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31.
E. Vetrivendan G. Thendral A. Ravi Shankar C. Mallika 《Materials and Manufacturing Processes》2017,32(12):1435-1441
The insulation resistance of conventional atmospheric plasma-sprayed alumina coatings with 10–15% porosity is ~1011 Ω. The presence of pores, lamellae boundaries, and other non-fillings dampens the insulation resistance of the coating. In the present study, aluminum phosphate was used to seal the surface of plasma-sprayed alumina coating and evaluate the effect of sealing on the insulation resistance and its thermal cycling response. Sealing was carried out with three concentrations of sealant (P/Al molar ratio of 3, 10, and 15). Characterization by X-ray diffraction and scanning electron microscopy revealed the primary sealing phase as aluminum metaphosphate and effective sealing of the pores by the aluminum phosphate phases. Insulation resistance is improved by two orders of magnitude after sealing the coated samples. Sealing with P/Al molar ratio 3 exhibited maximum insulation resistance of ~1013 Ω at room temperature. Thermal cycling studies between 650°C and 200°C on the sealed samples showed deterioration in thermal cycling life after sealing. 相似文献
32.
Alumina ceramic is well documented as a much-demanded advanced ceramic in the present competitive structure of manufacturing and industrial applications owing to its excellent and superior properties. The current article aimed to experimentally investigate the influence of several process variables, namely: spindle speed, feed rate, coolant pressure, and ultrasonic power, on considered machining characteristics of interest, i.e., chipping size and material removal rate in the rotary ultrasonic machining of alumina ceramic. Response surface methodology has been employed in the form of a central composite rotatable design to design the experiments. Variance analysis testing has also been performed with a view to observing the consequence of the considered parameters. The microstructure of machined rod samples was evaluated and analyzed using a scanning electron microscope. This analysis has revealed and confirmed the presence of plastic deformation that caused removal of material along with brittle fractures in rotary ultrasonic machining of alumina ceramic. The validity and competence of the developed mathematical model have been verified with test results. The multi-response optimization of machining responses (material removal rate and chipping size) has also been attempted by employing a desirability approach, and at an optimized parametric setting the obtained experimental values for material removal rate and chipping size were 0.4166?mm3/s and 0.5134?mm, respectively, with a combined desirability index value of 0.849. 相似文献
33.
Sanjay Sahare Ravi Kant Choubey Gurunath Jadhav Tejashree M. Bhave Samrat Mukherjee Sunil Kumar 《Journal of Superconductivity and Novel Magnetism》2017,30(6):1439-1446
In this report, we studied various structural and optical properties of pure and copper-doped cadmium oxide (CdO) thin films. Nanostructured Cu-doped CdO films were deposited using sol–gel spin-coating technique. The structural and morphological changes have been observed by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and atomic force microscopy (AFM) studies. The optical and electrical properties of the pure and Cu-doped CdO thin films were studied by UV–vis spectroscopy and four-point probe method, respectively. The XRD peaks show the formation of nanocrystalline CdO with cubic face-centered crystal structure. The band gaps of the as deposited films were found in the range of 2.32–2.73 eV, while after doping, it decreases due to structural deformation. The electrical resitivity was found to decrease approximately ~10 in Cu-doped CdO thin films. 相似文献
34.
Jayaprakash Vandana Kaliyur Ravi Shri Aishvarya Vinni Novi Swaroopini Ramachandran Hridya Radhakrishnan Vaidyanathan Vinoth Kumar 《IET nanobiotechnology / IET》2017,11(6):690
The present study deals with the production of 5‐hydroxymethyl furfural (HMF) from fructose by chemo‐conversion method using chemical catalyst, conventionally achieved by microwave‐assisted dehydration process. Five different chemical catalysts, namely oxalic acid, phosphotungstic acid and mesoporous titanium dioxide nanoparticles (TNPs) were compared at constant conditions of which TNPs yielded a maxima of 33.95%. The optimum temperature and catalyst loading were found to be 200°C and 20%, respectively, at a 5% optimum substrate concentration during 15 min optimum reaction time to yield 61.53% HMF. The efficiency of synthesised TNPs was investigated further through reusability studies. TNPs were properly recycled and the catalytic activity recovery was good even after a 14 batch reactions. The specific surface area of the TNP obtained is about 105.46 m2 /g and its pore‐volume is about 0.42 cm3 /g according to single point adsorption. A large accessible surface area combined with a minimal pore size (15.92 nm) obtained with mesoporous TNPs is desirable for better catalyst loading, high‐yield HMF, retention and reduced diffusion constraints.Inspec keywords: mesoporous materials, recycling, production management, dissociation, nanoparticles, nanotechnologyOther keywords: mesoporous titanium dioxide nanocatalyst, recyclable approach, one‐pot synthesis, 5‐hydroxymethyl furfural production, HMF, chemo‐conversion method, chemical catalyst, microwave‐assisted dehydration process, oxalic acid, phosphotungstic acid, mesoporous titanium dioxide nanoparticles, TNP 相似文献
35.
Rashmi Mahajan Akhshay Singh Bhadwal Nishant Kumar Mukil Madhusudanan Ramesh Namdeo Pudake Ravi Mani Tripathi 《IET nanobiotechnology / IET》2017,11(4):360
The present study reports a novel, facile, biosynthesis route for the synthesis of carbon nanodots (CDs) with an approximate quantum yield of 38.5%, using Musk melon extract as a naturally derived‐precursor material. The synthesis of CDs was established by using ultraviolet–visible (UV–vis) spectroscopy, Dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy and Fourier transform infrared (FTIR) spectroscopy. The as‐prepared CDs possess an eminent fluorescence under UV–light (λ ex = 365 nm). The size range of CDs was found to be in the range of 5–10 nm. The authors further explored the use of such biosynthesised CDs as a photocatalyst material for removal of industrial dye. Degradation of methylene blue dye was performed in a photocatalytic reactor and monitored using UV–vis spectroscopy. The CDs show excellent dye degradation capability of 37.08% in 60 min and reaction rate of 0.0032 min−1. This study shows that synthesised CDs are highly stable in nature, and possess potential application in wastewater treatment.Inspec keywords: carbon, nanostructured materials, nanofabrication, catalysis, photochemistry, ultraviolet spectra, visible spectra, photoluminescence, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectra, fluorescence, dyesOther keywords: green synthesis, highly stable CD, photocatalytic performance, biosynthesis route, carbon nanodots, quantum yield, Musk melon extract, naturally derived‐precursor material, ultraviolet‐visible spectroscopy, dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy, FTIR spectroscopy, fluorescence, biosynthesised CD, photocatalyst material, industrial dye, methylene blue dye degradation, photocatalytic reactor, UV‐vis spectroscopy, wastewater treatment, size 5 nm to 10 nm, time 60 min 相似文献
36.
A vendor-managed inventory (VMI) relationship between a downstream retailer and an upstream vendor consists of two distinct components: (i) information sharing (IS) and (ii) a shift in decision-making responsibility. This study compares these two components of VMI in a two-stage serial supply chain based on the ‘static uncertainty’ strategy under dynamic and random demand with fill rate constraints. Numerical experiments are conducted using analytical models to identify the conditions where the incremental value of VMI over IS is significant. The results provide guidelines relevant to academia and supply chain practitioners in taking VMI adoption decision above and beyond IS according to their specific business environment. 相似文献
37.
38.
Ravi Shanker Vidyarthy Dheerendra Kumar Dwivedi Vasudevan Muthukumaran 《Materials and Manufacturing Processes》2018,33(7):709-717
In the present work, the influence of process parameters such as welding current (I), welding speed (S), and flux coating density (F) on different aspects of weld bead geometry for example depth of penetration (DOP), bead width (BW), depth to width ratio (D/W), and weld fusion zone area (WA) were investigated by using the central composite design (CCD). 9–12% Cr ferritic stainless steel (FSS) plates were welded using A-TIG welding. It was observed that all input variables have a direct influence on the DOP, BW, and D/W. However, flux coating density has no significant effect on WA. Mathematical models were generated from the obtained responses to predict the weld bead geometry. An optimized DOP, BW, D/W, and WA of 6.95?mm, 8.76?mm, 0.80, and 41.99?mm2, respectively, were predicted at the welding current of 213.78 A, the welding speed of 96.22?mm/min, and the flux coating density of 1.99?mg/cm2. Conformity test was done to check the practicability of the developed models. The conformity test results were in good agreement with the predicted values. Arc constriction and reversal in Marangoni convection were considered as major mechanisms for the deep and narrow weld bead during A-TIG welding. 相似文献
39.
Micro-drilling in carbon fiber reinforced plastic (CFRP) composite material is challenging because this material machining is difficult due to anisotropic, abrasive and non-homogeneous properties and also downscaling of cutting process parameters affect the cutting forces and micro-drilled hole quality extensively. In this work, experimental results based statistical analysis is applied to investigate feed and cutting speed effect on cutting force components and hole quality. Analysis of variance based regression equation is used to predict cutting forces and hole quality and their trend are described by response surface methodology. Results show that roundness error and delamination factor have similar trends to those of radial forces and thrust force, respectively. Non-linear trends of cutting forces and hole quality errors are observed during downscaling of the micro-drill feed value. Optimization results show that cutting forces and hole quality errors are minimum at a feed value which is almost equal to the tool edge radius rather than at the lowest feed value. Therefore, the presented results clearly show the influences of size effects on cutting forces and hole quality parameters in micro-drilling of CFRP composite material. 相似文献
40.
Nipin KohliAuthor VitaeOnkar SinghAuthor Vitae Ravi Chand SinghAuthor Vitae 《Sensors and actuators. B, Chemical》2011,158(1):259-264
Nanoparticles of chromium oxide have been synthesized by following a co-precipitation route at various pH values of the precursor solution. Structural and morphological analysis were carried out by using XRD and TEM techniques which revealed that the size of nanoparticles synthesized at pH 9 was smaller as compared to those synthesized at other pH values. The thick films of synthesized samples were deposited on alumina substrate and their sensing response to methanol, ethanol and isopropanol was investigated at different operating temperatures. It was observed that all the sensors gave optimum response at 250 °C. It has been observed that sample prepared at pH 9, being a collection of smallest particles as compared to other samples, exhibited high sensing response to alcohol vapour. Sensor response of all the samples tested was significantly higher towards isopropanol vapour than towards methanol or ethanol.In the present study the effect of particle size on intergranular activation energy has been studied as well. It was found that smaller particles possess high activation energy and exhibit higher sensing response as compared to that of larger particles. This type of study may help in the selection of particle suitable for gas sensing. 相似文献