Architectural Control of Hierarchical Nanobelt Superstructures in Catanionic Reverse Micelles

BaXO₄ (X = Mo, W) nanobelts and a variety of hierarchical superstructures assembled from the nanobelts have been synthesized in a catanionic reverse‐micelle system. The effects of various factors, such as the mixing ratio (r) between the anionic and cationic surfactants, the temperature, and the presence of polymeric additives, on the formation of the nanobelts and their hierarchical assembly have been examined in detail. In particular, r has been shown to be powerful in modulating the formation and assembly of the BaMoO₄ and BaWO₄ nanobelts. Architectural control of the penniform nanobelt superstructures has been readily achieved by changing the experimental parameters. A plausible two‐stage growth mechanism has been proposed for the formation of penniform BaXO₄ nanobelt superstructures in catanionic reverse micelles.     

Elastic constants of face-centered cubic and L1<Subscript>2</Subscript> Ni-Si alloys: Composition and temperature dependence

The adiabatic elastic stiffness constants C _ij of Ni-Si single-crystal solid-solution alloys of two slightly different compositions, 10.78 and 11.17 at. pct Si, were measured over the temperature range from 20 °C to 900 °C using the rectangular parallelepiped resonance method. The isotropic elastic constants of the polycrystalline ordered intermetallic compound Ni₃Si containing 23 at. pct Si were also measured over this temperature range. Values of the C _ij for Ni₃Si were estimated from the data on the polycrystalline alloy, as well as from published data in the literature on isomorphous ternary ordered intermetallic compounds containing different amounts of Si. Using measured values and previously published data, the stiffness constants of Ni₃Ti were estimated; these are the only available data on this alloy. The estimated single-crystal elastic constants of Ni₃Si, as well as the experimentally measured bulk modulus, are considerably smaller than published values calculated from first-principles methods. The same is true for the C _ij of Ni₃Ti, but the discrepancies are smaller.     

2-巯基苯并噻唑衍生物摩擦学性能的研究

合成了S—(1—(2—苯并噻唑基巯基)—2—羟基)—丙基N，N—二烷基二硫代氨基甲酸酯和S—(1—(2—苯并噻唑基巯基)—2—乙酰基)—丙基N，N—二烷基二硫代氨基甲酸酯两种化合物。运用IR、MS、HNMR和元素分析等分析方法对其结构进行表征。用四球试验、HQ—l环块试验分别考察了其对润滑油的极压承载能力及抗磨减摩性能的影响。结果表明：在350SN中性油中添加所合成的化合物后可以显著降低四球长磨后磨斑直径、有效地降低摩擦副之间的摩擦系数，拥有优良的摩擦学性能。     

煤基链篦机-回转窑一步法直接还原设备改造及技术操作要点

本文主要论述了煤基链篦机-回转窑一步法直接还原关键设备改造及有关技术操作要点，并提出了进一步提高产量，稳定操作，延长作业周期，降低生产成本的技术改造方案。     

软启动器在深井泵电动机上的应用

论述了几种三相交流异步电动机的起动方式及其优缺点 ,介绍了新型的电子软启动方式在我厂深井泵电动机上的应用及取得的运行效果 ,为电动机软启动方式在工矿企业中的应用提供了应用经验。     

质子交换铌酸锂波导MMI光功分器

利用三维非旁轴近似光束传输法对退火质子交换铌酸锂渐变折射率分布波导中的自镜像效应进行分析与模拟 .在此基础上 ,利用退火质子交换技术在 X切 Y传铌酸锂衬底上进一步制作了 1× 8MMI光功分器 .测试表明器件实现了 1路分成 8路的光功分功能 .     

Resource management in the next-generation DS-CDMA cellular networks

Direct sequence code-division multiple access has been shown as the predominant access technology to provide high-speed multimedia services in next-generation wireless cellular networks. The DS-CDMA cellular network significantly differentiates itself from the traditional narrowband TDMA/FDMA system, in which great capacity gain can be explored by taking advantage of its unique characteristics. This article addresses resource management in DS-CDMA cellular networks. We first provide an overview of the DS-CDMA network and discuss the main challenges in the design of resource management schemes. We then examine several critical issues within the scope of resource management, including congestion control, rate and power control, and cell planning, with the emphasis on call admission control. Finally, we offer some insights and discussions on the performance aspects, strengths, and weaknesses of existing proposals.     

In situ polymerization and characterization of polyester‐based polyurethane/nano‐silica composites

Polyester‐based polyurethane/nano‐silica composites were obtained via in situ polymerization and investigated by Fourier‐transform infrared spectroscopy (FTIR), or FTIR coupled with attenuated total reflectance (FTIR‐ATR), Transmission electron microscopy (TEM), atomic force microscopy (AFM), an Instron testing machine, dynamic mechanical analysis (DMA) and ultraviolet‐visible spectrophotometry (UV‐vis). FTIR analysis showed that in situ polymerization provoked some chemical reactions between polyester molecules and nano‐silica particles. FTIR‐ATR, TEM and AFM analyses showed that both surface and interface contained nano‐silica particles. Instron testing and DMA data showed that introducing nano‐silica particles into polyurethane enhanced the hardness, glass temperature and adhesion strength of polyurethane to the substrate, but also increased the resin viscosity. UV‐vis spectrophotometry showed that nano‐silica obtained by the fumed method did not shield UV radiation in polyurethane films. Copyright © 2003 Society of Chemical Industry     

TPS/TDC3000系统串口通讯的规划与应用

针对TPS/TDC30 0 0系统串口通讯方式、机理进行了一般性的介绍 ,对规划与应用中常见的的问题 ,根据实际工程应用经验提出了解决方案。     

低乙烯含量抗冲聚丙烯的结构表征

采用二甲苯为溶剂，将不同乙烯含量（５％￣１５％质量）的抗冲聚丙烯用特定程序进行分级，将各样品分为室温下可溶于甲苯和不可溶于甲苯的两部分。使用＾１３Ｃ－ＮＭＲ方法和ＦＴ－ＩＲ方法对各组分进行表征，明确了乙烯链段在聚丙烯链上的分布，并在此基础上提出了产生这种链结构的聚合工艺的特点。