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51.
对癸二酸二甲酯与1,2,2,6,6-五甲基哌啶醇的酯交换反应进行了研究;分别考察了四异丙基钛酸酯、氨基锂、氧化二辛基锡3种催化剂的性能;采用氢核磁共振确定了产物的结构;考察了以四异丙基钛酸酯为催化剂时反应温度、反应时间、原料配比和催化剂用量对反应的影响。实验结果表明,四异丙基钛酸酯催化剂的催化效果最好;在癸二酸二甲酯与1,2,2,6,6-五甲基哌啶醇摩尔比1∶1.79、四异丙基钛酸酯催化剂的用量为反应物总质量的0.31%、反应温度180℃、反应时间6h的条件下,所得产物中单(1,2,2,6,6-五甲基-4-哌啶基)癸二酸甲酯(简称单酯)质量分数为23%和双(1,2,2,6,6-五甲基-4-哌啶基)癸二酸酯(简称双酯)质量分数为73%,单双酯质量比为1∶3.17,产物收率为93.3%。该方法可得到理想的单双酯比例及产物收率,具有很好的工业应用前景。 相似文献
52.
Xiang Cao Sheng Zhong 《Communications Letters, IEEE》2006,10(8):580-581
Lin et al., (2003) proposed a remote user authentication scheme for multi-server architecture. In this paper, we breaks this scheme by giving an attack. Our attack allows an adversary to impersonate any user in the system, as long as a single authentication message of that user is observed. 相似文献
53.
主要介绍了2003年EAGE岩石物性测试分析技术取得的新进展。从本届年会看,岩石物理内容主要涉及岩石物理模型建立、时延地震岩石物理与岩石各向异性分析、喷射频率和流体饱和度及其分布预测、岩石物理模拟等新方法、新技术、新成果。在充分考虑岩石物理受当地地质因素影响后,提出岩石物理模版概念,目的是为地质专家方便对岩性和流体的解释提供一种工具。 相似文献
54.
H. L. Du S. R. Rose Z. D. Xiang P. K. Datta X. Y. Li 《Materialwissenschaft und Werkstofftechnik》2003,34(4):421-426
The oxidation/sulphidation behaviour of a Ti‐46.7Al‐1.9W‐0.5Si alloy with a TiAl3 diffusion coating was studied in an environment of H2/H2S/H2O at 850oC. The kinetic results demonstrate that the TiAl3 coating significantly increased the high temperature corrosion resistance of Ti‐46.7Al‐1.9W‐0.5Si. The SEM, EDX, XRD and TEM analysis reveals that the formation of an Al2O3 scale on the surface of the TiAl3‐coated sample was responsible for the enhancement of the corroison resistance. The Ti‐46.7Al‐1.9W‐0.5Si alloy was also modified by Nb ion implantation. The Nb ion implanted and as received sampels were subjected to cyclic oxidation in an open air at 800oC. The Nb ion implantation not only increased the oxidation resistance but also substantially improved the adhesion of scale to the substrate. 相似文献
55.
Performance limitation due to statistical Raman crosstalk in a WDM system with multiple-wavelength bidirectionally pumped Raman amplification 总被引:1,自引:0,他引:1
A general theoretical model of statistical Raman crosstalk and its impact on system performance in a multiwavelength bidirectionally pumped Raman fiber amplifier (RFA) is developed for the first time, where we have taken modulation statistics, dispersion-induced pulse walk-off and signal-induced pump depletion into account. Two kinds of statistical Raman crosstalk, from signal-induced forward-pump depletion and from signal-signal Raman interaction, are included in one model. Formulas for normalized Raman crosstalk, Raman crosstalk-induced relative intensity noise spectral density, and its variance and system performance impact in terms of Q penalty are presented for both a single-span system and a dispersion-compensated multispan wavelength-division-multiplexed (WDM) link. Based on these formulas, we numerically investigate the impact of Raman crosstalk on system performance in a three-wavelengths bidirectionally pumped 40 /spl times/ 40-Gb/s WDM system for various fiber types. In addition, Raman crosstalk in a four-wavelength bidirectionally pumped RFA was experimentally measured. The results agree well with our theory. 相似文献
56.
求解二维结构-声耦合问题的一种直接方法 总被引:1,自引:1,他引:0
本文基于传递矩阵法(TMM)和虚拟边界元法(VBEM),提出了一种求解在谐激励作用下二维结构-声耦合问题的直接法。文中对任意形状的二维弹性环建立了一阶非齐次运动微分方程组,便于用齐次扩容精细积分法求解,对于含有任意形状孔穴的无穷域流体介质的Helmholtz外问题,采用复数形式的Burton-Miller型组合层势法建立了虚拟边界元方程,保证了声压在全波数域内存在唯一解。根据叠加原理并结合最小二乘法,提出了一种耦合方程的直接解法,由于该方法不存在迭代过程,因而具有较高的计算精度和效率。文中给出了二个典型弹性环在集中谐激励力作用下声辐射算例,计算结果表明本文方法较通常采用的混合FE/BE法更为有效。 相似文献
57.
Quality of service (QoS) support for multimedia services in the IEEE 802.11 wireless LAN is an important issue for such WLANs
to become a viable wireless access to the Internet. In this paper, we endeavor to propose a practical scheme to achieve this
goal without changing the channel access mechanism. To this end, a novel call admission and rate control (CARC) scheme is
proposed. The key idea of this scheme is to regulate the arriving traffic of the WLAN such that the network can work at an
optimal point. We first show that the channel busyness ratio is a good indicator of the network status in the sense that it
is easy to obtain and can accurately and timely represent channel utilization. Then we propose two algorithms based on the
channel busyness ratio. The call admission control algorithm is used to regulate the admission of real-time or streaming traffic
and the rate control algorithm to control the transmission rate of best effort traffic. As a result, the real-time or streaming
traffic is supported with statistical QoS guarantees and the best effort traffic can fully utilize the residual channel capacity
left by the real-time and streaming traffic. In addition, the rate control algorithm itself provides a solution that could
be used above the media access mechanism to approach the maximal theoretical channel utilization. A comprehensive simulation
study in ns-2 has verified the performance of our proposed CARC scheme, showing that the original 802.11 DCF protocol can
statically support strict QoS requirements, such as those required by voice over IP or streaming video, and at the same time,
achieve a high channel utilization.
Hongqiang Zhai received the B.E. and M.E. degrees in electrical engineering from Tsinghua University, Beijing, China, in July 1999 and January
2002 respectively. He worked as a research intern in Bell Labs Research China from June 2001 to December 2001, and in Microsoft
Research Asia from January 2002 to July 2002. Currently he is pursuing the PhD degree in the Department of Electrical and
Computer Engineering, University of Florida. He is a student member of IEEE.
Xiang Chen received the B.E. and M.E. degrees in electrical engineering from Shanghai Jiao Tong University, Shanghai, China, in 1997
and 2000, respectively, and the Ph.D. degree in electrical and computer engineering from the University of Florida, Gainesville,
in 2005. He is currently a Senior Research Engineer at Motorola Labs, Arlington Heights, IL. His research interests include
resource management, medium access control, and quality of service (QoS) in wireless networks. He is a Member of Tau Beta
Pi and a student member of IEEE.
Yuguang Fang received a Ph.D degree in Systems and Control Engineering from Case Western Reserve University in January 1994, and a Ph.D
degree in Electrical Engineering from Boston University in May 1997.
From June 1997 to July 1998, he was a Visiting Assistant Professor in Department of Electrical Engineering at the University
of Texas at Dallas. From July 1998 to May 2000, he was an Assistant Professor in the Department of Electrical and Computer
Engineering at New Jersey Institute of Technology. In May 2000, he joined the Department of Electrical and Computer Engineering
at University of Florida where he got the early promotion with tenure in August 2003 and has been an Associate Professor since
then. He has published over one hundred (100) papers in refereed professional journals and conferences. He received the National
Science Foundation Faculty Early Career Award in 2001 and the Office of Naval Research Young Investigator Award in 2002.
He is currently serving as an Editor for many journals including IEEE Transactions on Communications, IEEE Transactions on
Wireless Communications, IEEE Transactions on Mobile Computing, and ACM Wireless Networks. He is also actively participating
in conference organization such as the Program Vice-Chair for IEEE INFOCOM’2005, Program Co-Chair for the Global Internet
and Next Generation Networks Symposium in IEEE Globecom’2004 and the Program Vice Chair for 2000 IEEE Wireless Communications
and Networking Conference (WCNC’2000). 相似文献
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