双噁唑啉化合物对PBT的增粘作用

以２．２＇－双（２－唑啉）和双（２－唑啉基）苯作扩链剂，用焙融挤出的方法，对聚对苯二甲酸丁二酯（ＰＢＴ）进行扩链，考察扩链剂的用量、反应时间和反应温度对ＰＢＴ的特性粘度及端羧基含量（ＣＶ）的影响。结果表明，当用２，２＇－双（２－唑啉）作扩链剂时，ＰＢＴ的特性粘度［η］从０．７９９提高到０．９２６ｄＬ／ｇ，ＣＶ降至５ｅｑ／１０￣６ｇ以下；当用双（２－　唑啉基）苯作扩链剂，［η］从０．７６３增至０．９２５ｄＬ／ｇ，ＣＶ降至１０ｅｑ／１０￣６ｇ以下，达到了较满意的扩链效果。     

压力容器标准对不等厚板材对接要求的分析

欧盟、美国和我国压力容器标准对不等厚板材对接时均有削薄要求,通过有限元方法计算不同条件下连接时的应力分布,认为不等厚板材对接连接时,按照EN13445(2002)要求增加直边段,对减小局部应力有一定好处,对提高射线检测灵敏度有利.     

活性炭载体的超声波处理对Pt／C催化剂活性的影响分析

通过对活性炭载体进行不同条件的超声波处理获得了具有不同表面化学性质的载体，使用比表面积（BET）、酸碱滴定等技术手段对载体的物理化学性质进行了表征。将经过超声波处理的活性炭载体制备成Pt／C催化剂，并将催化剂直接用于催化反应，考察了活性炭载体的不同超声波处理条件对Pt／C催化剂性能的影响。实验发现，活性炭载体经过超声波处理后，表面灰分含量、pH值和中孔孔容有较大的变化；使用经过60min超声波处理后中孔孔容较大的活性炭作为载体制备的Pt／C催化剂，在催化加氢反应性能测试中显示了最高的催化活性。在此基础上，就活性炭载体的超声波处理对Pt／C催化剂活性的影响进行了讨论。     

Simple autocorrelation technique based on degree-of-polarization measurement

We demonstrate a simple optical-fiber-based autocorrelator for picosecond short pulses based on degree-of-polarization measurement while tuning the relative delay of the two orthogonal polarization states of the pulse. The pulsewidths of 20-, 40-, and 80-GHz pulse trains and 2-ps pulses generated by a mode-locked laser are measured. The <-10-dBm optical powers are used in the experiment. The measurement results agree well with the measurements using conventional techniques. Compared with conventional autocorrelators, this technique has the advantages of 1) wavelength independent, 2) significant less alignment, and 3) no high power required.     

Analysis of dinosaur samples by nuclear microscopy

Several dinosaur bone and eggshell fossil samples unearthed at different sites in China were analyzed by means of nuclear microscopy. Concentrations and distributions of elements such as Na, Mg, Al, P, S, Ca, Cr, Mn, Fe, Cu, Zn, As, Br, Sr, Y, Ce, Pb and U, etc. were obtained for each sample. The results of quantitative PIXE and RBS analyses show unusually high concentrations of U and Ce in several samples obtained from a period near the K-T boundary (between Cretaceous and Tertiary periods, 65 million years ago), suggesting that some form of environmental pollution could be the cause of dinosaur extinction.     

均布压力作用下厚壁圆管弯矩计算方法的探讨

建立了厚壁圆管弯矩计算公式，通过分析的均布压力作用下厚壁圆管与薄壁圆管压力相对误差，给出了厚壁圆管与薄壁圆管分类原则，了解和掌握这一原则对工程师大有禅益。     

Correction for photon attenuation in SPECT: analytical framework, average attenuation factors, and a new hybrid approach

We provide a unified framework for the investigation of convergence properties of the iterative algorithms for photon attenuation correction in SPECT, including the iterative Chang method--a commonly used approach in which an average attenuation factor calculated over all projection angles is employed in a pointwise correction scheme. A new average attenuation factor calculated along the projection line is introduced, which can compensate exactly for the attenuation effect in the case of a uniform activity distribution. We propose a new hybrid approach in which we use this new average attenuation factor initially and then shift to the iterative Chang method in later iterations. This hybrid approach was evaluated in a simulation study by use of a computer-generated phantom with both non-uniform activity and non-uniform attenuation distributions. The results demonstrate that this hybrid approach improves the convergence speed of the iterative Chang method and produces reconstructed images of high quality.     

用EVA复配物改善高含蜡原油低温流动性的研究

本文研究了采用化学处理剂改善南海高含蜡原油的低温流动性,结果表明,添加150ppm EVA复合化学处理剂,原油低温流动性得到明显改善,凝固点由32℃降至11.5℃,表观粘度降低86.9%,1;℃时屈服值降低98%。同时考察了添加温度,冷却速度以及化学处理剂的化学组成和结构对改善原油低温流动性的影响。根据南海高含蜡原油中蜡的组成和正构烷烃的碳数分布及其对不同结构的EVA的感受性,讨论了化学处理剂改善原油低温流动性的机理,指出,EVA中乙烯链长与原油中正构烷烃链长相近时才能形成共晶,起到改变原油中蜡的结晶形态的作用,达到降凝减粘效果。     

Glass-ceramics of barium strontium titanate for high energy density capacitors

Barium strontium titanate glass-ceramics were successfully produced with one major crystalline phase when Al₂O₃ was added to the melt. A dielectric constant of 1000 and a breakdown strength of 800 kV/cm was achieved; however the energy density was only measured to be 0.3–0.9 J/cm³. These energy density values were lower than anticipated due to the presence of dendrites and pores in the microstructure. Using BaF₂ as a refining agent improved the microstructure and doubled the energy density for BST 80/20 samples. However, no refining agent reduced the increasing amount of hysteresis that developed with increasing applied electric field. This phenomenon is believed to be due to interfacial polarization.