回火处理对高碳冷拔钢丝强度和塑性的影响

研究了６５钢冷拔钢丝在５００℃不同时间回火时的抗拉强度和延伸率的变化。试验结果发现，在回火初期，抗拉强度首先增长，然后随口火时间的延长连续降低，而延伸率始终在增长，增长速度是先快后慢。这种行为可归因于第一内应力的消除和ε－碳化物在形变铁素体中的析出以及后来再结晶的发生。     

Integration of mobile vehicles for automated material handlingusing Profibus and IEEE 802.11 networks

This paper focuses on a method to integrate mobile devices such as a mobile robot, automated guided vehicle, and unmanned container transporter to form an automated material handling system. In this paper, the stationary devices are connected via a Profibus network while the mobile devices are communicating via an IEEE 802.11 wireless LAN. In order to integrate these two networks, a protocol converter is developed on a PC platform that runs two interacting processes with shared internal buffers. The protocol converter performs a role of translator between two different protocols by converting the format of a data frame. In addition to this basic conversion function, the protocol converter has a virtual polling algorithm to reduce the uncertainty involved in accessing the wireless network. Finally, the integrated network. of Profibus and IEEE 802.11 is experimentally evaluated for its data latency and throughput, which shows the feasibility of the Profibus-IEEE 802.11 network for industrial applications involving mobile devices     

高频地波雷达相位补偿系统

OSMAR2000采用的是“一发八收,收发共用”模式的相控阵高频地波雷达.为了扩大其探测的范围,在新的雷达系统中将采用多发多收的模式,从而导致当信号通过通道后,信号的相位会因受到通道的调制而发生改变,使得雷达无法正常工作,因此需要对通道的相位进行实时监控和补偿.在参考了低频段的相位测量原理和射频段的相移电路的设计理论的基础上,该文提出了基于差分放大器、容阻和容感器件的高频地波雷达收发通道的相位控制系统.     

异构空间信息的分级共识模型研究

Internet上异构、分布的空间信息因各自独立、相对封闭而无法相互沟通和协作,从而形成了空间信息孤岛。论文利用计算机的知识表示理论和Ontology技术能够明确表达相关领域共识的特点,探索性地提出了异构空间信息的分级共识模型。该模型为解决上述问题提供了一条切实可行的新思路。     

Deactivation of copper-ion-exchanged hydrogen-mordenite-type zeolite catalyst by SO2 for no reduction by NH3

Deactivation of copper-ion-exchanged hydrogen-mordenite-type zeolite catalyst by SO₂ for NO reduction by NH₃ was examined in a fixed-bed flow reactor. The deactivation of the catalyst was strongly dependent on reaction temperature. At high reaction temperatures over 300°C, the catalyst did not lose its initial activity up to 50 h of operation, regardless of SO₂ feed concentration from 500 to 20,000 ppm. However, at low reaction temperatures near 250°C, apparent deactivation did occur. Changes in the physicochemical properties such as surface area and sulfur content of deactivated catalyst well correlated with catalyst activity, depending upon reaction temperatures. The deactivation was due to pore blocking and/or filling by deactivating agents, which plugged and/or filled the pores of catalyst. The deactivating agents deposited on the catalyst surface were presumed to be (NH₄)₂SO₄ and/or (NH₄)HSO₄ from the results of TGA and ion-chromatography measurement.     

Effect of partitioning on microstructure and properties of a medium carbon Ti Mo bearing high strength Q&P steel

In order to investigate the effect of partitioning procedures on microstructure and properties of a medium carbon Ti Mo bearing steel, the salt bath experiment, field emission SEM, TEM and tensile tests as well as wear tests were utilized to clarify the microstructural evolution and property changes treated by different partitioning parameters. The results show that the microstructures consist of tempered lath martensite, cementite and (Ti, Mo)C particles. With prolonging partitioning time or increasing partitioning temperature, the amount of laths martensite decreases and thicker martensite plates with blunt boundaries appear. In addition, with increasing partitioning temperature from 310℃ to 400℃, the tensile strength, hardness and low temperature toughness are simultaneously decreased, and the reduction reaches up to about 300MPa, 100HV and 20J, respectively. Finally, the wear performance of the samples partitioned below Ms is obviously better than that of samples partitioned above Ms. The morphology of worn surface of samples partitioned below Ms is characterized by plastic fatigue morphology, while the worn surfaces of samples partitioned above Ms are mainly dominated by grooves.     

Characterization of C-S-H from Highly Reactive β-Dicalcium Silicate Prepared from Hillebrandite

β-dicalcium silicate synthesized by thermal dissociation of hydrothermally prepared hillebrandite (Ca₂(SiO₃)(OH)₂) exhibits extremely high hydration activity. Characterization of the hydrates obtained and investigation of the hydration mechanism was carried out with the aid of trimethylsilylation analysis, ²⁹Si magic angle spinning nuclear magnetic resonance, transmission electron microscopy selected area electron diffraction, and XRD. The silicate anion structure of C-S-H consisted mainly of a dimer and a single-chain polymer. Polymerization advances with increasing curing temperature and curing time. The C-S-H has an oriented fibrous structure and exhibits a 0.73-nm dreierketten in the longitudinal direction. On heating, the C-S-H dissociates to form β-C₂S. The temperature at which βC₂S begins to form decreases with increasing chain length of the C-S-H or as the Ca/Si ratio becomes higher. The high activity of β-C₂S is due to its large specific surface area and the fact that the hydration is chemical-reaction-rate-controlled until its completion. As a result, the hydration progresses in situ and C-S-H with a high Ca/Si ratio is formed.     

氧气放电辅助激光淀积原位制备高T_c超导薄膜

采用低压氧气放电辅助的激光淀积方法,原位外延生长出零电阻温度91K,临界电流密度10~5A/cm~2的Y-Ba-Cu-O高温超导薄膜。扫描电镜和X光衍射分析结果表明,薄膜中超导相晶粒的生长具有c轴垂直于表面的择优取向。