乳化钻井液条件下高温高压气井气体扩散研究

高温高压下甲烷在油里的溶解度大，水包油乳化钻井液中存在油相，钻井作业中钻井液静置期间如起下钻、工具故障抢修等时间过长，储层中的甲烷气体会扩散到井眼里。在钻高含硫化氢及二氧化碳气井时，高温高压条件下天然气更有可能到达与油完全互溶的状态。文章将储层内的水平段井眼的气体扩散区域划分为4个区，外滤饼区、内滤饼区、滤液滞留区、滤液未污染区，根据外滤饼区、内滤饼区、滤液滞留区不同计算参数条件，计算预测了在使用水包油乳化钻井液情况下，储层中天然气通过扩散穿过3个区后，进入储层内井眼段环空导致的环空含气质量浓度变化，对环空内含气质量浓度随扩散时间、含油浓度因素的变化进行了定量计算。用伽略金有限元方法求解，计算表明，气体扩散量随钻井液静置时间延长而增加，水基钻井液加入油后与不加油的钻井液相比增大了气体扩散量。     

动感像素全息母版图案的设计制作研究

本文介绍了一种新颖的数码像素全息高速拍摄装置来实现全息母版的制作。提出和介绍了运用Photoshop软件一些特殊的图像处理功能设计制作动感像素全息图的方法,并结合多种防伪技术,使产生的图案具有不可仿制的图形畸变特点,并列举了设计实例。     

干涉型激光直写技术用于光盘防伪

利用作者研制的干涉型激光直写系统，阐述了干涉型激光直写设计OVD的方法，防伪特征，介绍了应用于光盘防伪的OVD技术和应用前景，给出了实验结果。     

高酸原油脱酸工艺技术研究

介绍了一种原油脱酸工艺方法。研究了温度、时间对高酸原油脱酸的影响,脱酸温度大于 260℃,脱酸反应较快。分析了高酸原油脱酸前后馏分酸值的变化,脱酸反应对130℃以上各馏分酸值降低都较多,180℃以上馏分脱酸率在80％以上。     

炼油厂碱性污水生物催化氧化预处理工艺研究

在对炼油厂碱性污水水质分析的基础上,提出采用生物催化氧化工艺对碱性污水进行预处理。试验结果表明,在水力停留时间为4 h,曝气量(标准状态)为8 m3／h的条件下,碱性污水的硫化物去除率可达90％以上,出水中的硫化物平均值为15．2 mg/L,CODCR、酚和油的去除率分别为47．5％,44．1％,50．8％,其中CODCR体积负荷为3．85 kg／(m3·d),是传统生化处理的10倍, 达到了污水预处理的目的。     

复合固体超强酸SO42-/Fe2O3-γ-Al2O3催化合成丁酸丁酯

采用沉淀硫酸化法制备了复合固体超强酸催化剂SO2-4/Fe2O3-γ-Al2O3,确定了其最佳制备工艺条件:硫酸浸渍浓度为0.6 mol/L,浸渍时间4 h;焙烧温度550℃,焙烧时间3 h.并采用该催化剂合成丁酸丁酯,考察了物料配比、催化剂用量和反应时间对酯化反应的影响,确定了丁酸丁酯的最佳合成条件:丁醇与丁酸摩尔比为1.4:1,催化剂用量0.9%(以反应物质量计),回流条件下反应3.0 h,在此最佳合成条件下,酯化率可达95.6%.     

Profile-Driven Component Placement for Cluster-Based Online Services

The growth of the Internet and of various intranets has spawned a wealth of online services, most of which are implemented on local-area clusters using remote invocation (for example, remote procedure call/remote method invocation) among manually placed application components. Component placement can be a significant challenge for large-scale services, particularly when application resource needs are workload dependent. Automatic component placement has the potential to maximize overall system throughput. The key idea is to construct (offline) a mapping between input workload and individual-component resource consumption. Such mappings, called component profiles, then support high-performance placement. Preliminary results on an online auction benchmark based on J2EE (Java 2 Platform, Enterprise Edition) suggest that profile-driven tools can identify placements that achieve near-optimal overall throughput.     

Monte Carlo simulation of gas phase polymerization of 1,3‐butadiene. Part II: Kinetics optimization and confirmation

Studies on the deactivations and initiations of gas phase polymerizations of 1,3‐butadiene have been achieved by Monte Carlo simulation. Initiation and deactivation control the reaction before and after the peak of the polymerization rate, respectively. The influence of polymerization temperature has been studied. Monte Carlo modeling of polymerization kinetics and mechanism was confirmed by the agreement of experimental data and simulation results of polymerizations run with a temporary evacuation of monomer. The balance of catalysts and active chains is established by both initiation and chain transfer reactions with cocatalyst, which causes a ‘pseudo‐stability’ stage. © 2003 Society of Chemical Industry     

Characteristics of low-leakage deep-trench diode for ESD protection design in 0.18-/spl mu/m SiGe BiCMOS process

This paper proposes a novel low-leakage BiCMOS deep-trench (DT) diode in a 0.18-/spl mu/m silicon germanium (SiGe) BiCMOS process. By means of the DT and an n/sup +/ buried layer in the SiGe BiCMOS process, a parasitic vertical p-n-p bipolar transistor with an open-base configuration is formed in the BiCMOS DT diode. Based on the two-dimensional (2-D) simulation and measured results, the BiCMOS DT diode indeed has the lowest substrate leakage current as compared to the conventional p/sup +//n-well diode even at high temperature conditions, which mainly results from the existence of the parasitic open-base bipolar transistor. Considering the applications of the diode string in electrostatic discharge (ESD) protection circuit designs, the BiCMOS DT diode string also provides a good ESD performance. Owing to the characteristics of the low leakage current and high ESD robustness, it is very convenient for circuit designers to use the BiCMOS DT diode string in their IC designs.     

以3D软件应用为中心的设计管理模式——PDS在配管设计中的应用

由PDS的特点入手,结合工程实践的应用情况,阐明了3D软件可以更广泛的应用于配管的设计中,强调了以3D模型为中心开展设计和管理的新模式.