水基Fe3O4磁流体的制备工艺研究

用共沉淀法制备Fe3O4磁流体,总结出用十二烷基磺酸钠与聚乙二醇作为表面活性剂制备水基磁流体的合适条件:(1)反应温度为室温或不高于35℃;(2)表面活性剂十二烷基磺酸钠的最佳用量为0.0030～0.0040 g/80 mL;(3)第一次包裹的最佳pH为9～10;(4)聚乙二醇作为第二次包裹的表面活剂时,体系最佳温度为40℃左右;(5)表面活性剂聚乙二醇的最佳用量为0.0050～0.0060 g/80 mL。通过实验制得了能稳定存在180 d的水基磁流体。并用透射电镜、红外光谱、分光光度计、古埃磁天平等进行了初步表征。     

Thermal analysis of styrene–alkyl methacrylate polymers. I. Glass transition temperatures

The glass transition temperatures (T_g's) of several polystyrenes and styrene–alkyl methacrylate copolymers and terpolymers were measured using thermomechanical analysis (TMA) and differential scanning calorimetry (DSC). The polymers studied had number-average molecular weights from 3000 to 250,000 g/mole. The results indicate that the composition dependence of the T_g's for the copolymers and terpolymers can be satisfactorily described by a general Fox equation. In general, the measured T_g's of the copolymer and terpolymer samples depend more on the steric effects of the constituent pendent groups than on their molecular weights. The chain flexibility rather than the size of the pendent group is the determining factor in the glass transition properties of the styrene polymers.     

Possible Energy Network with polygeneration system and CCS for China

On basis of adopting polygeneration systems for power and alternative fuels,capturing CO2 with near zero energy penalties,and storing CO2 on sites,a new kind of Energy Network can integrate energy utilization,CO2 capture,transportation and storage synthetically.Techno-economic analysis of this solution focusing on Inner Mongolia and the Yangtze River Delta districts had been carried with comparison to the chain method for energy utilization and CO2 sequestration.This solution can save 21.5% of energy,and re...     

图书馆的建筑设计格局与图书馆的管理思考

图书馆的建筑设计首要考虑的就是图书馆的管理。数字化图书馆的建设已经来临,我们从唐宋以前的宫廷藏书建筑、明代皇家藏书建筑、清代皇家藏书建筑、私人藏书楼及现代图书馆的藏书建筑格局来比较现在的高校图书馆的建筑设计格局。因而深入、系统地研究图书馆建筑功能、空间的组成及空间布局结构的变化和发展;归纳、总结高校图书馆建筑的设计理念和方法。通过这些研究,把从中得到的启发、经验运用于实践,图书馆建筑设计格局真正地服务于教学、科研,为中国高等教育事业的发展做出应有的贡献。     

当代教育理念与模式下的职业技术学院设计——以鹤壁职业技术学院新校区规划设计为例

面对社会对职业技术的日益重视,职业技术学校的发展也有了日新月异的变化.试图通过对鹤壁职业技术学院新校区的规划设计与分析,探讨当代教育理念与模式下高等职业技术教育的办学特色和校园文化对规划及建筑设计的影响,从而总结适应职业技术教育的设计理念和方法,塑造具有自身特色和体现城市风貌的职业技术学院.     

Progress and recent trend in MILD combustion

Moderate or intense low oxygen dilution(MILD)combustion plays a significant role in the mitigation of combustion-generated pollutants and greenhouse gases whilst meeting thermal efficiency needs.However,due to the lack of the fundamental knowledge on this combustion,there is a misconception that MILD combustion should be established by high preheating of the air,which has limited its application.Our research and development on this combustion has been performed for several years. We have found that the requ...     

网络融合边界的电信DoS攻击检测*

为了检测网络融合边界的电信拒绝服务攻击,首先针对攻击的类型分别提出了基于呼叫统计或流量信号分析的检测方法,并采用分步骤的策略设计了检测系统,将两种检测算法分别应用于粗检测步骤,再通过精检测步骤确认攻击并找出攻击源.模拟实验结果表明,该方案能够有效地检测出典型的攻击,并能够实时在线检测,具有良好的实用价值,为应对网络融合所带来的新安全问题提供了一种解决方案.     

基于单片机的病房无线呼叫系统设计

为解决传统病房有线呼叫系统存在的布线复杂、易出故障、维修不便、不能在现有床位基础上及时增加新床位信息等问题,提出了无线呼叫系统设计。采用STC89C52系列单片机作为主控芯片,nRF905作为无线收发的核心芯片,并配以相应的LCD显示屏和声光报警器,设计出了无线病房呼叫系统。结果表明,该系统可靠传输距离达90 m以上,具有一定的抗干扰性,且可以临时方便增加床位显示信息,能够满足医院的临时实际需求。该系统性能稳定,操作简便,可以有效代替传统有线呼叫系统。     

阳离子交换树脂催化合成十三碳二元酸二乙酯

以强酸性阳离子交换树脂为催化剂,十三碳二元酸与乙醇为原料合成十三碳二元酸二乙酯,考察了影响反应的因素。结果表明:醇酸摩尔比为4∶1,催化剂用量为酸质量的2%,在3分子筛脱水的情况下反应7 h,酯化率达98.4%,并且催化剂可重复使用3次。