灵芝孢子多糖提取工艺优化

采用响应面分析法对灵芝孢子多糖的提取工艺进行优化。考察3个变量(水料比、超声温度、微波时间)对灵芝孢子多糖提取率的影响,并通过响应面设计法确定灵芝孢子多糖提取技术的最佳工艺条件为水料比20∶1,超声提取时间为55 min,微波(200 W,60℃)提取时间20 min,在此条件下测得多糖的提取率为2.23%。     

超声波法提取魔芋飞粉中神经酰胺的初步研究

主要对超声波法提取魔芋飞粉中神经酰胺进行了初步探索,重点分析了温度、时间、料液比和提取溶剂对神经酰胺粗提物提取率的影响,确定了神经酰胺粗提物最佳提取工艺为温度60℃、时间为35 min、料液比为1∶4、提取溶剂为95%乙醇,神经酰胺粗提物的最高提取率可达2.89%.     

Simultaneous Determination of Abietic Acid and Dehydroabietic Acid Residues in Duck Meat by HPLC-PAD-FLD

Abietic acid (AA) and dehydroabietic acid (DHAA) are major components of rosin, and both of them are well-recognized causes of skin allergy. Rosin was once widely used for removal of duck feathers in China. In the present study, an analytical method was developed for simultaneous determination of AA and DHAA in duck meats. AA and DHAA were extracted with acetonitrile and cleaned by solid-phase extraction, followed by chromatographic separation on C18 column with methanol/2 mM phosphoric acid (86/14, v/v) as mobile phase. AA was detected by photodiode array detection (PAD) at 240 nm, while DHAA was detected by fluorescence detection (FLD) with excitation and emission at 225 and 287 nm, respectively. Limits of quantification for AA and DHAA were 50 and 15 μg/kg, respectively. The method was applied to analysis of AA and DHAA residues in meats of rosin-defeathered ducks and commercial ducks. The results indicated that removal of duck feathers by means of rosin could lead to residues of AA and DHAA in duck skins, and 5 out of 32 commercial ducks were found to be contaminated by AA and DHAA, ranging from 1,556.1 to 9,638.7 μg/kg and 476.4 to 2,623.8 μg/kg, respectively. The proposed method could be used to identify those rosin-defeathered ducks and to monitor the illegal use of rosin in duck processing.     

苦丁茶叶中生物类黄酮及芦丁含量的测定

通过分光光度法测得紫茎女贞芽叶、老叶、粗壮女贞芽叶、老叶生物类黄酮含量分别为:(2.67±0.23)%、(2.08±0.21)%、(3.15±0.18)%、(2.78±0.22)%.采用高效液相色谱法测得2种川产苦丁茶芦丁含量分别为:紫茎女贞芽叶、老叶分别为(0.118±0.011)%,(0.083±0.012)%,粗壮女贞芽叶、老叶(0.082±0.012)%,(0.065±0.008)%.2种川产苦丁茶中生物类黄酮含量丰富,可作为提取生物类黄酮的原料;芦丁含量很低,仅为生物类黄酮的2.3%～4.4%.     

超声辅助提取-高效液相色谱法测定荷叶中的生物碱

采用超声提取法提取荷叶中的O-去甲荷叶碱、N-去甲荷叶碱、荷叶碱和莲碱4种主要的生物碱,建立HPLC分析方法进行评价,为荷叶及相关产品的质量控制提供参考。选用Welch Materials C18色谱柱(250 mm×4.6 mm,5μm),以乙腈-水(含0.1%三乙胺)为流动相进行梯度洗脱,实现了O-去甲荷叶碱、N-去甲荷叶碱、荷叶碱和莲碱4种生物碱的同时基线分离。在0.1～50μg/mL范围内,O-去甲荷叶碱(R=0.999 8)、N-去甲荷叶碱(R=0.999 9)、荷叶碱(R=0.999 8)和莲碱(R=0.999 8)具有良好的线性关系,检出限分别为1.87、2.22、2.34和1.88 ng/mL(S/N=3∶1)。     

Fe~(3+)存在下DO冲击对好氧活性污泥处理制浆中段废水的影响

Fe3+存在下,考察了处理制浆中段废水的好氧活性污泥系统在溶解氧(DO)浓度为0.5mg/L和5.5mg/L冲击7d的处理效果和污泥特性,调整DO浓度为2.0mg/L进行7d的恢复实验,考察处理效果和污泥特性,并与不加铁的空白组对照。在DO浓度为0.5mg/L和5.5mg/L冲击下,加铁组和空白组处理效果均下降,污泥沉降性能变差,加铁组下降幅度小于空白组;恢复实验中,加铁组恢复速度相对较快。与DO浓度为0.5mg/L冲击相比,DO浓度为5.5mg/L冲击对系统的影响较小,但恢复阶段却相对较慢。     

VAV系统最高新风量的控制

介绍了国外ＶＡＶ系统最小新风量的几种控制方法,并对各种方法加以比较。指出稳压控制法和引射风机法是ＶＡＶ系统较好的最小新风量控制方法。     

公共机房数据库管理系统软件设计

按照数据库设计的过程及设计思想介绍微机机房数据库管理系统软件的模块化设计方案。     

采用变频技术替代自动阀控制的节能改造

介绍了采用变频技术自动控制抽风机转速从而改变抽风量,以达到节能的目的。     

基于IP的移动通信协议路由算法分析

因特网应用的快速发展,移动主机用户的不断增加,使得对移动计算机网络的研究显得更为重要。该文分析讨论了基于ＩＰ的移动通信协议的路由算法问题。通过对协议的路由选择格式、地址转换的复杂性、算法的额外开销、以及与Ｐ协议的兼容性和安全性等问题的讨论,着重分析了Ｃｏｌｕｍｈａ建议、Ｓｏｎｙ建议和ＩＥＴＦ建议的路由策略。