Thermophysical parameters for the combustion products from tetrazole-sodium tetrazolate mixtures

Measurements have been made on the thermal conductivity and specific heat of the powder product from quenching in nitrogen applied to the gas-liquid flame formed by the combustion of a tetrazole-sodium tetrazolate mixture in weight proportion 31. The thermal conductivity on the whole is a nonmonotone function of temperature in the range 100–450 K and has some local turning points associated with the multicomponent structure and the phase transitions associated with chemical and structural transformations.Translated from Inzhenrno-fizicheskii Zhurnal, Vol. 61, No. 3, pp. 422–426, September, 1991.     

Complete structure of glycopeptides isolated from IgG immunoglobulins of cow colostrum

Bovine immunoglobulins (IgG1 type) have been isolated from colostral whey. Hydrolysis by pronase, trypsin and (or) chymotrypsin yield several glycopeptides structural studies of which lead to the following results. 1. IgG1 colostral immunoglobulins possess two glycan moieties which are linked to the peptidic chain by an N-(beta-aspartyl)-N-acetylglucosaminylamine bound. 2. The peptidic sequence around the linkage region has been determined by classical methods and is as follows: Thr-Lys-Pro-Arg-Glu-Glu-Gln-Phe-Asn(Glycan)-Ser-Thr-Tyr-Arg. 3. The following procedures: partial acidic hydrolysis, periodic oxidation, hydrazinolysis-nitrous deamination, methylation and use of specific glycosidases allowed us to determine the structure of the glycan moieties which fit with the general following scheme: (see article) Thus they could be related to the general glycan structure so-called of "N-acetyllactosamine type" because they possess the pentasaccharidic core common to numerous glycoproteins Man alpha 1 leads to [Man alpha 1 leads to 6] Man beta 1 leads to 4 GlcNAc beta 1 leads to 4 GlcNAc beta 1 leads to Asn on which are conjugated 2 N-acetyllactosamine residues. Besides they present a microheterogeneity which is due to the varying number of additional N-acetylneuraminic acid and fucose residues. 4. These structures are compared to various immunoglobulin structures proposed by others: bovine serum IgG and human serum IgG, IgE and IgA.     

Meshless local Petrov-Galerkin method for continuously nonhomogeneous linear viscoelastic solids

A meshless method based on the local Petrov-Galerkin approach is proposed for the solution of quasi-static and transient dynamic problems in two-dimensional (2-D) nonhomogeneous linear viscoelastic media. A unit step function is used as the test functions in the local weak form. It is leading to local boundary integral equations (LBIEs) involving only a domain-integral in the case of transient dynamic problems. The correspondence principle is applied to such nonhomogeneous linear viscoelastic solids where relaxation moduli are separable in space and time variables. Then, the LBIEs are formulated for the Laplace-transformed viscoelastic problem. The analyzed domain is covered by small subdomains with a simple geometry such as circles in 2-D problems. The moving least squares (MLS) method is used for approximation of physical quantities in LBIEs.     

PEO／V2O5纳米复合薄膜的变色特性研究

为改善V2O5薄膜的电致变色性能，采用溶胶-凝胶法将具有高离子电导率并具有水溶性的聚环氧乙烷（PEO）直接嵌入V2O5层间，制备了PEO／V2O5纳米复合薄膜。采用标准三电极法从0．5mol／L LiClO4的PC电解质溶液向PEO／V2O5纳米复合薄膜注入锂离子，测量了纳米复合薄膜在注入不同数量锂离子时的可见光透射光谱以及对应的颜色变化，并运用循环伏安法测试其电化学性能。实验结果表明，PEO／V2O5纳米复合薄膜的循环伏安图出现了2对氧化还原峰，并且具有稳定的循环可逆性。随着应用电压的不同，薄膜呈现黄色、绿色和蓝色的多色可逆变化。PEO／V2O5纳米复合薄膜的电化学稳定性和机械性能都优于V2O5干凝胶薄膜，可以作为电致变色材料得到应用。X射线光电子能谱（XPS）成分分析表明PEO／V2O5纳米复合薄膜的电致变色效应与V、O的化合价和化学环境密切相关。     

A sequential method of calibrating measurement instruments with a Kalman filter

A recurrent algorithm is derived for estimating the parameters of a calibration curve with allowance for the errors in reproducing the inputs. That algorithm is combined with a proposed rule for halting the calibration to reduce considerably the length of the calibration, which promises a real economic advantage. __________ Translated from Izmeritel’naya Tekhnika, No. 4, pp. 32–38, April, 2006.     

Clock Recovery at 160 Gb/s and Beyond, Using a Fiber-Based Optical Power Limiter

We propose a simple all-optical clock recovery technique for short data packets at 160 Gb/s, and beyond, which is based on the concept of using a Fabry-Peacuterot filter (FPF). The novel feature of the technique is the use of a highly nonlinear fiber followed by an optical bandpass filter, centered at the initial carrier wavelength, which acts as an ultrafast power limiter, removing drastically the amplitude modulation of the FPF's output and providing the clock signal     

Development of a Net Shape Manufacturing Method for Ventilated Brake Discs in Single Piece Design

Carbon fibre reinforced ceramic matrix composites (CMC), originally developed for lightweight heat shields of spacecraft, are used for high performance brake discs in sports cars from different manufacturers. In contrast to the CMC materials for space applications, based on woven fabrics and costly manufacturing methods, these low cost friction materials are produced by liquid silicon infiltration of porous Carbon/Carbon (C/C) preforms, based on short fibre reinforced CFRP green bodies manufactured via warm press technique. In this work, different manufacturing methods for ventilated CMC brake discs are compared to each other, and the development of a new technology for the manufacture of single piece C/C‐SiC brake discs in net shape technique is presented.     

Mechanism of titanium sponge formation in the kroll reduction reactor

The Kroll process of magnesium reduction of titanium tetrachloride is used the world over the production of titanium metal in the form of sponge. Although the process has been in practice for the last five decades, there is no clear understanding of the reaction mechanism and sponge formation. The present study involved reduction experiments in a 2000 kg titanium sponge-capacity prototype reactor to develop a better understanding of TiCl₄ reduction of magnesium with respect to the process parameters. Experiments were also conducted in two smaller experimental reactors to study the temperature evolution during the process as a function of the TiCl₄ feed rate. Based on the results of all these experiments, a model has been proposed for the mechanism of sponge formation in the Kroll process.     

String-matching with OBDDs

Ordered binary decision diagrams (OBDDs) are a very popular graph representation for Boolean functions. They can be viewed as finite automata recognizing sets of strings of a fixed length, where the letters of the input strings are read at most once in a predefined ordering. The string matching problem with string w as pattern, consists of determining, given an input string, whether or not it contains w as substring. We show that for a fraction of orderings tending to 1 when n increases arbitrarily, the minimal size of an OBDD solving the string matching problem for strings of length n has a growth which is an exponential in n.     

Influence of compression aging on phase transition temperatures in single crystalline Ni‐rich NiTi shape memory alloys

The present paper considers the phase transition behavior of a single crystal Ni‐rich NiTi alloy which was compression aged to produce one single family of Ni₄Ti₃ precipitates. The single crystal material was produced in a two stage process. Polycrystalline material was first melted under an inert atmosphere and remelted when single crystals were produced. Compression aging treatments in <111>‐orientation were carried out in order to suppress all but one family of Ni₄Ti₃‐precipitates which nucleate and grow on {111}‐planes of the B2 matrix. The objective of this study is to investigate the influence of Ni₄Ti₃‐precipitates on the martensitic transformation behavior. It was previously shown that grain boundaries provide heterogeneous nucleation sites for the formation of Ni₄Ti₃; this results in heterogeneous microstructures which undergo multiple step martensitic transformations. Single crystals avoid grain boundaries and the present study aims at clarifying how homogeneously precipitated particles affect martensitic transformations.