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The characterisitics of the development of helium porosity in bcc and fcc alloys and structural steel after irradiation with
40-keV He+ up to dose 5⋅1020 m−2 at 20°C and subsequent annealing at 650°C for 1 h and 5 h are studied by transmission electron microscopy. It it found that
under these conditions smaller bubbles with high density are formed in bcc than in fcc materials. It is shown that for an
annealing time of 5 h higher porosity is formed in all materials, except nickel, than with 1 h annealing. This is due to the
inflow of thermal vacancies from the free surface. The data obtained are discussed from the standpoint of the formation of
various helium-containing complexes, their thermal stability, and the diffusion mobility of the matrix atoms.
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Translated from Atomnaya Energiya, Vol. 99, No. 2, pp. 115–120, August 2005. 相似文献
85.
Cintia Maria Rodrigues Rosa Mateus Vinícius Casagrande da Silva Leandro Gonçalves de Aguiar Heizir Ferreira de Castro Larissa Freitas 《应用聚合物科学杂志》2020,137(41):49258
Magnetic polymers supports have proven to be valuable materials for enzyme immobilization, as they allow recovering the catalyst by magnetic separation, precluding the need for costly and time-consuming separation steps. In this study, magnetic copolymer supports were synthesized using styrene (STY) and different crosslinking agents (divinylbenzene, ethylene glycol dimethacrylate, or triethylene glycol dimethacrylate) and initiators (azobisisobutyronitrile or benzoyl peroxide) and used to immobilize Candida antarctica lipase B (CALB). The aim was to obtain biocatalysts with high enzymatic activity and satisfactory morphological properties for use in biotransformation reactions. Two morphological properties known to influence the immobilization yield were taken into consideration, specific surface area, and swelling index. Experimental data were compared to the predictions of a model based on molar balance, method of moments, numerical fractionation, and elementary gel structures. The high correlation (R2 = 0.9974) between experimental and predicted values demonstrated the suitability of the model for estimating the textural properties of enzyme supports. CALB was successfully immobilized, showing high hydrolytic activity (500–700 U g−1) and good thermal stability at 50°C. CALB/STY-EGDMA-M was 14 times more stable than free CALB. The results confirm the efficiency of the immobilization method and the suitability of the copolymers for enzyme immobilization. 相似文献
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Vinícius de Carvalho Neiva Pinheiro Alberto L. Francato Warren B. Powell 《国际能源研究杂志》2020,44(11):8635-8653
Intermittent energy sources such as wind and solar have recently been growing a lot faster than dispatchable energy sources in Brazil, which made investments in energy storage systems become an attractive possibility in the country. Current operational policies for energy dispatch do not consider storage systems and need adjustments to fit this technology. With this motivation, we use reinforcement learning techniques to develop policies for managing storage systems in a grid that can handle time-varying inputs and loads, with rolling forecasts. We use a deterministic lookahead (DLA) policy which has been parametrically modified to perform well in the presence of uncertain forecasts. For realistic simulations, the base model considers important characteristics in a grid that influence the interaction between scheduling and real-time operation such as power and ramping capacities, notification times, and stochastic forecasts. The parametric modification with tunable parameters allows an optimal balance between two conflicting services provided by the storage system: time-shifting and spinning reserves. Optimal reserves ranged from 35% to 100%, depending on the tested dataset, which shows the importance of tuning. Differently from stochastic lookahead policies, which are computationally expensive, parameterized DLA policies can be applied to real-time operation after being optimized in a stochastic base model. 相似文献
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Caio Machado Fernandes Marcos Vinícius Palmeira de Mello Nazir Escarpini dos Santos Alessandra Mendonça Teles de Souza Mauricio Lanznaster Eduardo Ariel Ponzio 《工业材料与腐蚀》2020,71(2):280-291
4-Chloro-N-(pyridin-2-ylmethyl)aniline (CPYA) was synthesized by a simple and inexpensive method and tested as a corrosion inhibitor in acid medium for mild steel by using gravimetric studies and electrochemical measurements. An average maximum efficiency of 96.0% was achieved at 4.59 mmol/L. Corrosion kinetic and thermodynamic parameters were also analyzed. Surface analyses (atomic force microscopy and scanning electron microscopy) show that protection is enabled by adsorption on the metal, forming a film. Quantum chemical calculations were performed to access information regarding the molecular structure in the corrosive medium and to support interpretation of the results obtained by experimental methods. 相似文献
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Busarakorn Mahayothee Nilobon Komonsing Pramote Khuwijitjaru Marcus Nagle Joachim Müller 《International Journal of Food Science & Technology》2019,54(2):460-470
In this study, drying of red-fleshed dragon fruit at different temperatures (40, 50, 60, 70 and 80 °C) and air velocities (1.0 and 1.5 m s−1) was conducted under the specific humidity of 25 g H2O kg−1 dry air. The results showed that drying at higher temperatures resulted in shorter drying times. However, temperature and air velocity did not significantly affect the total betacyanin contents and antioxidant capacities in dried products. Seven betacyanins identified by LC-MS were betanin, isobetanin, phyllocactin, isophyllocactin, betanidin 5 –O-(6′O-3-hydroxybutyryl)-β-glucoside, isobetanidin 5 –O-(6′O-3-hydroxybutyryl)-β-glucoside and decarboxylated phyllocactin. In addition, the temperature increased the isomerisation of betacyanins. The most preferable condition for preserving the colour and betacyanin contents of red-fleshed dragon fruit was the drying at a temperature of 80 °C and air velocity of 1.5 m s−1 since it could shorten the drying time and give a bright red colour to the dried product as well as it had no significant impact on the betacyanins. 相似文献
89.
Mussel (Perna perna) Processing by an Alternative Method and Packaging Under Modified Atmosphere to Improve Physicochemical and Microbiological Characteristics 下载免费PDF全文
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