamination a robustifed version of these rules is recommended. 相似文献
968.
This paper presents the mass transfer results from an impinging liquid jet to a rotating disk. The mass transfer coefficients were measured using the electrochemical limiting diffusion current technique (ELDCT). Rotational Reynolds number (Rer) in the range of 3.4 × 104–1.2 × 105, jet Reynolds number (Rej) 1.7 × 104–5.3 × 104 and non-dimensional jet-to-disk spacing (H/d) 2–8 were taken into consideration as parameters. It was found that the jet impingement resulted in a substantial enhancement in the mass transfer compared to the case of the rotating disk without jet. 相似文献
969.
970.
During experiments on the MSL-1 (first microgravity science laboratory) mission of the space shuttle (STS-83 and STS-94, April
and July 1997), a droplet of palladium-silicon alloy was electromagnetically levitated for viscosity measurements. For the
nondeforming droplet, the resultant magnetohydrodynamic (MHD) flow inside the drop can be inferred from motion of impurity
particulates on the surface. In the experiments, subsequent to melting, Joule heating produces a continuous reduction of viscosity
of the fluid resulting in an acceleration of the flow with time. These observations indicate formation of a pair of co-rotating
toroidal flow structures inside the spheroidal drop that undergo flow instabilities. As the fluid temperature rises, the amplitude
of the secondary flow increases, and beyond a point, the tracers exhibit noncoherent chaotic motion signifying emergence of
turbulence inside the drop. Assuming that the observed laminar-turbulent transition is shear-layer type, the internal structure
of the toroidal loops is used to develop a semiempirical correlation for the onset of turbulence. Our calculations indicate
that the suggested correlation is in modest agreement with the experimental data, with the transition occurring at a Reynolds
number of 600. 相似文献