Duplex positioning method for increasing the fatigue life of threaded connections under eccentric loading

A new method, duplex positioning method DPM, to increase the fatigue lifetime of the threaded connection under eccentric loading is presented. When DPM is applied, the most damaged stud regions periodically are removed from risky positions by a change of the stud’s and nut’s mutual position in the axial direction alongside with a change of the stud’s position in respect to bending plane. The mathematical model for DPM enables us to predict its efficiency. To simulate the fatigue strength of the stud the following was used: Patterson’s and Kenny’s thread deflection factors, solutions for the distributions of the axial load and bending moment along the threads, Neuber’s method for the stress concentration factors in multiplier notches, Heywood’s formulas for the stress due to the thread flank loading and for the combined stresses, as well as the results of the photoelastic analysis of the araldite models under eccentric loading.

     

Effect of supercritical CO2 extraction process parameters on oil yield and pigment content from by‐product hemp cake

This research gives an insight into the possibility of exploiting the one of the food industry's by‐products – pressed hemp cake. The complete recovery of oil from pressed hemp cake was achieved. Residual oil that remained in cake after pressing was extracted with supercritical CO₂ by applying different process parameters. Optimal extraction conditions were determined using response surface methodology. Total pigment contents of the oils obtained were determined. Extraction pressure had the most significant influence on yield and pigment content of extracted hemp cake oil. Depending on the pressure, the chlorophyll a content ranged from 101.11 to 378.28 mg kg^?1 and chlorophyll b from 65.14 to 189.78 mg kg^?1, while total carotene content was in the range from 33.58 to 132.67 mg kg^?1. The remaining oil in pressed hemp cake after supercritical CO₂ extraction was determined to be 0.56 ± 0.08% and the defatted cake was rich in proteins and fibre.     

Characterization of B4C-SiC ceramic composites prepared by ultra-high pressure sintering

Additive-free boron carbide (B₄C) – silicon carbide (SiC) ceramic composites with different B₄C and β-SiC powders ratio were densified using the high-pressure “anvil-type with hollows” apparatus at 1500 °C under a pressure of 4 GPa for 60 s in air. The effect of starting powders ratio on the composites sintering behavior, relative density, microstructural development, and thermomechanical properties was studied. The sintered samples hardness was found to be in the range from 24 to 31 GPa. The thermal conductivity measurements, conducted in the temperature range from room temperature to 1000 °C, showed that the thermal diffusivity of sintered samples was between 6 and 9.5 mm²/s whereas the thermal conductivity was in the range from 16 to 28 W/(m K). The results of this study show that the high-pressure sintering can be a very effective low-temperature densification method for the obtainment of additive-free B₄C - β-SiC ceramic composites.     

An Evaluation of Steel Embrittlement Caused by Welding

The fracture toughness of the HAZ in welds on a HSLA structural steel was assessed by using two types of precracked small-scale fracture-mechanics specimens. The microstructure of the single- and double-pass HAZs was simulated on a Gleeble machine at two different cooling rates. A direct measurement of K_Ic was not possible due to the limited size of both kinds of specimens. A suitable adaptation of the loading diagrams was performed in order to produce relevant data about the fracture properties of the investigated sub-zones of the HAZ.     

Liquid–liquid equilibrium for the systems hydrocarbon–thiophene or pyridine–1-hexyl-3,5-dimethylpyridinium bis(trifluoromethylsulfonyl)imide

Liquid–liquid equilibrium for eight ternary systems involving one hydrocarbon (n-hexane, n-heptane, i-octane or toluene), thiophene or pyridine and an ionic liquid (1-hexyl-3,5-dimethylpyridinium bis(trifluoromethylsulfonyl)imide) was experimentally determined at atmospheric pressure and 25°C. Equilibrium data are presented with binodal curves as well as with tie lines. The suitability of ionic liquid (IL) for extractive desulfurization and denitrification was evaluated in terms of solute distribution ratio and selectivity. Extraction experiments with three-component and seven-component (n-hexane, n-heptane, i-octane, toluene, thiophene, pyridine and IL) systems have been performed. The equilibrium data in three-component systems were well described with Non-Random Two-Liquid (NRTL) and Universal Quasi-Chemical (UNIQUAC) models.     

DMSO Chemically Alters Cell Membranes to Slow Exocytosis and Increase the Fraction of Partial Transmitter Released

Dimethyl sulfoxide (DMSO) is frequently used as a solvent in biological studies and as a vehicle for drug therapy; but the side effects of DMSO, especially on the cell environment, are not well understood, and controls with DMSO are not neutral at higher concentrations. Herein, electrochemical measurement techniques are applied to show that DMSO increases exocytotic neurotransmitter release, while leaving vesicular contents unchanged. In addition, the kinetics of release from DMSO‐treated cells are faster than that of untreated ones. The results suggest that DMSO has a significant influence on the chemistry of the cell membrane, leading to alteration of exocytosis. A speculative chemical mechanism of the effect on the fusion pore during exocytosis is presented.     

PM6 and DFT study of free radical scavenging activity of morin

Flavonoids have long been recognised for their general health-promoting properties, of which their antioxidant activity may play an important role. In this work, we have studied the properties of flavonoid morin using semiempirical and density functional theory (DFT) methods in order to validate the application of the recently developed parametric method 6 (PM6). Reaction enthalpies related to mechanisms of free radical scavenging by flavonoid morin were calculated by DFT and PM6 methods in gas-phase, water, DMSO and benzene. It has been shown that fast semiempirical PM6 method can mimic results obtained by means of more accurate time consuming DFT calculations. Thermodynamically favoured mechanism depends on reaction medium: SPLET (sequential proton loss electron transfer) is preferred in water and DMSO, and HAT (hydrogen atom transfer) is predominant in gas-phase. In benzene these two mechanisms are competitive.     

Reliability of force–time curve characteristics during maximal isometric leg press in differently trained high-level athletes

The aim of this research was to establish the metrologic values of the isometric force–time characteristics of leg extensors in differently trained, healthy male athletes and non-athletes. 99 subjects performed a standardized “isometric leg press” test. Even though the results showed a high statistical significance in terms of representativeness, generalizability and reliability for all contractile characteristics of observed measured variables, different methodological approaches were required in order to obtain the most valid results for differently trained and untrained subjects. Based on the results obtained, and from the aspect of the methodology of testing different isometric force characteristics, it was possible to conclude that the standardization of the isometric leg press requires two trials in football, where the most reliable data was from the first trial (the communality rates (H²) from 0.866 to 0.969). Water polo and basketball require three trials. The most reliable data was from the third and second trial in water polo (H² from 0.909 to 0.986). In basketball the most reliable data was from the second trial (H² from 0.824 to 0.987). The untrained healthy adult population requires four trials, and the most reliable data was from the third trial (H² from 0.961 to 0.995).     

Effects of access phases lengths on performance of IEEE 802.15.6 CSMA/CA

In this paper, we study interplay of prioritizing mechanisms in recently released IEEE 802.15.6 standard for Wireless Body Area Networks (WBANs). Among eight User Priorities (UPs) we study the impact of access phases lengths and CSMA/CA mechanism on the network performance. We consider a star-topology single-hop WBAN in which the hub operates in beacon mode with superframe boundaries. Our study is conducted in saturation regime and an error prone channel in order to indicate performance bounds for all UPs. We have developed an analytical model for the CSMA/CA-based Medium Access Control (MAC) layer of IEEE 802.15.6 which includes Markov chain and probabilistic models for all UPs. In order to validate the analytical model we have developed a simulation model in OPNET. We investigate the effectiveness of deploying exclusive access phases and second random access phase on the network performance. We also examine the medium utilization and normalized throughputs of all UPs. Obtained performance bounds indicate potential tradeoff between the prioritizing parameters which affect the saturation throughputs.     

Potential development of bioethanol production in Vojvodina

The Autonomous Province of Vojvodina is an Autonomous Province in Serbia, containing about 27% of its total population according to the 2002 Census. Contribution of renewable energy sources in total energy consumption of Vojvodina contemporary amounts to less than 1%, apropos 280 GWh/year. By combining of methods of introduction of new and renewable sources, systematic application of methods for increasing of energetic efficacy, as well as of introduction of the new technologies, percentage of contribution of the non-conventional energy sources in Vojvodina could be increased to as much as 20%. This paper presents the potential of development of bioethanol production in Vojvodina. Production of bioethanol on small farms can be successfully applied for processing of only 30 kg of corn per day, with obtaining of crude ethanol in the so-called “brandy ladle” and use of lygnocellulosic agricultural wastes as an energy source. In a case of construction of a larger number of such plants, the only possible solution is seen in the principle of construction of the so-called “satellite plants”, which will on small farm produce crude ethanol, with obtaining and consumption of stillage for animal feeding, and consumption of agricultural wastes as energetic fuels. If stillage is to be used as feed in wet feeding, it is estimated that, because of restrictions established by the magnitude of animal farm, the upper limit of capacity of such enterprises that process is at some 10–15 tons of corn per day, and production of 3000–3500 hL of absolute ethanol per day. In such a case, for animal feeding necessary is to have herd with 1300–1700 of milking cows or 5000–25,000 heads of sheep and/or pigs. Technological model of separate grain processing ad bioethanol production from dextrose hydrolysates of starch is interesting for countries possessing plants for bioethanol production from molasses and plants for cereals processing into starch and dextrose hydrolysates of starch.