MINERALOGICAL, PORE AND PETROPHYSICAL CHARACTERISTICS OF THE DEVONIAN JAUF SANDSTONE RESERVOIR, HAWIYAH FIELD, EASTERN SAUDI ARABIA

Throughout the subsurface of the Arabian Peninsula, the approximately 460ft thick, Devonian Jauf Formation generally consists of well-compacted, low-porosity sandstones and shales, but it also includes friable and highly porous sandstones which form significant gas and condensate reservoir intervals. The mineralogy and pore properties of these reservoir intervals at the Hawiyah field (part of the giant Ghawar structure) were studied by integrating petrographic data with petrophysical measurements of reservoir sandstone samples.
The reservoir sandstones are mainly composed of quartz arenites containing small amounts of altered potassium feldspar grains, authigenic illite and chlorite. Based on the pore types, which reflect the habits of the intergranular clays, three reservoir sandstone types have been defined: Type A, characterized by macroporosity; Type B, with microporosity; and Type C, with combined laminations of Types A and B. The dominance of pore-lining clay (as in Type A) or pore-filling clay (as in Type B) is the principal factor controlling the petrophysical properties of the samples. Types A and C sandstones contain macro pores, but irreducible water saturation is high (25 to 45%) compared to clean samples elsewhere, because of the presence of micropores associated with clay. In Type B sandstones the irreducible water saturation is commonly greater than 40% because all the pores spaces are in the microporosity range. The irreducible water saturation in Type B sandstones increases rapidly as porosity decreases. When porosity is less than 10%, the corresponding permeability is 0.2 mD, but no economic production can be expected because water saturation is as high as 100%. In the producing intervals, authigenic clays result in low electrical resistivity due to high water saturation; however, water-free gas is produced.     

Encapsulation and Ostwald Ripening of Au and Au–Cl Complex Nanostructures in Silica Shells

We report a general template strategy for rational fabrication of a new class of nanostructured materials consisting of multicore shell particles. Our approach is demonstrated by encapsulating Au or Pt nanoparticles in silica shells. Other superstructures of these hollow shells, like dimers, trimers, and tetramers can also be formed by nanoparticle‐mediated self‐assembly. We have also used the as‐prepared multicore Au–silica hollow particles to perform the first studies of Ostwald ripening in confined microspace, in which chloride was found to be an efficient mediating ligand. After treatment with aqua regia, Au–Cl complex is formed inside the shell, and is found to be very active under in situ transmission electron microscopy observations while confined in a microcell. This aspect of the work is expected to motivate further in situ studies of confined crystal growth.     

Improved homogenization of Ni in sintered steels through the use of Cr-containing prealloyed powders

The homogenization of Ni in powder metal (PM) steel compacts is usually difficult even after high-temperature sintering at 1250°C. An earlier study by the authors demonstrated that this problem can be alleviated through the addition of 0.5 wt pct Cr in the form of stainless steel powders. To further improve the microstructure and mechanical properties of Ni-containing PM steels and to understand the mechanisms, an attempt was made in this study using the Fe-3Cr-0.5Mo prealloyed powder as the base material. The results showed that the distribution of the Ni additives was significantly improved. As a result, the tensile strength of the Fe-3Cr-0.5Mo-4Ni-0.5C compact sintered at 1250°C reached 1323 MPa. The elongation was higher than 1 pct. These sinter-hardened properties, which were attained using a slow furnace cooling rate, were comparable to those of the sinter-hardened alloys reported in the literature using accelerated cooling and were equivalent to those of the best quenched-and-tempered alloys registered in the Metal Powder Industries Federation (MPIF) standards. These improvements were attributed to the positive effect of Cr addition on alloy homogenization due to the reduction of the repelling effect between Ni and C, as was demonstrated through the thermodynamic analysis using the Thermo-Calc program.     

Sensor guided handling and assembly of active micro-systems

Positioning accuracies in the range of a few micrometers and below are necessary for the assembly of active micro-systems. In order to reach these accuracies, an assembly system for sensor guided micro-assembly is developed in the Collaborative Research Centre 516 “Design and manufacturing of active micro-systems”. The combination of a parallel robot with an integrated 3D vision sensor and a micro-gripper enables to reach relative positioning accuracies below 1 μm.     

Comprehensive heat exchange model for a semiconductor laser diode

By measuring the total energy flow from an optical device, we can develop new design strategies for thermal stabilization. Here we present a comprehensive model for heat exchange between a semiconductor laser diode and its environment that includes the mechanisms of conduction, convection, and radiation. We perform quantitative measurements of these processes for several devices, deriving parameters such as a laser's heat transfer coefficient, and then demonstrate the feasibility of thermal probing for the nondestructive wafer-scale characterization of optical devices.     

Experimental studies of the bond response of three-wire strands and some influencing parameters

The bond behavior of prestressing strands is of great importance for the capacity of precast prestressed concrete structures. In the present study, the bond behavior of three-wire strands, and some influencing parameters, were examined by means of steel encased pull-through and push-in tests. The three mechanisms: adhesion, friction and other mechanical actions were found to be present at the strand-concrete interface at different slip values. The results from the experiments showed that the micro roughness of the strand surface strongly affected the initial bond response of the strand, that is the adhesion in the interface. The maximum bond capacity of indented three-wire strands was found to be directly connected to the geometric properties of the strand indents. The influence of the concrete strength on the bond capacity of the strand was hard to interpret. However, the density of the concrete matrix was found to be a better parameter for determine the influence of the concrete rather than the compressive strength.     

Understanding silica-supported metal catalysts: Pd/silica as a case study

Supported metal catalysts, particularly noble metals supported on SiO₂, have attracted considerable attention due to the importance of the silica–metal interface in heterogeneous catalysis and in electronic device fabrication. Several important issues, e.g., the stability of the metal–oxide interface at working temperatures and pressures, are not well-understood. In this review, the present status of our understanding of the metal–silica interface is reviewed. Recent results of model studies in our laboratories on Pd/SiO₂/Mo(1 1 2) using LEED, AES and STM are reported. In this work, epitaxial, ultrathin, well-ordered SiO₂ films were grown on a Mo(1 1 2) substrate to circumvent complications that frequently arise from the silica–silicon interface present in silica thin films grown on silicon.     

High-resolution images from low-resolution compressed video

Surveys the field of super resolution (SR) processing for compressed video. The introduction of motion vectors, compression noise, and additional redundancies within the image sequence makes this problem fertile ground for novel processing methods. In conducting this survey, though, we develop and present all techniques within the Bayesian framework. This adds consistency to the presentation and facilitates comparison between the different methods. The article is organized as follows. We define the acquisition system utilized by the surveyed procedures. Then we formulate the HR problem within the Bayesian framework and survey models for the acquisition and compression systems. This requires consideration of both the motion vectors and transform coefficients within the compressed bit stream. We survey models for the original HR image intensities and displacement values. We discuss solutions for the SR problem and provide examples of several approaches.     

High slew-rate CMOS operational amplifier

A 0.8 /spl mu/m CMOS operational amplifier configuration with a slew rate in excess of 2 V/ns and a unity gain bandwidth of 55 MHz with a load capacitance of 15 pF is proposed. This employs a dynamic technique that turns on a large current source when the rate of change of input is larger than a pre-decided value.