2,3,4- or 2,3,5-trisubstituted furans: catalyst-controlled highly regioselective ring-opening cycloisomerization reaction of cyclopropenyl ketones

2,3,4- or 2,3,5-trisubstituted furans were highly regioselectively formed from the cycloisomerization reaction of the same starting cyclopropenes 1 via the subtle choice of the transition metal halides. Under the catalysis of 5 mol % PdCl2(CH3CN)2, 2,3,5-trisubstituted furans 2 were given in 50-88% yields with 95-99% regioselectivities, while 2,3,4-trisubstituted furans 3 were formed in 78-96% yields with 99% regioselectivities under the catalysis of 5 mol % CuI.     

自发参量下转换光场的实验研究进展综述

自发参量下转换(spontaneous parametric down-conversion,SPDC)光场是基于单色泵浦光子流和量子真空噪声对非线性晶体的综合作用而产生的,它固有的量子起源决定了在非经典光场研究中的重要地位和作用.对SPDC光场的相干特性和它在绝对测量光电探测器量子效率中的应用进行了深入而细致的研究和探讨.     

HYQ-965-Ⅲ解堵剂的研制及现场应用

针对涠洲11-4油田W11-4D-A1井返吐油基泥浆堵塞油管问题,以渗透剂、乳化剂、分散剂、互溶剂为原料,制备了HYQ-965-Ⅲ解堵剂.考察了不同配方解堵剂中原料间的配伍性和溶垢效果,研究了最佳配方:渗透剂Ⅰ20%、乳化剂Ⅰ10%、分散剂10%、互溶剂10%、海水50%.将该解堵剂在W11-4D-A1井进行应用,从现场使用情况看,HYQ-965-Ⅲ对油基泥浆、原油具有很好的分散能力,成功解除了油管堵塞,达到预期设计要求.     

Dynamics of the uptake of free amino acids in the blood serum of the portal vein during the digestion of isolated krill protein

The rate of absorption of amino acids obtained from isolated krill protein administered to rat stomach was studied. Absorption of casein amino acids was determined for reference purposes. Rats subjected to 48-hour fasting were administered krill isolate and casein in the form of homogenates at a rate 540 mg protein per 100 g bw in 6 ml of distilled water. The concentration of free amino acids in the portal vein was measured after 30 minutes, 1, 3 and 6 hours. The content of amino acids was measured by ion-exchange chromatography with the use of an automatic analyzer of amino acids. The digestion of krill protein proceeds at a high rate. This ensures the maximal augmentation of the concentration of most amino acids in the blood of the portal vein 30 min after isolate administration to the stomach.     

磷脂产品的常用法规、术语、指标

介绍了有关组织对磷脂的法规、术语、指标及意义.     

攀钢1号和2号方坯连铸工艺及设备

介绍了攀钢提钒炼钢厂1号和2号方坯连铸机的性能参数、工艺布置及流程、设计特点、装备水平,及攀钢通过技术改造新建1号和2号方坯连铸机,彻底淘汰模铸实现全连铸的实践经验.     

Influence of ZnO and P2O5 Content on Modified HZSM-5 on Aromatization of FCC Gasoline

Catalytic properties of different content of ZnO and P₂O₅ supported on HZSM-5 zeolites were studied in the conversion of FCC gasoline (75°C-120°C) into aromatic hydrocarbons with a temperature of 430°C, a liquid hourly space velocity of 1.0 hr^-1, and a pressure of 0.1 MPa. In the reaction, when the contents of ZnO and P₂O₅ are 2% and 4%, respectively, Zn-P/HZSM-5 showed the highest selectivity and activity to aromatic hydrocarbons and conversion of olefins. The content of aromatics in the liquid product and the yield of aromatics reached as high as 94.53%, 68.87%, and 51.74%, respectively.     

Extended analysis of ground impedance measurement using the fall-of-potential method

An extended analysis of ground impedance measurement using the fall-of-potential method will be presented. An interesting curve that represents the exact locations of the potential probe when the potential and current probes are in different directions is obtained for the first time. Curves representing measurement error are also presented for the case when the potential probe is placed in locations where the correct ground impedance cannot be measured. A similar analysis for ground impedance measurements in multilayer soils is also discussed. The study presented in this paper has extended the theory of the conventional fall-of-potential method and the results obtained can serve as a practical guide for ground impedance measurements made using this method.     

叠前地震数据的规则化

本文通过对动校正前积分法DMO原理的探讨，在借鉴Canning(1996)提出的利用DMO实现三维数据规则化的方法和Biondi(1998)提出的三维叠前地震数据方位角校正方法的基础上，从方位角校正的角度入手，利用DMO和DMO^-1相结合的处理流程对地震数据进行规则化，以得到新的规则的观测系统下具有所需特定方位角的观测数据。此方法可用于解决叠前地震数据道插值、陆上地震勘探中不规则观测数据的规则化和海上地震勘探中的羽状现象校正等问题，可将已有地震观测数据转变为特定观测系统的叠前地震数据，以便于某些处理方法的应用。此方法原理简单并具有广泛的适用性。