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941.
Three series of polyurethane adhesives—polyethyleneadipateurethane (PEAU), polybuthyleneadipateurethane (PBAU), and polyhexyleneadipateurethane (PHAU)—with the same MW and hard/soft segment ratio, based on the three polyesters polyethyleneadipate (PEA), polybuthyleneadipate (PBA), polyhexyleneadipate (PHA), with 4,4′-diphnylmethane diisocyanate (MDI), and butendiol were synthesized by solution polymerization. The crystallinity of these polyesters and polyurethanes (PUs) and the compatibility of blends of PUs with PVC were studied by means of wide-angle x-ray diffraction (WAXD), differential scanning calorimetry (DSC), dynamic thermomechanical analysis (DMA), testing of solubility, and phase contrast microscopy. The results indicated that PBAU/PVC and PHAU/PVC were compatible systems, but PEAU/PVC was incompatible. The adhesive strengths of the three adhesives were quite different from one another, in the order of PBAU ≥ PHAU ? PEAU. The influences of crystallinity and compatibility on adhesion were discussed, and the Diffusion Theory for PU-PVC systems was recommended. © 1995 John Wiley & Sons, Inc. 相似文献
942.
Benzene alkylation with propane has been studied over HZSM-5 loading 3.1–15.4 wt% Mo in continuous-flow microreactor under
350 °C and atmospheric pressure with the highest activity obtained at 6.7 wt% Mo loading. C7–9 aromatics were obtained as main products while the total amount of benzene rings kept unchanged. i-Propylbenzene and n-propylbenzene are formed primarily, while toluene, ethylbenzene, and ethyl-toluene are formed secondly from the propylbenzenes.
Catalytic performance of 6.7 wt% Mo/HZSM-5(38) partially poisoned by NH3 shows that the strong acid sites play a crucial role in the alkylation. Low SiO2/Al2O3 ratio of HZSM-5 in the Mo modified catalysts gives high propane conversion. Two hydrothermal treatment methods were applied
to the 6.7 wt% Mo/HZSM-5(38) catalyst, caused decrease of propane conversion but result in different product distribution.
A possible reaction mechanism concerning bifunctional active centers resulted from combination of loaded Mo species and strong
acid centers on HZSM-5 is proposed. 相似文献
943.
Hsi-Jen Chen Shan-Huei Yang Shun-Hsing Huang Y.P. Chyou 《Journal of the Chinese Institute of Chemical Engineers》2007
This paper addresses an integrated design of paraffin-reformer, gas separations and the electricity production with a solid oxide fuel cell (SOFC). The overall design consists of three modules. First module is a system of paraffin reformer. In this module, the paraffin feed stream is to send to a steam-reformer. In the second module, the gas separations method illustrated is the combination of a methane-permeable membrane with a pressure-swing adsorption (PSA). In the third module, the purified hydrogen is fed to the SOFC unit. To be energy efficient, this paraffin-fueled SOFC system is designed with the consideration of heat integration. The intent of this paper is to provide a possible, alternative way of cogeneration systems for refinery and petrochemical plants. 相似文献
944.
A novel multiwalled carbon nanotube (CNTs) supported vanadium catalyst was prepared. The structure of catalyst prepared was characterized by TEM, BET, FTIR, XRD and temperature-programmed desorption (TPD) methods. The results indicated that vanadium particles were highly dispersed on the wall of carbon nanotubes. The V2O5/CNT catalysts showed good activities in the SCR of NO with a temperature range of 373–523 K. The Lewis acid sites on the surface of V2O5/CNT are the active sites for the selective catalytic reduction (SCR) of NO with NH3 at low temperatures. It was suggested that the reaction path might involve the adsorbed NH3 species reacted with NO from gaseous phase and as well as the adsorbed NO2 species. The diameter of CNTs showed positive effect on the activities of the catalysts. Under the reaction conditions of 463 K, 0.1 Mpa, NH3/NO = 1, GHSV = 35,000 h−1, and V2O5 loading of 2.35 wt%, the outer diameter of CNTs of 60–100 nm, the NO conversion was 92%. 相似文献
945.
946.
947.
基于RFID的虚拟标签算法研究与改进 总被引:3,自引:2,他引:1
针对室内定位算法VIRE的定位精度,特别是邻近边界目标的定位精度较低的问题,以RFID标签定位为研究基础,从改变VIRE算法中虚拟标签的插值方式和在边界上加入虚拟标签两个方面进行研究和改进。使用拉格朗日插值代替VIRE算法中的线性插值方式,使虚拟标签的数据更加接近实际环境值;在边界上加入虚拟参考标签能增加已知标签数,防止在计算待定位标签坐标时引入误差标签。实验结果表明,标签定位精度有了明显提高,整体能提高了35%,邻近边界标签定位精度提高较大,可达到50%以上。 相似文献
948.
Despite the successes in the last two decades, the state-of-the-art face detectors still have problems in dealing with images in the wild due to large appearance variations. Instead of leaving appearance variations directly to statistical learning algorithms, we propose a hierarchical part based structural model to explicitly capture them. The model enables part subtype option to handle local appearance variations such as closed and open month, and part deformation to capture the global appearance variations such as pose and expression. In detection, candidate window is fitted to the structural model to infer the part location and part subtype, and detection score is then computed based on the fitted configuration. In this way, the influence of appearance variation is reduced. Besides the face model, we exploit the co-occurrence between face and body, which helps to handle large variations, such as heavy occlusions, to further boost the face detection performance. We present a phrase based representation for body detection, and propose a structural context model to jointly encode the outputs of face detector and body detector. Benefit from the rich structural face and body information, as well as the discriminative structural learning algorithm, our method achieves state-of-the-art performance on FDDB, AFW and a self-annotated dataset, under wide comparisons with commercial and academic methods. 相似文献
949.
950.
Drawing upon a relationship quality framework, this study identifies how satisfaction, trust and different styles of handling conflict influence online buyers’ participation intentions in reputation systems associated with a C2C online shopping platform. Furthermore, we investigate how these effects are moderated by social conformity and the perceived value of knowledge. The results of a survey of 269 online buyers indicate that satisfaction, trust and an accommodating conflict handling style positively impact the intention to submit positive ratings, whereas an avoiding conflict handling style negatively affects the intention to submit positive ratings. Implications and suggestions for future research are provided. 相似文献