稀土树脂相分光光度法研究

在HCl—KCl(pH0.5)介质中,稀土—三溴偶氮胂二元络合物能较好地被阴离子交换树脂吸附。RE_2O_8在0～8μg/25ml范围内符合比尔定律,以双波长等吸收点法(测量波长λ_1=650nm,参比波长λ_2=740nm)扣除树脂背景影响,应用于稀土矿中稀土总量测定,结果令人满意。     

Condom use: A self-efficacy model.

A survey of heterosexually active college students gathered information about condom use, self-efficacy (SE), outcome expectancies, sexual attitudes, peer group influences, AIDS knowledge, and a perceived vulnerability to AIDS. On the basis of A. Bandura's (1986) social-cognitive theory, a structural model with SE as the central mediator was formulated and evaluated with LISREL. This model explained 46% of the variance in condom use from judgments of SE and effects attributable to peers and 53% of the variance in SE from outcome expectancies and peer group influences. Sexual attitudes, AIDS knowledge, and perceived vulnerability did not predict condom use. Most students were well-informed about HIV transmission but reported not feeling at risk, even though many engaged in risky sexual behavior. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

黑河干流中游地区耗水量变化的历史分析

黑河流域水资源极其匮乏，加之地区上的配置不均衡和中游地区水土资源的过度开发，导致黑河下游出现了严重的生态环境问题，已影响到我国北方广大地区生态环境质量，受到国家的高度重视和全社会的广泛关注。黑河水资源开发利用主要集中在中游地区，该区是全国重要的商品粮、蔬菜和经济作物生产基地之一，耗水量占流域耗水量的85％以上，是黑河的主要耗水区和径流利用区。利用黑河上游控制站莺落峡站和中游控制站正义峡站水文资料，分析了黑河中游耗水量的变化，结果表明：20世纪80年代以前黑河中游耗水量在4．4亿m^3左右，比较稳定；进入20世纪80年代以后，耗水量明显增加，80年代耗水量比70年代以前增加了1．97亿－2.49亿m^3;90年代耗水量又比80年代增加了1.64亿m^3左右；80年代以来流域耗水量呈明显增加的趋势，这是以人类活动影响为主的结果。     

高海拔长日低温条件下选择水稻光温敏核不育系的效果和方法研究

在高海拔长日低温、低海拔日高温、低海拔长日高温和人工气候室长光低温条件下，进行了光温敏不育水稻分离世代的不育株出现频率以及选择实用型不育系的效果和选择方法的研究。     

A New Variable Diffusion Drying Model for the Second Falling Rate Period of Paddy Dried in a Rapid Bin Dryer

The objectives of this article is to propose a new drying model for the second falling rate period known as the variable diffusion controlled period that follows after the first falling rate period and to propose a new method to determine the second critical moisture content that separates these two periods. Experimental work on paddy drying at minimum fluidization velocity was carried out in a rapid bin dryer. The effects of operating temperatures (60-120°C) and bed depths (2-6 cm) on the paddy drying characteristics were investigated. It was found that the normalized drying rate of paddy was proportional to the normalized moisture content in the first falling rate period but in the second falling rate period, the normalized drying rate of the material varies exponentially with the normalized moisture content. The different relationship between the normalized drying rate and the normalized moisture content in the first and second falling rate periods indicate that two different mechanism of moisture transport are at work. The new exponential model of the second falling rate period and the linear model of the first falling rate period were found to fit the experimental data very well. Derivation from variable diffusion equation shows that the linear model is the result of constant diffusion coefficient whereas the new exponential model is the result of linear diffusion coefficient. This also implies that the first falling rate period is a constant diffusion controlled period and the second falling rate period is a variable diffusion controlled period. In addition, drying kinetics data of a drying process that fits the exponential model over a very slow drying period will show that the drying process is under the effect of a linear diffusion coefficient. It was also found that the proposed new method to determine the second critical moisture content that distinguishes between the first and second falling rate periods by using a sudden change in the value of the drying rate gradient to a much lower value at that point is more rigorous and yet simpler than the method of determining the specific location of the receding drying boundary since it is based on the behavior of the actual drying kinetic data.     

Preparation of cross-section specimens for transmission electron microscopy from alpha-Al2O3/Ni solid state bonded bicrystal interfaces.

The technique which is described combines the advantages of the techniques formerly proposed in the literature in each stage of the preparation of transmission electron microscopy (TEM) specimens including a single metal-ceramic interface. It allows easy handling of the thin foils in spite of their brittleness. Preferential thinning of the softer material in the two-phase foil is prevented, and both sides of the interface are thinned down to comparable thicknesses. The nickel-alumina bicrystal interface observed in TEM is neat and free from any reaction layer. This method is easily adaptable to other metal-ceramic systems.     

Double melting behavior of cyclic tris(ethylene terephthalate)

Summary Cyclic tris(ethylene terephthalate) (CTET) was separated from oligomeric extract of poly(ethylene terephthalate) by the conventional solvent separation method. The structure of CTET was characterized by differential scanning calorimetry, X-ray diffraction, and scanning electron microscopy. It is shown that the double melting behavior of meltcrystallized CTET is attributed to the morphological change created by heat-treatment. The effect of the morphological change on the crystal structure of CTET was also examined.     

Impact of Aspen Log Storage with and without Protection on OSB Performance

Outdoor log storage without protection can change the mechanical and chemical properties of wood due to infection by various fungi. To understand how outdoor log storage affects the wood and, subsequently, the strandboard quality, two piles of aspen logs were set up outside and stored for a period of four months (July to November). One of the piles was treated with a biological solution to prevent fungal growth. The other one was stored without treatment. Both piles contained non-debarked and partially debarked logs. Evaluation of sap stain development indicated that all logs had been colonized by staining fungi with average stain coverage of 9.37 to 57.18% and maximum stain penetration of 3.58 to 7.27 cm over the log cross section. The variation of fungal colonization depended on log treatment and bark condition. The most effective way to prevent stain growth was the combination of biological treatment and partial debarking. A series of strandboard was prepared from fresh and aged aspen logs. All boards made from stored logs were statistically comparable to or superior to the control boards made from fresh aspen logs. The boards made from treated/partially debarked and untreated/non-debarked logs were statistically comparable to each other except for wet MOR. In addition, these two board types were statistically stronger than other boards made from treated/non-debarked and untreated/partially debarked logs in terms of IB and water resistance. Some individual stained strands were observed on the finished board surface. Less staining was found in the boards prepared from biologically treated and partially debarked logs, compared with those made from other stored logs.     

ARCGIS环境下基于DEM的流域特征提取

研究选取位于陕西省延安城南12 km处的万花乡向阳沟小流域。采用1∶10000大比例尺的比例尺5 m分辨率的DEM作为基本的地形数据,应用ESR I公司开发的ARCG IS地理信息系统软件进行流域特征的提取。经分析得到了研究区域河网特征以及研究区其它常用的流域特征信息,与实际河流水系特征基本吻合,认为应用DEM划分的流域结果是合理的。     

氧气顶吹转炉吹炼过程动态模型

通过炉气流量和成分的在线采样信息，用积分法计算熔池排出碳量，并根据熔炼体系中碳的守恒，动态推算熔池含碳量，由此来预报吹炼终点。较深入研究了提高炉气流量检测精度的方法，如心平衡修正和钢液成分反馈修正等，并采用了滤波算法，这些措施有利于提高动态模型的精度。