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31.
纳米β-NiOOH的固相合成及其性能 总被引:14,自引:1,他引:13
首次利用固相氧化法制备了 β NiOOH纳米粉体样品 ,经X射线衍射和透射电镜测试结果表明所得样品 β NiOOH粒子呈球形 ,粒径大小在 2 0~ 40nm之间。热重与差热分析结果表明当温度超过 10 0℃ ,样品开始不可逆地分解为NiO。运用恒流充放电、循环伏安以及Tafel极化等电化学测试对样品的电化学性能进行了初步研究。结果表明 :β NiOOH的交换电流密度高于 β Ni(OH) 2 的交换电流密度约一个数量级 ,具有较好的电极可逆性、较高的质量比容量以及优良的容量保持率 ,适于作为Zn/NiOOH类型镍电池的正极活性材料 相似文献
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33.
LU Xili WU Ye CAI Wei TANG Wenjun 《武汉理工大学学报(材料科学英文版)》2005,20(B12):287-289
A series of random and block poly( L-lactide-co-e-caprolactone ) ( PCLA ) copolymers whh different composition are prepared using stannous octaoate as catalyst.The effects of the amount of initiator on the intrinsic viscosity have been investigated. The structure of the PCLA copolymers is characterized by means of nuclear magnetic resonance( NMR ), Fourier transform infrared spectrum ( FTIR ), differential scanning calorimetry ( DSC ) and X- ray diffraction ( XRD ) methods. It is shown that the synthesis condition and the composition of copolymers obrious influence on the structure of PCLA copolymers. Hydrolytic degradation of the copolymers in a PBS solution of pH 7.4 at 37.0℃ shows that the copolymers of different composhions degrade at different rates. 相似文献
34.
The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding. 相似文献
35.
The new structure of fibre glass reinforced plastics bolt 总被引:4,自引:0,他引:4
The develop actuality and direction of FRP (fibre glass reinforced plastics) bolt in the world are analyzed. The new type structure of FRP bolt was designed. Trial data indicate that, all kinds of capability target of this FRP bolt all achieve and exceed the country stand-ard, substitute present metal bolt, wood bolt and bamboo bolt and other side bolt, it can gain magnitude technology and economy benefit. FRP bolt mechanization product line produce ef-ficiency is high, its throughput a day are 750 base, this can meet demand of hit-small mining company. 相似文献
36.
用己二酸二酰肼(ADH)对透明质酸(HA)进行化学修饰,制备交联透明质酸(HA-ADH)薄膜。粘度法测试表明HA-ADH是一种可降解的生物材料,并且与HA相比,HA.ADH的降解速率减慢。在此基础上,研究了以疏水性的替硝唑(TDZ)和亲水性的头孢唑啉钠(CEZ)为模拟药物的HA-ADH药物载体薄膜的释药性能。紫外-可见(UV-Vis)吸收光谱检测表明,HA-ADH是一种疏水性药物TDZ的优良缓释制荆,这是由于TDZ的疏水性和HA-ADH薄膜的缓慢溶胀和降解性能的结合而得到的,药物的释放主要受扩散机制控制。 相似文献
37.
针对碳酸盐岩气藏部分气井生产效能低的状况,决定在长庆气田下古生界尝试开展加砂压裂重复改造试验,以期提高低产、低效气井的产量,延长气田稳产期。通过潜心研究、精细设计及现场质检监控,优选了4口老井进行加砂压裂重复改造现场试验。从试验结果来看,虽然只有1口井取得明显的改造效果,但4口井加砂压裂施工都是成功的,说明对碳酸盐岩气藏实施加砂压裂是可以实现的,但在选井思路和压裂工艺方面还有待探索和研究。 相似文献
38.
Transglutaminase (TGase) was separated from the culture broth of an isolated strain of Streptoverticillium mobaraense. The crude enzyme was prepared by centrifugation, ultrafiltration, precipitation by alcohol, centrifugation and freeze‐drying. The yield after these processes was 65–70%. Then the enzyme was purified to homogeneity by chromatography on CM‐cellulose and Sephadex G‐75 on which the yields were about 70% and 80%, respectively; the purified folds reached 2.5–4.7 and 1.08–2.06, respectively. The molecular weight of this TGase was 39,500–40,100 Da by gel filtration chromatography. Optimum enzyme activity was observed in the pH range of 5.0–7.0, and it was maintained stable at 20–40C. The optimal temperature and pH was 52C and 6.0, respectively. At 1 mM and 5 mM metal ion or inhibitors concentration, TGase activity was strongly inhibited by Zn2+ and NEM, and not affected obviously by Ba2+, Ca2+, Co2+, Cu2+, Fe2+, Fe3+, Mg2+, Mn2+, Na+ as well as PMSF and EDTA. The effects of these additions on this TGase were compared with those of other microbial TGases. 相似文献
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40.