Novel one-step route for synthesizing sub-micrometer PSt hollow spheres via redox interfacial-initiated method in inversed emulsion

Interfacial-initiated polymerization of styrene (St) was carried out in inversed emulsion with cumene hydroperoxide (CHPO) and ferrous sulfate (FeSO₄)/disodium ethylenediaminetetraacetate (NaEDTA)/sodium formaldehyde sulfoxylate (SFS) as the redox initiation system. The water-soluble Fe²⁺-NaEDTA-SFS acted as the reducing component and the oil-soluble CHPO as the oxidant component of the redox initiation system. Therefore, the primary radicals were produced mainly at the oil/water interface to initiate the polymerization of St. Thus, sub-micrometer hollow polystyrene (PSt) spheres were obtained by one-stage polymerization, which was supported by the techniques of transmission electron microscopy (TEM) and field emission scanning electron microscopy (FESEM).     

住宅建筑结构中隔震技术的应用和经济评价

对当前隔震系统做了简单介绍 ,介绍了基础隔震的技术和施工方法等。讨论在住宅结构中推广隔震技术的方法 ,对各种类型的住宅结构做经济评价 ,讨论推广的可能性和难点。     

A dynamic programming method for analysis of bridges under multiple moving loads

A dynamic programming (DP) method is presented for analysis of statically determinate and indeterminate bridges subjected to moving loads such as those specified by the American Association of State Highway and Transportation Officials (AASHTO) specifications. These loads consist of uniform lane loading, two-axle truck loading and two-axle truck plus one-axle semitrailer loading. The solution of the DP problem is based on the use of influence line diagrams and extremum functions. Recurrence formulae have been developed for various types of AASHTO live loads. The procedure presented in this article is quite general and can be applied to any type of structures with linear behaviour and any type of moving loads. Six examples are presented: a simply-supported beam, a simply-supported Pratt truss, an arch bridge, a continuous Pratt truss, a continuous frame and a cable-stayed bridge.     

油田放射性作业人员外周血淋巴细胞染色体畸变的观察

本文调查了油田212例受γ射线和中子混合辐射照射的作业人员和30例正常人的外周血淋巴细胞染色体畸变。作业人员受γ射线照射的人均年受照剂量为1.28mGy。调查结果表明,放射性测井人员与正常人相比染色体畸变率有显著差异。     

A new kind of compound solid-state quasi-optical power combiner

In this paper, a new kind of solid-state quasi-optical power combiner is presented. It consists of two or more singlecavity multiple-device power combiners and a Fabry-Perot cavity. The experimenal results using six Gunn diodes at X-band show that the total output power is higher than 400 mW, the total combining efficiency is as high as 83%, and the frequency stability is better than 10^?5.     

基于HMM方法的动态手势轨迹训练性能研究

基于HMM(Hidden Markov Model,隐形马尔可夫模型)对动态手势轨迹的训练是手势识别的关键技术之一。本文对HMM的模型训练采用Baum.Welch算法,并分别从迭代次数,样本个数选取,以及模型初值选取等方面对动态手势轨迹的训练性能进行了研究。实验结果表明HMM方法对具有时空特性的动态手势轨迹识别是非常有效的。     

现场总线技术的特点及其在热电站的应用

阐述了现场总线技术的含义、主要特点和优点,对比了现场总线控制系统与DCS系统的区别,介绍了现场总线技术在洛阳石化分公司热电站的典型应用及其发展前景。     

CO毒化AB5型合金分形特征研究

研究了三种贮氢合金 L a Ni5、L a Ni4 .7Al0 .3、Ml Ni4 .5Al0 .5被 10 0× 10 - 6 CO毒化后的分形特征 ,求出这三种合金在含 10 0× 10 - 6 CO的氢中循环 ,分维分别为 0 .2 5 4 7、0 .170 9、0 .0 72 5。可以较好的解释合金被毒化的宏观现象。     

3-N-丙酰基-2-芳基-5-(3-碘苯基)-1,3,4-(口恶)唑啉类化合物的合成及表征

以3-碘苯甲酸为原料,在浓硫酸作用下与乙醇反应制得3-碘苯甲酸乙酯(1),再以无水乙醇为溶剂,在105℃化合物1与80％的水合肼反应8 h,制得3-碘苯甲酰肼(2)。在无水乙醇中,在90～95℃化合物2分别与4-甲基苯甲醛、2-氯苯甲醛、4-氯苯甲醛、4-羟基苯甲醛、2,4-二氯苯甲醛、4-甲氧基苯甲醛、3-硝基苯甲醛、4-硝基苯甲醛和4-二甲氨基苯甲醛反应得到相应的酰腙[3(a～i)]。最后化合物3(a～i)分别与丙酸酐脱水环化成了3-N-丙酰基-2-芳基-5-(3-碘苯基)-1,3,4-(口恶)唑啉类化合物[4(a～i)],收率分别为86．2％,70．5％, 80．1％,68．2％,62．4％,75．2％,73．2％,70．5％和63．2％。并通过元素分析,IR,1H NMR和MS对化合物4(a～i)的结构进行了表征。