Extraction and purification of penicillin G from fermentation broth by water-compatible molecularly imprinted polymers

Highly selective molecularly imprinted polymer (MIP) was synthesized by using methacrylic acid as functional monomer, trimethylolpropane trimethacrylate as cross-linker, chloroform as porogen and penicillin G potassium as template molecule. These imprinted polymers were used as solid-phase extraction sorbent for the selective extraction of penicillin G from the fermentation broth samples. Various parameters affecting the extraction efficiency of the MIP particles such as; effects of pH, wash and eluent solutions were evaluated. Molecular recognition properties and selectivity of these MIPs were estimated and the obtained results revealed high affinity for the target antibiotic. Equilibrium binding experiments were done to assess the performance of the MIP relative to non imprinted polymer (NIP). After optimizing the extraction parameters in molecularly imprinted solid-phase extraction (MISPE), successful imprinting was confirmed by comparison of the recoveries from the fermentation broth, ranging between 24–26% (RSD 4.1–4.5%, n = 4) for the NIPs and 83–88% (RSD 3.1–3.4%, n = 4) for the MIPs.     

A novel imperialist competitive algorithm for bi-criteria scheduling of the assembly flowshop problem

This paper deals with the two-stage assembly flowshop scheduling problem with minimisation of weighted sum of makespan and mean completion time as the objective. The problem is NP-hard, hence we proposed a meta-heuristic named imperialist competitive algorithm (ICA) to solve it. Since appropriate design of the parameters has a significant impact on the algorithm efficiency, we calibrate the parameters of this algorithm using the Taguchi method. In comparison with the best algorithm proposed previously, the ICA indicates an improvement. The results have been confirmed statistically.     

Vulnerability assessment of irregular steel structures under traveling fires

This paper investigates the response of tall setback irregular steel moment resisting structures under traveling fires. A seven‐story steel regular structure (RS) is first designed for gravity and seismic loads and then it is fireproofed for a fire resistance rating (FRR) of 120 min based on the ISO834 fire. Some architectural changes are then imposed on the RS to make it a setback irregular structure (SBS). Based on the traveling fire methodology, both structures are then subjected to fire curves ranging from 1% to 100% for the fire load density (q_f) of 570 MJ/m². As in the SBS, the distribution of gravity loads is not uniform; the structural fire analyses are performed twice: when the fires start from left to right and then vice versa. The results show the FRR of the RS is minimized under the fire size of 22% with the collapse time of 87.0 min. In the SBS, when the fires start from left to right and then from right to left, the FRR is minimized under the fire size of 20% with the collapse times of 75.0 and 79.0 min, respectively. This shows that the SBS is more vulnerable toward traveling fires than the RS. In order to monitor the role of q_f in the FRRs of the structures, q_f is then reduced, and the required analyses are repeated. This process continues to where no collapse is observed under all the fire sizes. The results indicate that the RS would remain stable if the q_f is decreased to 480 MJ/m², implying that a 16% increase should be considered to the required FRR. As for the SBS, the q_f should be decreased to 440 MJ/m² to make it stable, meaning that a 25% increase should be considered to the required FRR.     

Opportunistic Relaying for MIMO Amplify-and-Forward Cooperative Networks

We consider a wireless relay network with multiple antenna terminals over Rayleigh fading channels, and apply distributed space-time coding (DSTC) in amplify-and-forward (A&F) mode. The A&F scheme is used in a way that each relay transmits a scaled version of the linear combination of the received symbols. It turns out that, combined with power allocation in the relays, A&F DSTC results in an opportunistic relaying scheme, in which only the best relay is selected to retransmit the source’s space-time coded signal. Furthermore, assuming the knowledge of source-relay CSI at the source node, we design an efficient power allocation which outperforms uniform power allocation across the source antennas. Next, assuming M-PSK or M-QAM modulations, we analyze the performance of the proposed cooperative diversity transmission schemes in a wireless relay networks with the multiple-antenna source and destination. We derive the probability density function (PDF) of the received SNR at the destination. Then, the PDF is used to determine the symbol error rate (SER) in Rayleigh fading channels. We derived closed-form approximations of the average SER in the high SNR scenario, from which we find the diversity order of system R min{N _s , N _d }, where R, N _s , and N _d are the number of the relays, source antennas, and destination antennas, respectively. Simulation results show that the proposed system obtain more than 6 dB gain in SNR over A&F MIMO DSTC for BER 10^?4, when R = 2, N _s  = 2, and N _d  = 1.     

Comparison of energy conservation building codes of Iran,Turkey, Germany,China, ISO 9164 and EN 832

To improve the energy efficiency of buildings via compliance to regulation in Iran, Code No. 19 was devised in 1991. The code lacks high level aims and objectives, addressing the characteristics of Iranian buildings. As a consequence, the code has been revised and is not completely implemented in practice, and still remains inefficient. As with any energy coding system, this code has to identify the right balance between the different energy variables for the Iranian climate and way of life. In order to assist improvements to high level objectives of Code 19, this code is compared with ISO 9164, EN 832, German regulation, TS 825 of Turkey and China’s GB 50189 to understand how these have adapted international standards to national features. In order to test the appropriateness of Code 19, five case study buildings in Iran are assessed against Code 19 as well as Turkish standard TS 825 and the results are compared. The results demonstrate that Code 19 is efficient in calculations of building envelope, but it needs improvements in the areas of ventilation, gains from internal and solar sources. The paper concludes by offering suggestions for improving the code.     

Inspection and Monitoring of Concrete Structures via Radiography and Weighted Nuclear Norm Minimization Method

Russian Journal of Nondestructive Testing - The location of reinforcement bar in concrete, the bar corrosion, diameter and the depth below the surface are important factors in the evaluation of the...     

Outage performance of downlink communications in cognitive-based two-tier networks: cooperative and non-cooperative femtocells

Femtocell deployment, which is a promising approach to the coverage and capacity improvement of indoor communications, suffers from cross-tier interference. Therefore to make the femtocell technology practical this issue needs to be addressed appropriately. One serious type of cross-tier interference occurs in downlink communication, in which a macrocell user is located far from its macro base station. In this setup, the communication of the adjacent femto access points with their users makes the macrocell user experience a low SINR. This paper considers this scenario and shows how cognitive-enabled femto access points can cope with cross-tier interference. More precisely, we compute the outage probability of macro users in a two-tier network when femto access points use the energy detection-based spectrum sensing technique to find the unoccupied frequency subband. To improve the outage probability of macro users, we also study the effectiveness of cooperation among neighbor femto access points. In all cases, the analytical expressions are validated by computer simulations which confirm the accuracy of the used approximations.

     

ElmNet: a benchmark dataset for generating headlines from Persian papers

Multimedia Tools and Applications - Headline generation is a challenging subtask of abstractive text summarization, which its output should be a summary, shorter than one sentence. It would be...