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A series of phosphorus‐containing, wholly aromatic thermotropic copolyesters from acetylated 2‐(6‐oxide‐6H‐dibenz〈c,e〉〈1,2〉oxa phosphorin‐6‐yl)‐1,4‐dihydroxy phenylene, p‐acetoxybenzoic acid, terephthalic acid, and isophthalic acid were prepared by melting polycondensation. The structure and basic properties of the polymers, such as the glass‐transition temperature (Tg), melting temperature (Tm), thermal stability, crystallinity, and liquid crystallinity, were investigated with Fourier transform infrared, elemental analysis, differential scanning calorimetry (DSC), thermogravimetric analysis, wide‐angle X‐ray diffraction, and hot‐stage polarizing optical microscopy. The copolyesters had relatively high Tg values ranging from 183 to 192°C. The Tm values obtained from DSC curves for samples P‐20 and P‐25 were 290 and 287°C, respectively (where the number in the sample name indicates the molar fraction of the phosphorus‐containing monomer in the reactants). The initial flow temperatures of other samples observed with hot‐stage polarizing microscopy were 271–290°C. The 5% degradation temperatures in nitrogen ranged from 431 to 462°C, and the char yields at 640°C were 41–52%. All the copolyesters, except P‐40, were thermotropic and nematic. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 1278–1284, 2002 相似文献
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THERMODYNAMICSANDPHASEEQUILIBRIUMOFCu-Y-O,Cu-Y-S,Cu-Y-O-SLIQUIDSOLUTIONS¥Du,Ting;Li,Guodong(CentralIronandSteelResearchinstit... 相似文献
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文章介绍了煤矿现有的调度电话录音系统,设计了调度电话监控上传系统来实现录音文件的上传和调度电话查询系统实现录音文件的查询和远程回放。系统通过输入查询取代了传统的人工查询的工作方式,大大节约了生产调度成本,同时为煤矿人员考勤和定位也提供了准确依据。由于其配置容易、操作方便、实用性高,因此具有很好的维护性和推广性。 相似文献
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The Journal of Supercomputing - With the wide spread of image information, it is an urgent problem to protect image property rights and crack down on piracy. Watermarking algorithm is an effective... 相似文献
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Liang Zhang Ting Wang Bo Yuan Bin Yu Zhichao Chen 《Advanced Engineering Materials》2023,25(11):2201823
Herein, an innovative powder-cored wire arc additive manufacturing (PC-WAAM) process is proposed to fabricate γ-TiAl thin-walled intermetallic alloy. The metallography, phase composition, and mechanical properties at different thin-wall locations are characterized. The results show that the alternatively distributed layer-like microstructure composed of α2 (Ti3Al) and γ (TiAl) phases is obtained along the building direction. The content of α2 phase exhibits the tendency of decreasing from the bottom to top region. This unique microstructure characteristic is closely related to the typical thermal cycling history during deposition. Moreover, the tensile strength and microhardness of the top region are lower than the middle and bottom region. In general, the current PC-WAAM technique shows promising capability of fabricating γ-TiAl intermetallic alloy with low cost. This work becomes a valuable reference for understanding the evolution mechanism of microstructure and paves the way for the flexible and customized additive manufacturing of γ-TiAl alloy. 相似文献
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Comparison of image reconstruction by using near‐field and far‐field data for an imperfect conductor
Image reconstruction by using near‐field and far‐field data for an imperfectly conducting cylinder is investigated. A conducting cylinder of unknown shape and conductivity scatters the incident wave in free space and the scattered near and far fields are measured. By using measured fields, the imaging problem is reformulated into an optimization problem and solved by the genetic algorithm. Numerical results show that the convergence speed and final reconstructed results by using near‐field data are better than those obtained by using far‐field data. This work provides both comparative and quantitative information. © 2001 John Wiley & Sons, Inc. Int J RF and Microwave CAE 11: 69–73, 2001. 相似文献