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91.
Gomez-Vega JM Sugimura H Takai O Hozumi A 《Journal of materials science. Materials in medicine》2001,12(10-12):923-927
Ongoing research is reported aimed at preparing mesoporous silica coatings on various substrates for medical applications by a biomimetic approach (self-assembling of organic/inorganic sol-gel systems into ordered structures). Tetraethylorthosilicate (TEOS) was selected as the silica precursor, and amphiphilic triblock copolymers poly(ethylene oxide)-poly(propylene oxide)-poly(ethylene oxide), and the cationic surfactant cetyltrimethyl ammonium chloride (CTAC), as structure-directing agents. The mesochannels diameter could be adjusted by changing the directing agent, and a preferred alignment of the mesostructure was observed independently of the used substrate (glass, silicon, Ti or Ti6Al4V). Three different treatments (thermocalcination, photocalcination, and solvent extraction) have been also studied to remove the organic templates, of which photocalcination showed to be the most versatile. When soaked in a simulated body fluid, mesoporous silica coatings induced apatite formation after seven days. 相似文献
92.
Electron microscopic in situ hybridization (EM-ISH) is a useful method in determining the localization of a specific nucleic acid at the ultrastructural level. Since the EM-ISH protocol includes many steps, no standard protocol for EM-ISH is available yet. In this study, we optimized quantitatively the critical conditions with respect to embedding resin, nucleic acid labeling and hybridization reaction time, by using adenovirus-infected cells as the indicator cells. The optimal detection of an adenovirus-specific nucleic acid was obtained by overnight hybridization reaction on sections embedded in Lowicryl K4M resin. Random-primed-labeled probes improved the reactivity. At least 60% of virus particles in paracrystalline arrays was found to contain viral DNA. These arrays in adenovirus-infected cells are useful in evaluating quantitatively the efficiency of protocols of EM-ISH. 相似文献
93.
Pore structure of porous ceramics synthesized from water-based slurry by freeze-dry process 总被引:6,自引:0,他引:6
A unique porous ceramic with complex pore structure was synthesized by the freeze-dry process. A water-based ceramic slurry was frozen while controlling the growth direction of ice, and sublimation of the ice were generated by drying it at a reduced pressure. By sintering this green body, a porous ceramic with complex pore structure was obtained, where macroscopically aligned open pores exceeding 10 m in size contained minute pores of about 0.1 m in their internal walls. Wide control of the porosity was possible by changing the concentration of the starting slurry. The pore size distribution as well as the microstructure were substantially affected by the freezing and sintering temperatures. Optimization of the synthesis conditions was investigated in order to obtain the desired pore structure. 相似文献
94.
95.
H. Goto 《International journal of control》2013,86(4):651-660
This research focuses on event varying discrete event systems with capacity and order constraints, and derives two state-space representations that stand for the earliest and latest times of event occurrences. Moreover, we consider rescheduling methods for these representations that can be applied even when the relevant parameters are changed after the commencement of the job. The two state-space representations derived have forms that are similar to dual systems in modern control theory. In online scheduling, it is often essential to keep track of state changes or the float times of jobs continuously. For the calculation of the float times, both earliest and latest times must be calculated. Hence, the derived representations are an attractive tool for solving online scheduling problems. 相似文献
96.
Shengfang Shi Sunghun Cho Tomoyo Goto Tohru Sekino 《Journal of the American Ceramic Society》2021,104(6):2753-2766
To further improve the mechanical performance and reduce the percolation threshold by controlling microstructures, Al2O3-TiC composites containing 0-20 vol% TiC were fabricated via in situ reaction synthesis. Graphite (ATC) and carbon nanotubes (ATCT) were used as carbon sources. The composites were also fabricated via a conventional process using a TiC starting powder (AT). X-ray diffraction analysis and scanning electron microscopy observation results indicated successful fabrication of the composites with various microstructures. TiC particles in ATCT were completely dispersed at grain boundaries, whereas in ATC and AT, these particles were either intragranular or intergranular dispersed. The composites could be listed as follows, ATCT > ATC > AT, that is, in descending order of the reinforcing flexural strength and fracture toughness. The nanoindentation measurement indicated the optimum hardening effect of ATCT. The ATCT composite also exhibited the highest fracture toughness, which was 49% higher than that of the monolithic Al2O3. Crack deflection was considered as the main toughening mechanism while crack bridging behavior also occurred in ATCT. For a given TiC content, ATCT exhibited the lowest electrical resistivity, owing mainly to the complete grain-boundary dispersion of the relatively large TiC particles. The similarity of the Al2O3 grain size and TiC particle size of ATCT contributed to the lowest percolation threshold achieved (11.2%), which (to date) is the lowest value that has been reported for the Al2O3-TiC system. 相似文献
97.
Bhupesh C. Roy Motonobu Goto Akio Kodama Tsutomu Hirose 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1996,67(1):21-26
Essential oils and cuticular waxes were extracted from peppermint leaves with supercritical carbon dioxide in a semicontinuous-flow extractor. The effects of CO2 flow rate and pressure on the extraction rate were studied within the flow rate range of (4·1–9·8) × 10−5 kg s−1 and the pressure range of 10–30 MPa. Flow rate effect indicated that the intraparticle diffusion resistance was not dominant in this process. The extraction rate of cuticular waxes increased remarkably with the pressure, whereas that of essential oils was almost constant as compared with cuticular waxes. The concentration of cuticular waxes at the exit of the extractor was close to the solubility of triacontane while that of essential oils was much lower than the solubility of 1-menthol. 相似文献
98.
Tomoko Okuyama Jun Shirakawa Kazuki Tajima Yoko Ino Heidrun Vethe Yu Togashi Mayu Kyohara Ryota Inoue Daisuke Miyashita Jinghe Li Nozomi Goto Taiga Ichikawa Shingo Yamasaki Haruka Ohnuma Rie Takayanagi Yayoi Kimura Hisashi Hirano Yasuo Terauchi 《International journal of molecular sciences》2020,21(21)
99.
A Phytol‐Enriched Diet Activates PPAR‐α in the Liver and Brown Adipose Tissue to Ameliorate Obesity‐Induced Metabolic Abnormalities 下载免费PDF全文
100.
The importance of concrete permeability is discussed relative to its effect on durability. Experimental studies were made of the effect of water/cement ratio and curing temperature on the porosity, pore size distribution and permeability of cement pastes. Although total porosities of samples cured at 60°C are smaller than in those cured at 27°C, the pore volume larger than 750Å radius is greater in the 60°C samples and is related to higher permeabilities also in the latter. 相似文献