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971.
The extraction of Te(IV) from aqueous solutions containing various ligands was studied using various inert organic diluents
and other solvents. The extraction was carried out from solutions of various mineral (HCl, HBr, HI, HNO3) and organic (citric, oxalic) acids of various concentrations. The organic phase was an inert diluent (cyclohexane, CCl4, chloroform, benzene, p-xylene, toluene, nitrobenzene) or a solution of 20 vol % Aliquat-336, 20 vol % trioctylamine, or 30 vol % TBP in p-xylene. A correlation between the distribution of Te(IV) and some physicochemical properties of the diluents and the possibility
of extraction separation radioactive Te isotopes and their daughters, i.e., radioactive I isotopes, were examined. In most
cases, the Te(IV) distribution ratio decreases in the order nitrobenzene > CHCl3 > CCl4 > p-xylene > benzene > toluene > cyclohexane.
Published in Russian in Radiokhimiya, 2007, Vol. 49, No. 4, pp. 353–358.
The text was submitted by the authors in English.
An erratum to this article is available at . 相似文献
972.
Transglutaminase (TGase) was separated from the culture broth of an isolated strain of Streptoverticillium mobaraense. The crude enzyme was prepared by centrifugation, ultrafiltration, precipitation by alcohol, centrifugation and freeze‐drying. The yield after these processes was 65–70%. Then the enzyme was purified to homogeneity by chromatography on CM‐cellulose and Sephadex G‐75 on which the yields were about 70% and 80%, respectively; the purified folds reached 2.5–4.7 and 1.08–2.06, respectively. The molecular weight of this TGase was 39,500–40,100 Da by gel filtration chromatography. Optimum enzyme activity was observed in the pH range of 5.0–7.0, and it was maintained stable at 20–40C. The optimal temperature and pH was 52C and 6.0, respectively. At 1 mM and 5 mM metal ion or inhibitors concentration, TGase activity was strongly inhibited by Zn2+ and NEM, and not affected obviously by Ba2+, Ca2+, Co2+, Cu2+, Fe2+, Fe3+, Mg2+, Mn2+, Na+ as well as PMSF and EDTA. The effects of these additions on this TGase were compared with those of other microbial TGases. 相似文献
973.
S. C. Hogg H. V. Atkinson P. Kapranos 《Metallurgical and Materials Transactions A》2004,35(3):899-910
The rheology of Al-30Si-5Cu and Al-30Si-5Cu-2Mg spray-formed alloys has been characterized after holding at various times
and temperatures, using semisolid rapid compression to obtain load-displacement curves. Microstructures were examined after
partial remelting and compression in an attempt to understand the flow behavior. The initial resistance to flow generally
increased with holding time at temperature. This increase was attributed to the increased strength of a three-dimensional
(3-D) solid silicon network present in these alloys in the semisolid state, with the initial resistance to flow smaller in
the magnesium-containing alloys. With increased temperature, the initial resistance decreased due to increased liquid content
and grain spheroidization. The viscosity vs shear rate response was studied using the approach of Laxmanan and Flemings. The materials shear thinned rapidly during the
test conditions, in which the shear rate rapidly increased from approximately 2.5 to 92 s−1. The results were fitted to a power-law model, and the viscosities showed a drop of approximately two to four orders of magnitude
when extrapolated to a shear rate of 1000 s−1 (a typical value in actual component manufacture). The rapid compression test, which is close to conditions present in component
manufacture, was shown to have more in common with a shear rate jump experiment, rather than steady-state viscometry. 相似文献
974.
Finite sample properties of estimators of spatial autoregressive models with autoregressive disturbances 总被引:1,自引:0,他引:1
The article investigates the finite sample properties of estimators for spatial autoregressive models where the disturbance
terms may follow a spatial autoregressive process. In particular we investigate the finite sample behavior of the feasible
generalized spatial two-stage least squares (FGS2SLS) estimator introduced by Kelejian and Prucha (1998), the maximum likelihood
(ML) estimator, as well as that of several other estimators. We find that the FGS2SLS estimator is virtually as efficient
as the ML estimator. This is important because the ML estimator is computationally burdensome, and may even be forbidding
in large samples, while the FGS2SLS estimator remains computationally feasible in large samples.
Received: 20 January 2001 / Accepted: 31 August 2001 相似文献
975.
High crude oil prices and pollution problems have drawn attention to alternative vehicle technologies and fuels for the transportation sector. The question is: What are the benefits/costs of these technologies for society? To answer this question in a quantitative way, a web-based model (http://vehiclesandfuels.memebot.com) has been developed to calculate the societal life cycle costs, the consumer life cycle costs and the tax for different vehicle technologies. By comparing these costs it is possible to draw conclusions about the social benefit and the related tax structure. The model should help to guide decisions toward optimality, which refers to maximum social benefit. The model was applied to the case of Thailand. The life cycle cost of 13 different alternative vehicle technologies in Thailand have been calculated and the tax structure analyzed. 相似文献
976.
977.
978.
The basic physicochemical principles of preparation of emulsion fuel compositions based on heavy and extra-heavy crude cuts
were analyzed with consideration of the nature and content of the phases constituting the emulsion, type of chemical additives
— emulsifiers and stabilizers, and type of equipment for production of emulsion fuels.
__________
Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 5, pp. 51–56, September–October, 2007. 相似文献
979.
Martín A. Rodríguez Ricardo M. Carranza Raúl B. Rebak 《Metallurgical and Materials Transactions A》2005,36(5):1179-1185
Alloy 22 (N06022) is the current candidate alloy used to fabricate the external wall of the high-level nuclear waste containers
for the Yucca Mountain repository. It was of interest to study and compare the general and localized corrosion susceptibility
of Alloy 22 in fluoride and chloride solutions at 90 °C. Standard electrochemical tests such as cyclic potentiodynamic polarization,
amperometry, and electrochemical impedance spectroscopy were used. Studied variables included the solution pH and the alloy
microstructure (thermal aging). Results show that Alloy 22 is highly resistant to general corrosion in all the solutions tested.
Thermal aging is not detrimental and even seems to be slightly beneficial for general corrosion at the higher solution pHs.
Pitting corrosion was never observed. Crevice corrosion was found only for high chloride-containing solutions after anodic
polarization. The presence of fluoride ions together with chloride ions seems to increase the susceptibility of Alloy 22 to
crevice corrosion compared to pure chloride solutions.
This article is based on a presentation made in the symposium “Effect of Processing on Materials Properties for Nuclear Waste
Disposition,” November 10–11, 2003, at the TMS Fall meeting in Chicago, Illinois, under the joint auspices of the TMS Corrosion
and Environmental Effects and Nuclear Materials Committees. 相似文献
980.