固载于SBA-15分子筛中的同双核金属配合物催化剂

合成了3种同双核金属配合物[M2LCl3]Cl(L代表配体三亚乙基四胺,M代表Co,Cu,Cr),采用微波加热法合成了SBA-15分子筛,采用浸渍法将3种同双核金属配合物分别固载在表面官能化的SBA-15分子筛(SBA-15-NH2分子筛)中制得负载型催化剂。傅里叶变换红外光谱、X射线衍射、紫外可见光谱和热分析表征结果表明,同双核金属配合物被固载后,其结构仍保持完整。以环己烷氧化反应为探针反应,考察了[Co2LCl3]Cl/SBA-15-NH2,[Cu2LCl3]Cl/SBA-15-NH2,[Cr2LCl3]Cl/SBA-15-NH2催化剂的活性,环己烷转化率分别为11.0%,49.5%,57.9%;对于[Cr2LCl3]Cl/SBA-15-NH2催化剂,当分别以乙睛、丙酮和冰醋酸为溶剂时,环己烷转化率分别为57.9%,52.1%,34.2%,3次重复实验的环己烷转化率分别为57.9%,47.8%,46.5%,表明该催化剂具有较好的活性和重复使用性。     

Study of Density Behavior During LHCD and IBW Heating in the HT-7 Superconducting Tokamak

A new method using special shape parameters has been introduced to study density behavior with synergy of lower hybrid current drive (LHCD) and ion Bernstein wave (IBW) heating in the HT-7 superconducting tokamak. During the synergy of the LHCD and IBW heating an improved confinement plasma was achieved, and the electron density was increased and peaked.     

CAPP系统中工艺卡片生成过程的研究

以AutoCAD2 0 0 0为开发平台、VC + + 6 0为开发环境、ObjectARX2 0 0 0为开发工具、SQLServer为后台数据库 ,通过编写writeText、fillGykztb、fillGykjtb等自定义函数 ,生成工艺卡片 ,并实现工序内容在工艺卡片中的分页显示等功能。     

The integral representations of solutions for circular plate problems without any hold

In this article, the following results are obtained: (1) a special solution and a general solution (non-series form) for circular plate problems are given; (2) integral representations of solutions for circular plate problems without any hold with built-in edge conditions and simply supported edge conditions are found.     

新型光电混合式电流互感器设计

设计了一种光电混合式电流互感器,它由传感头、光纤传输和光电转换器、信号处理电路和工作电源4部分组成。这种结构具有绝缘性能高、可靠性强、质量小等特点,并对误差情况进行了分析。     

Efficient fine granularity scalability using adaptive leaky factor

Fine Granularity Scalability (FGS) video coding has been adopted by the MPEG-4 standard for video streaming applications. In this paper, we propose a novel FGS coding scheme, which applied adaptive leaky factors for the enhancement layer prediction to further improve the coding efficiency of FGS. A flexible method that can dynamically determine the leaky factors according to the network conditions is also presented. With the proposed method, a better trade-off between the coding efficiency and drifting reduction can be achieved, and the coding performance is further improved compared with using a fixed leaky factor. Experimental results show that the proposed method can further improve the coding efficiency over a wide range of bitrate and packet loss ratio, and still keep the original characteristics, such as fine granularity, and bandwidth adaptation.     

岩性圈闭储层描述技术及应用

本文以高分辨率地震资料为基础，应用测井、钻井等资料，从沉积微相分析入手，建立了以河道砂体、河口坝砂体为主的地质及地震响应模型，并根据地震反射波组特征、地震反演的阻抗值及其他地震属性参数，确定了研究区的砂体变化及其分布规律，总结出一套针对薄互层特点的岩性圈闭识别技术。本文方法在大庆长垣以西古龙和他拉哈西地区的实际应用中取得了明显的效果。     

降低汽油烯烃含量裂化催化剂LBO-12的研制与开发

探讨了催化裂化过程降低汽油烯烃的反应原理，研究了催化剂各组分对裂化汽油性质影响的规律性，围绕提高氢转移活性，提出制备降烯烃裂化催化剂的技术路线，并研制开发了新型LBO-12降烯烃催化剂，固定流化床反应器对中试样品的评价和工业应用结果表明，该催化剂在不损失汽油辛烷值的前提下，降低催化裂化汽油烯烃能力较强，并具有较高的水热活性稳定性和良好的抗重金属污染特性。     

AOI技术在激光微孔产品检查中的应用

在过去几年里,小型PCB诸如硅芯片级以及便携式移动电话的生产者和设计者们已经发现:如果要保持自己的竞争力并具备生产高密度封装板能力,就必须采用微孔技术。微孔技术的出现要求针对微孔缺陷的有效检测手段对工艺进行过程控制。本文对激光微孔的自动光学检测进行了详细介绍。