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51.
Summary The diffusion of C.I. direct orange 34(MW=299) and benzoic acid(MW=122) through degraded semicrystalline polyethylene glycol(PEG)/poly(L-lactide)(PLLA) block copolymers with various PEG contents and PEG segment lengths at 37°C was studied by UV-visible spectroscopy, differential scanning calorimetry(DSC), wide angle X-ray diffractometer (WAXS) and scanning electron microscopy(SEM). The influences of the PEG contents, PEG segment lengths and hydrolytic degradation of PEG/PLLA copolymers on the solute diffusion coefficient and mode for transport were investigated. It is concluded that the diffusion rate increases with the increase of PEG contents and PEG segment lengths in PEG/PLLA copolymers. This is understandable that the increase of PEG content and PEG segment length both make the degree of crystallinity decrease. The steady state of mass flux could not be reached at the diffusion times up to 1000 h, because the copolymers underwent hydrolysis reaction during this period. Furthermore, it is understood that the characteristic time of diffusion as defined by the square of film thickness at an instant of time over the diffusion coefficient of solute through polymer decreases with the increasing diffusion time. 相似文献
52.
随着移动通信技术的不断发展,手机的普及率在不断上升,而短信作为传统的移动通信服务,长久以来一直在人们的日常生活中占据着极为重要的位置。可以说,短信在一定程度上记录了人们生活的轨迹。但是,现有的短信管理系统仅对短信进行以联系人为特征分类、以时间为顺序显示的简单非智能化的管理,导致了用户手机中各类短信混杂不清,短信的管理效率极低。通过研究短信的特征,分析传统的基于文档频率的特征值提取方法和基于互信息的特征值提取方法的优势与不足,提出了一种适用于短信的基于词频和互信息的特征值提取方法,并结合短信长度实现了一种改进的贝叶斯分类算法。实验证明,算法在进行短信分类时可以得到相当可观的召回率和准确率。 相似文献
53.
The isothermal cure of an epoxy-novolac molding compound was studied by means of Fourier-transform infrared spectroscopy (FTIR) and dielectrometry (DE). Results obtained were compared with previous differential scanning calorimetric (DSC) observations. The behavior of epoxide conversion (FTIR) measured via FTIR was found similar to (but not exactly coinciding with) the extent of cure (DSC) determined previously by means of DSC. As for the DE analysis, directly measurable properties such as permittivity () and loss factor () varied in a complicated manner during the course of cure, showing strong dependence on both temperature and frequency. Other dielectric parameters (such as ionic conductivity, relaxed permittivity, and characteristic relaxation time) previously suggested in the literature as suitable for cure monitoring purposes were found difficult to determine within the limited frequency range (100 to 104 Hz) here. With some arbitrariness, the relative drop in log (at 100 Hz) was taken as an index (DE) for the extent of cure. It was observed that DE behaves in a manner similar to FTIR and DSC Comments on the application of these three techniques in the characterization of thermosetting systems were given. 相似文献
54.
The UV‐curable urethane‐acrylates based on 2‐hydroxyethyl methacrylate (HEMA)‐terminated polyurethane (PU) for lithographic and coating applications are investigated in this study. Series of PU prepolymers were made from 4,4‐diphenyl methane diisocyanate (MDI), poly(propylene oxide) glycol (PPG 400), poly(butylene adipate)glycol (PBA 500), or poly(tetramethylene oxide) glycol (PTMO 1000) and are terminated with HEMA. The 2,2‐azobisisobutyronitrile (AIBN) was used as a UV‐initiator under air atmosphere. The curing kinetics of HEMA‐terminated PU film were studied. The curing analysis, using FTIR and reaction kinetics, indicate the reaction rate equation correlates well with the film thickness [T], initiator concentration [I], unreacted double bond concentration [C?C], and exposed energy [E] of the reaction system. The kinetic rate equation for the UV‐curable reaction can be written as © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 91: 3162–3166, 2004 相似文献
55.
56.
Wen‐Bin Liau Yu‐Ting Sun Ling‐Yueh Yang Lee‐Yih Wang Wen‐Yen Chiu Kuo‐Huang Hsieh Sheng‐Mao Tseng 《应用聚合物科学杂志》2006,102(6):5406-5413
The polyaniline (PANI)‐coated polystyrene (PS) latexes were synthesized, and the electrically conductive films were prepared thereafter. The weight ratio of PANI was 5%. Thermal analysis of the latices was performed using DSC and TGA. In this study, the electrically conductive films were prepared above the PS glass transition temperature (Tg). During the film formation, the effects of the annealing temperature and atmosphere (air or N2) on the film resistance were investigated. In addition, the film morphology was observed utilizing scanning electron microscopy. The film resistance decreased in the initial heating stage due to the increasing temperature and the compaction of film. Then the film resistance increased with further annealing due to the aging of PANI. Typically, the film resistance was about 6000 Ω/sq, and the conductivity was 0.3 S/cm. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5406–5413, 2006 相似文献
57.
58.
CeO2 particles confined within the pores of an SBA-15 mesoporous silica host were prepared by incipient wetness impregnation (IMP)
and deposition precipitation (DP) methods. The materials were characterized by XRD, N2-adsorption and temperature programmed reduction (TPR) to evaluate the structure, texture, and redox properties. The preparation
procedure had significant impact on the assembling mode of CeO2 inside the SBA-15 mesopores. A high dispersion of CeO2 particles was achieved via DP, whereas the dispersion of CeO2 prepared by IMP was found to be inhomogeneous and CeO2 partially blocked the pores. The CO conversion in the water-gas-shift reaction was enhanced over 1 wt% Pt supported on CeO2-modified SBA-15 obtained by DP. 相似文献
59.
Two surface modification methods—plasma surface treatment and chemical agent treatment—were used to investigate their effects on the surface properties of ultrahigh‐molecular‐weight polyethylene (UHMWPE) fibers. In the analyses, performed using electron spectroscopy for chemical analysis, changes in weight, and scanning electron microscope observations, demonstrated that the two fiber‐surface‐modified composites formed between UHMWPE fiber and epoxy matrix exhibited improved interfacial adhesion and slight improvements in tensile strengths, but notable decreases in elongation, relative to those properties of the composites reinforced with the untreated UHMWPE fibers. In addition, three kinds of epoxy resins—neat DGEBA, polyurethane‐crosslinked DGEBA, and BHHBP‐DGEBA—were used as resin matrices to examine the tensile and elongation properties of their UHMWPE fiber‐reinforced composites. From stress/strain measurements and scanning electron microscope observations, the resin matrix improved the tensile strength apparently, but did not affect the elongation. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 655–665, 2007 相似文献
60.
利用MACD趋势指标与K线形态图进行相互验证技术,改进一般的基于MACD的证券买卖准则。实证结果表明,基于改进后的MACD买卖准则进行证券投机,几乎能使投机者捕捉到每一波段行情,从而获取较高收益。 相似文献