先进封装电镀中活性边界层的减薄

晶圆表面如果有一层薄且均匀的流体边界层,将有助于克服光刻图形带来的挑战,得到更均匀的金属沉积层。     

High-performance soft x-ray spectromicroscopy beamline at SSRF

The Shanghai Synchrotron Radiation Facility (SSRF) is the first third-generation synchrotron facility in China and operated at an electron energy of 3.5 GeV. One of the seven beamlines in the first construction phase is devoted to soft x-ray spectromicroscopy and is equipped with an elliptically polarized undulator light source, a plane grating monochromator, and a scanning transmission x-ray microscope end station. Initial results reveal the high performance of this beamline, with an energy resolving power estimated to be over 10,000 at the argon L-edge and a spatial resolution better than 30 nm.     

侧限状态下高压实高庙子膨润土非饱和渗透性的试验研究

高放废弃物深地质处置库中,由高压实膨润土形成的人工屏障,起着阻障围岩中地下水渗入内库并引起核素迁移以及库内高放废物的辐射扩散的作用。因此,有必要研究侧限状态下高压实膨润土的非饱和渗透性能。采用瞬时截面法试验研究了侧限状态下高压实高庙子膨润土的非饱和渗透特性。结果表明:侧限状态下,干密度为1.7g/cm3的高压实高庙子膨润土的非饱和渗透系数,数值为1.13×10-13～8.41×10-15m/s,且与土中吸力呈非单一增减关系。当土中吸力约为68MPa时,非饱和渗透系数最小;吸力大于68MPa时,其非饱和渗透系数随着吸力的增加而增加;而当吸力小于68MPa时,非饱和渗透系数随着土中吸力的增加而减小。     

云芝多糖提取工艺的优化及其性能研究

采用超声波提取法,选取溶剂、超声时间、温度、pH作为提取因素,进行单因素实验和L9(34)正交实验,来优化云芝多糖的提取工艺,探讨在常见食品添加剂、常见饮料、一些重金属离子等存在下对云芝多糖稳定性的影响,并对云芝多糖进行了体外抗氧化活性研究。结果表明,云芝多糖的最佳提取条件为以2%的Na2CO3溶液为提取介质,温度45℃,pH为8.5,超声时间50 min,提取率可高达13.87%,云芝多糖在常见食品添加剂、碳酸饮料、苏打水等介质中稳定性较好,云芝多糖对羟基自由基具有较好清除能力,云芝多糖有良好的开发应用价值。     

PARAMETRIC MATCHING SELECTION OF MULTI-MEDIUM COUPLING SHOCK ABSORBER

To achieve the dual demand of resisting violent impact and attenuating vibration in vibration-impact-safety of protection for precision equipment such as MEMS packaging system, a theoretical mathematical model of multi-medium coupling shock absorber is presented. The coupling of quadratic damping, linear damping, Coulomb damping and nonlinear spring are considered in the model. The approximate theoretical calculating formulae are deduced by introducing transformation-tactics. The contrasts between the analytical results and numerical integration results are developed. The resisting impact characteristics of the model are also analyzed in progress. In the meantime, the optimum model of the parameters matching selection for design of the shock absorber is built. The example design is illustrated to confirm the validity of the modeling method and the theoretical solution.     

水文基本建设项目资金支付进度控制的影响因素与措施

近年来,水文基本建设项目多、投资量大,工程建设进度和投资完成进度受自然、人为等多方面因素影响,如何保证按期完成工程建设,保证工程建设资金支付进度满足要求,笔者在从事水文基建项目管理过程中进行了探索和尝试,分析了制约资金支付进度的不利因素,提出了有针对性的措施。     

Comparision Between Main TransportMethods Underground

ＣｏｍｐａｒｉｓｉｏｎＢｅｔｗｅｎＭａｉｎＴｒａｎｓｐｏｒｔＭｅｔｈｏｄｓＵｎｄｅｒｇｒｏｕｎｄＬｉＳｈａｎＸｕＪｉｃｈａｎｇ（ＤｅｐａｒｔｍｅｎｔｏｆＭｅｃｈａｎｉｃａｌＥｎｇｉｎｅｅｒｉｎｇ,ＫｕｎｍｉｎｇＵｎｉｖｅｒｓｉｔｙｏｆＳｃｉｅｎｃｅ...     

Enhanced removal of phosphate from water by fabricating a novel dual metal MIL-101(Fe/Zr)

Metal-based compounds are promising adsorbents for phosphate.A novel dual metal-organic framework as an effective adsorbent for phosphate was synthesized by a solvothermal method.The structure analysis revealed that the as-prepared adsorbent (denoted as MIL-101(Fe/Zr)) possessed a porous polyhedral structure with a large specific surface area of 479.1 m2/g and a pore width of 3.4 nm.The X-ray diffraction pattern and Fourier transform infrared spectra suggested that the MIL-101(Fe/Zr) shared a similar structure with MIL-101(Fe),implying successful incorporation of Zr atoms as a second metal into the MIL-101(Fe) structure.Kinetic adsorption of PO43—by MIL-101(Fe/Zr) conformed to the pseudo-second-order model and intraparticle diffusion model,while adsorption isotherm fitted the Freundlich model well (R2=0.978 5).It is suggested that such an adsorption belonged to multiply-layer adsorption.The adsorption capacity of MIL-101(Fe/Zr) was to be 66.00 mg/g.MIL-101(Fe/Zr) performed well at a wide range of pH 2.0~10.0 and high ionic strength (0~40 mg/L NaCl).A structural analysis indicated that the complexation interaction was mainly responsible for PO43—adsorption.These findings can inspire preparation of other dual metal MOFs adsorbent for phosphate removal and recovery from water.     

Eu3+激活的碱土金属钼酸盐荧光粉合成及其发光性质

采用高温固相反应法制备了CaMoO4：Eu,A（A=Li,Na,K）系列和MMoO4：Eu,Li（M=Ca,Sr,Ba,Mg）系列的发光材料,并采用X射线衍射,荧光光谱对这2个系列发光材料的结构及其发光性质进行了对比研究．结果表明,CaMoO4：Eu,A（A=Li,Na,K）系列荧光粉具有相同的结构,均属于四方晶系,具有相似的光谱性质,碱金属离子为Li时发光性能最好．MMoO4：Eu,Li（M=Ca,Sr,Ba,Mg）系列荧光粉中,MgMoO4：Li,Eu为单斜晶系,底心结构,其他3种荧光粉为四方晶系,体心结构．在395nm近紫外光激发下,CaMoO4：Eu,Li发光性能最好．     

《墨子閒詁》题名疏证

《墨子閒詁》是孙诒让一生最重要的学术成果,不仅集清代墨学研究之大成,更是推动近代以来墨学研究尤其是中国古代逻辑研究空前发展的文本基础。近百年来,中华汉字经历了多次的简化和改革,致使很多学术文本的简化版本和原著繁体版本之间产生理解上的差异,《墨子閒詁》就是最好的例证。该著作的简化版在当前存在两个不同的、使用率都很高的版本：《墨子閒詁》《墨子间诂》。就此,通过辨析简体字和繁体字、通假字和异体字的演变,对出现的这种现象从语形、语义、语用上进行合理解释;然后通过考证原作者署此书名时的真实意旨,还原《墨子閒詁》的本义,并给出其简体版本的合理答案：《墨子间诂》。