AN ENERGY ANALYSIS OF BELT POLISHING PROCESS AND ITS APPLICATIONS TO TIME CYCLE AND TRACKING EFFECTS

Belt polishing is a fine machining process widely used to improve surface texture and to increase wear resistance and fatigue life. Despite the basics of this manufacturing process are not yet well understood, the cycle-time and the belt oscillations frequency are considered as fundamental process variables. In this article, their effects on the surface characterization and on the form aspects are investigated in connection with the principal physical mechanisms activated during the superfinishing operations (cutting, ploughing and sliding). With this aim, an energy approach of the belt polishing process, coupled with SEM observations of the abrasive belt, is introduced. Two belt polishing energetic regimes are identified and then discussed.     

Chemical vapor deposition of pyrolytic carbon on carbon nanotubes: Part 1. Synthesis and morphology

The chemical vapor deposition of the pyrocarbon from a CH₄+H₂ mixture is investigated using nanofilamentous substrates. The process consists of growing carbon nanotubes via a catalytic process, which then are thickened by pyrolytic carbon deposition to reach diameters in the nanometer to micrometer range. A key characteristic of the experimental reactor used was the long length of its isothermal zone, preceded (and followed) by a low thermal gradient zone. This allowed us to investigate the role of the variation of the local gas phase composition, which depends on the post-cracking secondary reactions, and on the quantity and quality of the deposited carbon. The ‘time of flight’ of the reactive species was found to be a leading parameter in the pyrolytic carbon deposition process. Various nanometric and micrometric morphologies, several of which are new, were synthesised and found constituted with an association of different sub-morphologies. The various morphologies, that can be sorted following a factor of morphological complexity, were investigated by scanning electron microscopy.     

Characterization of Palladium Nanoparticles Adsorpt on Polyacrylic Acid Particles as Hydrogenation Catalyst

Palladium particles can be prepared in sizes of a few nanometers from Pd(OAc)₂in the presence of a block copolymer in aromatic unpolar solvents with suitable reducing agents like NaBH₄ or LiAlH₄. After mixing the organic metal solution with a polyacrylic acid (PAA) dispersion of defined concentration and following a crosslinking process with an epoxide, reactive membranes with a well-defined pore diameter were obtained. The catalytic activity of the prepared palladium particles incorporated in the crosslinked PAA network has been proven by the gas phase hydrogenation of propyne in a special membrane reactor.     

Practical Considerations for Recursive DFT Implementation in Numerical Relays

In this paper, practical considerations for recursive Discrete Fourier Transform (DFT) implementation in numerical relays are presented. The DFT filter instabilities which would produce accumulated errors are emphasized. The aspects ruling error accumulation of the estimated magnitude and phase are highlighted. Novel solutions directed for the elimination of error accumulation are proposed and intensively tested. Digital signal processing (DSP) board based test set-up is utilized for the experimental verification. The paper results are valuable for the protection engineers particularly those concerned with the development and implementation of numerical relays     

A neural networks algorithm for data path synthesis

This paper presents a deterministic parallel algorithm to solve the data path allocation problem in high-level synthesis. The algorithm is driven by a motion equation that determines the neurons firing conditions based on the modified Hopfield neural network model of computation. The method formulates the allocation problem using the clique partitioning problem, an NP-complete problem, and handles multicycle functional units as well as structural pipelining. The algorithm has a running time complexity of O(1) for a circuit with n operations and c shared resources. A sequential simulator was implemented on a Linux Pentium PC under X-Windows. Several benchmark examples have been implemented and favorable design comparisons to other synthesis systems are reported.     

Synthesis of oligocaprolactone vinyl ether macromonomers and their use for indomethacin encapsulation in polymer nanoparticles based on polycaprolactone macromonomer–maleic anhydride–N‐vinyl pyrrolidone terpolymers

Oligocaprolactone macromonomers functionalized with vinyl ether have been synthesized by polymerization of ε‐caprolactone in the presence of hydroxy ethyl or butyl vinyl ether and characterised by NMR and Maldi time‐of‐flight mass spectroscopy. These macromonomers have been copolymerized with maleic anhydride and N‐vinyl pyrrolidone to give terpolymers, which have been used to obtain nanoparticles by the phase‐separation‐dialysis method. Previously dissolving indomethacin in the terpolymer solution allows one to encapsulate the drug inside the nanoparticles. Copyright © 2005 Society of Chemical Industry     

A process-tolerant out-of-band blocker rejection technique for SAW-less receivers

In this paper, an active filtering technique is presented which is capable of filtering the out-of-band blockers in wireless receivers. The concept is based on the feedforward cancellation technique where a blocker replica is subtracted at the output of the low-noise amplifier (LNA). In contrast to the previously reported feedforward cancellation methods, exact gain and phase matching are easily obtained in the proposed architecture to produce a highly selective narrowband frequency response at the output of the LNA with wide rejection bandwidth. For the proof of concept, the system is implemented in a 65 nm CMOS technology. It occupies a total area of 0.8 mm² and the current consumption is 24 mA from a 1.2 V supply. The system post-layout simulations showed a blocker rejection of more than 33 dB for blocker signals 100 MHz away from the desired signal when the feedforward path is activated. The noise figure (NF) of the entire system is 3.8 dB that degrades to 5.8 dB when the feedforward path is activated.     

Deficiency of the ATM protein expression defines an aggressive subgroup of B-cell chronic lymphocytic leukemia

The gene mutated in ataxia telangiectasia, ATM, on human chromosome 11q22-q23 is implicated in cell cycle control and DNA repair. Ataxia telangiectasia patients as well as ATM-deficient mice are immune deficient and develop lymphoproliferative disease. Abnormalities in 11q22.3-q23.1 have also been described in B-cell chronic lymphocytic leukemia (B-CLL). We analyzed B-CLL samples for loss of heterozygosity (LOH) using microsatellite markers located at the ATM (D11S2179), mixed-lineage leukemia (MLL; D11S1356), and BCL1 (D11S987) loci, all of which are located around 11q23. Five (14%) of 36 informative cases showed LOH at the ATM gene, and two of these five cases had LOH at the MLL gene. No LOH was detected at the BCL1 locus, and none of the cases showed LOH at the MLL gene without LOH at the ATM gene. Four of these five cases with LOH at the ATM gene were studied for ATM protein expression by Western blot analysis. All four cases lacked ATM protein. An additional 111 cases of B-CLL were studied for expression of ATM protein by Western blot analysis and RIA. Thirty-eight (34%) of these cases showed ATM levels <50% of that seen in normal lymphoid cells. No morphological or immunophenotypic difference was observed between ATM-deficient B-CLL cases and cases with normal ATM expression. However, patients with ATM deficiency had significantly shorter survival times (35.66 versus 97.3 months; P = 0.003) and more aggressive disease, suggesting that ATM is involved in the leukemogenesis of B-CLL. These data also suggest that the ATM gene may play a role in the reported 11q23 abnormality in B-CLL, which also characterizes an aggressive disease.     

Thermal Conductivity of Silicate and Borate Glasses

Thermal conductivities of silicate and borate glasses were determined at 30°C by steady-state methods. From the experimental data, factors representing the contribution of individual oxides (on a weight-percent basis) were calculated by the least-squares method. The experimental thermal conductivities and those calculated from the factors obtained agree fairly well.     

Characterizing the shape of anatomical structures with Poisson's equation

Poisson's equation, a fundamental partial differential equation in classical physics, has a number of properties that are interesting for shape analysis. In particular, the equipotential sets of the solution graph become smoother as the potential increases. We use the displacement map, the length of the streamlines formed by the gradient field of the solution, to measure the "complexity" (or smoothness) of the equipotential sets, and study its behavior as the potential increases. We believe that this function complexity = f(potential), which we call the shape characteristic, is a very natural way to express shape. Robust algorithms are presented to compute the solution to Poisson's equation, the displacement map, and the shape characteristic. We first illustrate our technique on two-dimensional synthetic examples and natural silhouettes. We then perform two shape analysis studies on three-dimensional neuroanatomical data extracted from magnetic resonance (MR) images of the brain. In the first study, we investigate changes in the caudate nucleus in Schizotypal Personality Disorder (SPD) and confirm previously published results on this structure. In the second study, we present a data set of caudate nuclei of premature infants with asymmetric white matter injury. Our method shows structural shape differences that volumetric measurements were unable to detect.