Formation and retention of local melted films in AZ91 friction stir spot welds

The formation of local melted films during friction stir spot welding of as-cast AZ91D and thixomolded AZ91 material is investigated. The average temperatures close to the tip of the rotating pin vary from 438 to 454 °C during the dwell period in friction stir spot welding. These measured temperature values are higher than the melting temperature of α-Mg + Mg₁₇Al₁₂ eutectic (437 °C). It is suggested that the temperature in the stir zone during the dwell period is determined by the relative proportions of α-Mg and (α-Mg + Mg₁₇Al₁₂) eutectic material, which are incorporated during friction stir spot welding. Based on the stir zone temperature measurements and a detailed examination of material located at the root of the pin thread it is suggested that material is moved downwards via the pin thread and into the stir zone during the dwell period in friction stir spot welding. Evidence of local melted film formation is observed in the stir zone of AZ91 spot welds. It is suggested that melted films are retained since their dissolution rate is much slower in the high temperature stir zone than it is when melted films is formed in the stir zone during Al 7075-T6 friction stir spot welding. The spontaneous melting temperature, solute diffusion rate and the thermodynamic driving force for droplet dissolution are much higher during Al 7075-T6 friction stir spot welding.     

合成2,4-二叔丁基苯酚工业试验

以离子交换树脂为催化剂，苯酚和甲基叔丁基醚为原料合成2，4-二叔丁基苯酚(简称2，4酚)，合成产物经过滤再经间歇真空精馏精制提纯，得到高纯度的2，4酚成品。成品精馏后釜中残液在酸性白土催化剂的作用下通过歧化反应生成对叔丁基苯酚，再经精馏提纯得到成品对叔丁基苯酚。通过工艺优化，使2，4酚、对叔丁基苯酚形成联产生产工艺，降低了生产原料消耗和成本。     

吉林闹枝金矿床黄铁矿的标型特征研究

从成因矿物学及找矿矿物学的观点出发，系统地研究了闹枝金矿床黄铁矿的形态、粒度、化学成分、热电性、硫同位素方面的标型特征，为矿床的成因研究和深部远景评价提供了矿物学依据。     

An alternative method to compute the component fractions in the geometrical optical model: visual computing method

A method called visual computing was used to solve angular four-components' proportions and directional vegetation cover fraction for discrete canopies and continuous row-planted plants. It proved effective to predict the angular characteristics on pixel scale. The method could be an alternative way to a classical solution of geometrical optical models. A visual computing method would be effective especially when the canopies' spatial distribution and shapes were irregular and could not be described statistically.     

脉冲电镀最佳参数之探索和优化

本文利用正交实验法对脉冲电镀各控制参数进行试验,对影响分散能力、镀层可靠性及外观质量的各种因素进行探讨,寻找影响外观质量的显著因子并加以控制,同时进一步优化脉冲电镀的工艺参数。     

低发射率材料红外法向发射率谱测量方法的研究

采用热管技术研制了材料发射率谱的专用测量附件;利用双温测量技术,在P-E983型红外分光光度计及3600型数据站上进行了较低温度下低发射率材料红外法向发射率谱测量方法的研究.实测了几种材料的发射率谱;讨论了影响测量误差的诸因素.     

含杂质流体的流量测量

结合工程实例.介绍了几种实用的含杂质流体的流量测量方案,供自动化仪表设计及维堆护人员参考。     

Two-dimensional pentagon quasicrystal in an Al-Co-Ni-Tb alloy obtained by quenching under high static pressure

A transmission electron microscopy study of quasicrystals was carried out in Al-Co-Ni-Tb alloy which was obtained by quenching under high static pressure and a new two-dimensional pentagonal quasicrystal was discovered. An unique five-fold axis is observed in its diffraction patterns and the periodicity along the five-fold axis is 0.4 nm. Another feature of the pentagonal phase is that no extinction exists in the diffraction patterns along the direction perpendicular to the five-fold axis. A comparison of the high resolution electron microscopy images of the pentagonal phase and the decagonal quasicrystal is given. The effect of high pressure is discussed.     

管内含蜡原油降温过程中的放热问题

利用两种管段和两种原油，进行了降温过程自然对流放热参数的测试和研究。采用滞流点确定降温第二阶段中凝油边界的移动，区分管内的对流区与导热区。由实验数据回归得到适用于含蜡原油降温过程的自然对流放热准则方程式。用该方程式计算的自然对流放热系数值比按无限空间自然对流准则方程式计算值小20％～50％。